EN 1601:2017
Current
The latest, up-to-date edition.
Liquid petroleum products - Determination of organic oxygenate compounds and total organically bound oxygen content in unleaded petrol - Method by gas chromatography (O-FID)
08-09-2017
European foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Apparatus
6 Sampling
7 Procedure
8 Calculation
9 Procedure for the determination of a higher
oxygenate compound content
10 Total organically bound oxygen content
11 Expression of results
12 Precision
13 Test report
Annex A (informative) - Guidance on the oxygen selective
detection (O-FID) technique
Bibliography
This European Standard specifies a gas chromatographic method for the quantitative determination, in unleaded petrol having a final boiling point not greater than 220 °C, of individual organic oxygenate compounds in the range 0,17 % (m/m) to 15 % (m/m) in a direct analysis (without dilution), and total organically bound oxygen up to 3,9 % (m/m).For samples for which one of the oxygenate compounds content is higher than 15 % (m/m), a procedure with a dilution of the sample before the analysis is given.NOTE 1The conversion from percent mass to percent volume is done using the calculation mentioned in 8.3 and 9.5.3.NOTE 2Precision data are not available for an oxygenate compound content higher than 15 % (m/m); see Introduction.NOTE 3For the purposes of this European Standard, the terms "% (m/m)" and "% (V/V)" are used to represent respectively the mass fraction, µ, respectively the volume fraction, φ.WARNING - The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this European Standard to take appropriate measures to ensure the safety and health of personnel prior to application of the standard, and fulfil statutory and regulatory requirements for this purpose.
Committee |
CEN/TC 19
|
DevelopmentNote |
Supersedes PREN 1601. (08/2017)
|
DocumentType |
Standard
|
PublisherName |
Comite Europeen de Normalisation
|
Status |
Current
|
Supersedes |
Standards | Relationship |
DIN EN 1601:2017-10 | Identical |
I.S. EN 1601:2017 | Identical |
DIN EN 1601:2016-06 (Draft) | Identical |
PN-EN 1601:2017-09 | Identical |
NEN EN 1601 : 2017 | Identical |
BS EN 1601:2017 | Identical |
BS 2000-408(2014) : 2014 COR 2014 | Identical |
UNE-EN 1601:2018 | Identical |
UNI EN 1601 : 2017 | Identical |
SS-EN 1601:2017 | Identical |
UNI EN 1601 : 2014 | Identical |
NF EN 1601 : 2017 | Identical |
NS EN 1601 : 2017 | Identical |
GOST R EN 1601 : 2007 ERRATA 2009 | Identical |
SN EN 1601 : 2017 | Identical |
NF EN 1601 : 2015 | Identical |
NBN EN 1601 : 2014 | Identical |
BS 2000-408(1997) : 1997 | Identical |
S.R. CEN/TR 15993:2018 | AUTOMOTIVE FUELS - ETHANOL (E85) AUTOMOTIVE FUEL - BACKGROUND TO THE PARAMETERS REQUIRED AND THEIR RESPECTIVE LIMITS AND DETERMINATION |
I.S. EN 14517:2004 | LIQUID PETROLEUM PRODUCTS - DETERMINATION OF HYDROCARBON TYPES AND OXYGENATES IN PETROL - MULTIDIMENSIONAL GAS CHROMATOGRAPHY METHOD |
BS EN ISO 22854:2016 | Liquid petroleum products. Determination of hydrocarbon types and oxygenates in automotive-motor gasoline and in ethanol (E85) automotive fuel. Multidimensional gas chromatography method |
DD CEN/TS 15293:2011 | Automotive fuels. Ethanol (E85) automotive fuel. Requirements and test methods |
BS ISO 8178-5:2008 | Reciprocating internal combustion engines. Exhaust emission measurement Test fuels |
I.S. EN 228:2017 | AUTOMOTIVE FUELS - UNLEADED PETROL - REQUIREMENTS AND TEST METHODS |
BS EN 14517:2004 | Methods of test for petroleum and its products. BS 2000-526: Liquid petroleum products. Determination of hydrocarbon types and oxygenates in petrol. Multidimensional gas chromatography method |
DIN EN 228:2004-03 | AUTOMOTIVE FUELS - UNLEADED PETROL - REQUIREMENTS AND TEST METHODS |
CEN/TR 15993:2018 | Automotive fuels - Ethanol (E85) automotive fuel - Background to the parameters required and their respective limits and determination |
09/30206692 DC : 0 | BS EN 228 - AUTOMOTIVE FUELS - UNLEADED PETROL - REQUIREMENTS AND TEST METHODS |
S.R. CEN TS 15293:2011 | AUTOMOTIVE FUELS - ETHANOL (E85) AUTOMOTIVE FUEL - REQUIREMENTS AND TEST METHODS |
PD CEN/TR 16514:2013 | Automotive fuels. Unleaded petrol containing more than 3,7 % (m/m) oxygen. Roadmap, test methods, and requirements for E10+ petrol |
09/30199323 DC : 0 | BS EN 15293 - AUTOMOTIVE FUELS - ETHANOL (E85) AUTOMOTIVE FUEL REQUIREMENTS AND TEST METHODS |
BS 2000-156(2007) : 2007 | PETROLEUM PRODUCTS AND RELATED MATERIALS - DETERMINATION OF HYDROCARBON TYPES - FLUORESCENT INDICATOR ADSORPTION METHOD |
13/30279896 DC : 0 | BS ISO 8178-5 - RECIPROCATING INTERNAL COMBUSTION ENGINES - EXHAUST EMISSION MEASUREMENT - PART 5: TEST FUELS |
I.S. EN ISO 22854:2016 | LIQUID PETROLEUM PRODUCTS - DETERMINATION OF HYDROCARBON TYPES AND OXYGENATES IN AUTOMOTIVE-MOTOR GASOLINE AND IN ETHANOL (E85) AUTOMOTIVE FUEL - MULTIDIMENSIONAL GAS CHROMATOGRAPHY METHOD (ISO 22854:2016) |
ISO 8178-5:2015 | Reciprocating internal combustion engines Exhaust emission measurement Part 5: Test fuels |
DIN EN 228:2017-08 | AUTOMOTIVE FUELS - UNLEADED PETROL - REQUIREMENTS AND TEST METHODS |
PD CEN/TR 15993:2013 | Automotive fuels. Ethanol (E85) automotive fuel. Background to the parameters required and their respective limits and determination |
12/30263877 DC : 0 | BS EN ISO 22854 - LIQUID PETROLEUM PRODUCTS - DETERMINATION OF HYDROCARBON TYPES AND OXYGENATES IN AUTOMOTIVE-MOTOR GASOLINE - MULTIDIMENSIONAL GAS CHROMATOGRAPHY METHOD |
PREN 228 : DRAFT 2009 | AUTOMOTIVE FUELS - UNLEADED PETROL - REQUIREMENTS AND TEST METHODS |
EN ISO 22854:2016 | Liquid petroleum products - Determination of hydrocarbon types and oxygenates in automotive-motor gasoline and in ethanol (E85) automotive fuel - Multidimensional gas chromatography method (ISO 22854:2016) |
BS EN 15553:2007 | Petroleum products and related materials. Determination of hydrocarbon types. Fluorescent indicator adsorption method |
ISO 22854:2016 | Liquid petroleum products Determination of hydrocarbon types and oxygenates in automotive-motor gasoline and in ethanol (E85) automotive fuel Multidimensional gas chromatography method |
DIN EN 15553:2007-07 | Petroleum products and related materials - Determination of hydrocarbon types - Fluorescent indicator adsorption method |
EN 14517:2004 | Liquid petroleum products - Determination of hydrocarbon types and oxygenates in petrol - Multidimensional gas chromatography method |
EN 228:2012+A1:2017 | Automotive fuels - Unleaded petrol - Requirements and test methods |
UNE-EN ISO 22854:2016 | Liquid petroleum products - Determination of hydrocarbon types and oxygenates in automotive-motor gasoline and in ethanol (E85) automotive fuel - Multidimensional gas chromatography method (ISO 22854:2016) |
S.R. CEN/TR 16514:2013 | AUTOMOTIVE FUELS - UNLEADED PETROL CONTAINING MORE THAN 3,7% (M/M) OXYGEN - ROADMAP, TEST METHODS, AND REQUIREMENTS FOR E10+ PETROL |
I.S. CWA 15293:2005 | AUTOMOTIVE FUELS - ETHANOL E85 - REQUIREMENTS AND TEST METHODS |
I.S. EN 15553:2007 | PETROLEUM PRODUCTS AND RELATED MATERIALS - DETERMINATION OF HYDROCARBON TYPES - FLUORESCENT INDICATOR ADSORPTION METHOD |
CEN/TS 15293:2011 | Automotive fuels - Ethanol (E85) automotive fuel - Requirements and test methods |
EN 15553:2007 | Petroleum products and related materials - Determination of hydrocarbon types - Fluorescent indicator adsorption method |
DIN EN 14517:2004-12 | METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - BS 2000-256: LIQUID PETROLEUM PRODUCTS - DETERMINATION OF HYDROCARBON TYPES AND OXYGENATES IN PETROL - MULTIDIMENSIONAL GAS CHROMATOGRAPHY METHOD |
CEN/TR 16514:2013 | Automotive fuels - Unleaded petrol containing more than 3,7 % (m/m) oxygen - Roadmap, test methods, and requirements for E10+ petrol |
UNE-EN 228:2013 | Automotive fuels - Unleaded petrol - Requirements and test methods |
ISO 3171:1988 | Petroleum liquids — Automatic pipeline sampling |
EN 228:2012+A1:2017 | Automotive fuels - Unleaded petrol - Requirements and test methods |
ISO 3170:2004 | Petroleum liquids — Manual sampling |
ISO 3675:1998 | Crude petroleum and liquid petroleum products Laboratory determination of density Hydrometer method |
EN ISO 12185:1996 | Crude petroleum and petroleum products - Determination of density - Oscillating U-tube method (ISO 12185:1996) |
EN ISO 3675:1998 | Crude petroleum and liquid petroleum products - Laboratory determination of density - Hydrometer method (ISO 3675:1998) |
ISO 12185:1996 | Crude petroleum and petroleum products — Determination of density — Oscillating U-tube method |
ISO 3838:2004 | Crude petroleum and liquid or solid petroleum products Determination of density or relative density Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods |
ISO 4259:2006 | Petroleum products Determination and application of precision data in relation to methods of test |
EN ISO 3170:2004 | Petroleum liquids - Manual sampling (ISO 3170:2004) |
EN ISO 3838:2004 | Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods (ISO 3838:2004) |
EN ISO 3171:1999 | Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988) |
EN ISO 4259:2006 | Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006) |
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