ISO 15472:2010
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The latest, up-to-date edition.
Surface chemical analysis X-ray photoelectron spectrometers Calibration of energy scales
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French, English
04-19-2010
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ISO 15472:2010 specifies a method for calibrating the binding-energy scales of Xray photoelectron spectrometers, for general analytical purposes, using unmonochromated Al or Mg Xrays or monochromated Al Xrays. It is only applicable to instruments which incorporate an ion gun for sputter cleaning. It further specifies a method to establish a calibration schedule, to test for the binding-energy scale linearity at one intermediate energy, to confirm the uncertainty of the scale calibration at one low and one high binding-energy value, to correct for small drifts of that scale and to define the expanded uncertainty of the calibration of the binding-energy scale for a confidence level of 95 %. This uncertainty includes contributions for behaviours observed in interlaboratory studies but does not cover all of the defects that could occur. ISO 15472 is not applicable to instruments with binding-energy scale errors that are significantly non-linear with energy, to instruments operated in the constant retardation ratio mode at retardation ratios less than 10, to instruments with a spectrometer resolution worse than 1,5 eV, or to instruments requiring tolerance limits of 0,03 eV or less. It does not provide a full calibration check, which would confirm the energy measured at each addressable point on the energy scale and which would have to be performed in accordance with the manufacturer's recommended procedures.
| DevelopmentNote |
Supersedes ISO/DIS 15472. (04/2010)
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| DocumentType |
Standard
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| Pages |
30
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| PublisherName |
International Organization for Standardization
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| Status |
Current
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| Supersedes |
| Standards | Relationship |
| NEN ISO 15472 : 2010 | Identical |
| BS ISO 15472:2010 | Identical |
| NF ISO 15472 : 2006 | Identical |
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| ISO 20903:2011 | Surface chemical analysis Auger electron spectroscopy and X-ray photoelectron spectroscopy Methods used to determine peak intensities and information required when reporting results |
| BS ISO 10810:2010 | Surface chemical analysis. X-ray photoelectron spectroscopy. Guidelines for analysis |
| ISO 10810:2010 | Surface chemical analysis X-ray photoelectron spectroscopy Guidelines for analysis |
| BS ISO 15470:2017 | Surface chemical analysis. X-ray photoelectron spectroscopy. Description of selected instrumental performance parameters |
| ISO 13424:2013 | Surface chemical analysis X-ray photoelectron spectroscopy Reporting of results of thin-film analysis |
| ASTM E 2735 : 2014 : REDLINE | Standard Guide for Selection of Calibrations Needed for X-ray Photoelectron Spectroscopy (XPS) Experiments |
| 10/30199175 DC : 0 | BS ISO 16243 - SURFACE CHEMICAL ANALYSIS - RECORDING AND REPORTING DATA IN X-RAY PHOTOELECTRON SPECTROSCOPY (XPS) |
| BS ISO 13424:2013 | Surface chemical analysis. X-ray photoelectron spectroscopy. Reporting of results of thin-film analysis |
| BS ISO 16243:2011 | Surface chemical analysis. Recording and reporting data in X-ray photoelectron spectroscopy (XPS) |
| 11/30230635 DC : 0 | BS ISO 16129 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - PROCEDURES FOR ASSESSING THE DAY-TO-DAY PERFORMANCE OF AN X-RAY PHOTOELECTRON SPECTROMETER |
| BS ISO 24237:2005 | Surface chemical analysis. X-ray photoelectron spectroscopy. Repeatability and constancy of intensity scale |
| ISO 16243:2011 | Surface chemical analysis — Recording and reporting data in X-ray photoelectron spectroscopy (XPS) |
| PD ISO/TR 18196:2016 | Nanotechnologies. Measurement technique matrix for the characterization of nano-objects |
| 04/30109364 DC : DRAFT FEB 2004 | ISO 24236 - SURFACE CHEMICAL ANALYSIS - AUGER ELECTRON SPECTROSCOPY - REPEATABILITY AND CONSTANCY OF INTENSITY SCALE |
| 03/301547 DC : DRAFT JAN 2003 | ISO 19318 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - REPORTING OF METHODS USED FOR CHARGE CONTROL AND CHARGE CORRECTION |
| 04/30109361 DC : DRAFT FEB 2004 | ISO 24237 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - REPEATABILITY AND CONSTANCY OF INTENSITY SCALE |
| 18/30368969 DC : 0 | BS ISO 16129 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - PROCEDURES FOR ASSESSING THE DAY-TO-DAY PERFORMANCE OF AN X-RAY PHOTOELECTRON SPECTROMETER |
| 09/30191895 DC : 0 | BS ISO 10810 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - GUIDELINES FOR ANALYSIS |
| ASTM E 2108 : 2016 : REDLINE | Standard Practice for Calibration of the Electron Binding-Energy Scale of an X-Ray Photoelectron Spectrometer |
| ISO/TR 18196:2016 | Nanotechnologies — Measurement technique matrix for the characterization of nano-objects |
| ISO 15470:2017 | Surface chemical analysis — X-ray photoelectron spectroscopy — Description of selected instrumental performance parameters |
| BS ISO 16129:2012 | Surface chemical analysis. X-ray photoelectron spectroscopy. Procedures for assessing the day-to-day performance of an X-ray photoelectron spectrometer |
| BS ISO 24236:2005 | Surface chemical analysis. Auger electron spectroscopy. Repeatability and constancy of intensity scale |
| BS ISO 20903:2011 | Surface chemical analysis. Auger electron spectroscopy and X-ray photoelectron spectroscopy. Methods used to determine peak intensities and information required when reporting results |
| ISO 16129:2012 | Surface chemical analysis X-ray photoelectron spectroscopy Procedures for assessing the day-to-day performance of an X-ray photoelectron spectrometer |
| ISO 24237:2005 | Surface chemical analysis — X-ray photoelectron spectroscopy — Repeatability and constancy of intensity scale |
| ISO/IEC 17025:2005 | General requirements for the competence of testing and calibration laboratories |
| ISO 7873:1993 | Control charts for arithmetic average with warning limits |
| ISO 18115-1:2013 | Surface chemical analysis — Vocabulary — Part 1: General terms and terms used in spectroscopy |
| ISO 7870-1:2014 | Control charts Part 1: General guidelines |
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