ISO 4277:1977
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
Cryolite, natural and artificial Conventional test for evaluation of free fluorides content
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02-16-2019
English, French
11-01-1977
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Applicable to products having contents of AlF3 of more than 0.15 % (m/m) or of NaF of more than 0.4 % (m/m). Covers sintering of a test portion with a known quantity of sodium fluoride in a muffle furnace at a temperature of (790 10) C. Under these conditions, aluminium fluoride in excess of that required by the stoichiometric formula AlF3 .3NaF reacts to form cryolite; extraction of the ground sintered mass with boiling water. Acidification with hydrochloric acid solution to a pH less than 3.7 and titration of the excess sodium fluoride with thorium nitrate solution in the presence of alizarin-S as indicator. Has also been approved by the IUPAC.
| DocumentType |
Standard
|
| Pages |
3
|
| PublisherName |
International Organization for Standardization
|
| Status |
Withdrawn
|
| Standards | Relationship |
| NBN T 03 445 : 1983 | Identical |
| BS 4993-5:1980 | Methods of test for aluminium fluoride for industrial use Determination of moisture content (Karl Fischer method) |
| BS 4993-9:1980 | Methods of test for aluminium fluoride for industrial use Determination of sulphur content (X-ray fluorescence spectrometric method) |
| BS 5050-11(1980) : 1980 | METHODS OF TEST FOR CRYOLITE - DETERMINATION OF SULPHATE CONTENT |
| BS 5050-9(1980) : 1980 | METHODS OF TEST FOR CRYOLITE - DETERMINATION OF MOISTURE CONTENT (KARL FISHER METHOD) |
| ISO/TR 4277:2009 | Cryolite, natural and artificial Conventional test for evaluation of free fluorides content |
| BS 4993-8:1980 | Methods of test for aluminium fluoride for industrial use Determination of sulphate content |
| BS 5050-13(1983) : 1983 | METHODS OF TEST FOR CRYOLITE - DETERMINATION OF PHOSPHORUS CONTENT |
| BS 5050-10(1980) : 1980 | METHODS OF TEST FOR CRYOLITE - DETERMINATION OF MOISTURE CONTENT (GRAVIMETRIC METHOD) |
| BS 5050-12(1980) : 1980 | METHODS OF TEST FOR CRYOLITE - DETERMINATION OF SULFUR CONTENT (X-RAY FLUORESCENCE SPECTROMETRIC METHOD) |
| BS 4993-10:1983 | Methods of test for aluminium fluoride for industrial use Determination of phosphorus content |
| PD ISO/TR 4277:2009 | Cryolite, natural and artificial. Conventional test for evaluation of free fluorides content |
| BS 4993-6:1980 | Methods of test for aluminium fluoride for industrial use Determination of moisture content (gravimetric method) |
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