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EN 14103:2011

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of ester and linolenic acid methyl ester contents

Superseded date

01-30-2020

Superseded by

EN 14103:2020

Published date

04-20-2011

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Foreword
1 Scope
2 Principle
3 Reagents
4 Apparatus
5 Sampling
6 Procedure
7 Expression of results
8 Precision
9 Test report
Annex A (informative) - Chromatograms of a FAME samples -
        Determination of ester content - Summary of the
        analysis conditions
Annex B (informative) - Results of an interlaboratory trial
Bibliography

The purpose of this document is to describe a procedure for the determination of the ester content in fatty acid methyl esters (FAME) intended for incorporation into diesel oil. It also allows determining the linolenic acid methyl ester content. It allows verifying that the ester content of FAME is greater than 90 % (m/m) and that the linolenic acid content is between 1 % (m/m) and 15 % (m/m).This method is suitable for FAME which contains methyl esters between C6 and C24.NOTEFor the purposes of this European Standard, the terms "% (m/m) and %(v/v)" are used to represent respectively the mass and volume fractions.WARNING - The use of this method may involve hazardous equipment, materials and operations. This method does not purport to address to all of the safety problems associated with its use, but it is the responsibility of the user to search and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
CEN/TC 307
DevelopmentNote
Supersedes PREN 14103. (08/2011)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Superseded
SupersededBy

09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
I.S. EN 16300:2012 AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE IN FATTY ACID METHYL ESTERS (FAME) - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
I.S. EN 14213:2003 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS
DIN EN 16300:2012-11 Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
UNE-EN 16300:2013 Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
BS EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14214:2014-06 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
BS 2000-607(2012) : 2012 AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE IN FATTY ACID METHYL ESTERS (FAME) - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
PD ISO/TS 17307:2016 Petroleum products. Biodiesel. Determination of total esters content by gas chromatography
I.S. EN 14214:2012 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
ISO/TS 17307:2016 Petroleum products — Biodiesel — Determination of total esters content by gas chromatography
UNI EN 14214 : 2014 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
IP PM EC : 2009(R2016) DETERMINATION OF THE FATTY ACID METHYL ESTER CONTENT OF AVIATION TURBINE FUEL - SOLID PHASE EXTRACTION AND GAS CHROMATOGRAPHY METHOD
PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
BS EN 16300:2012 Automotive fuels. Determination of iodine value in fatty acid methyl esters (FAME). Calculation method from gas chromatographic data
11/30245755 DC : 0 BS EN 16300 - AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
XP M15 032 : 2010 XP AUTOMOTIVE FUELS - FATTY ACID METHYL AND ETHYL ESTERS (FAME AND FAEE) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
ASTM D 8144 : 2018 Standard Test Method for Separation and Determination of Aromatics, Nonaromatics, and FAME Fractions in Middle Distillates by Solid-Phase Extraction and Gas Chromatography
UNI EN 16300 : 2013 AUTOMOTIVE FUELS - DETERMINATION OF IODINE VALUE IN FATTY ACID METHYL ESTERS (FAME) - CALCULATION METHOD FROM GAS CHROMATOGRAPHIC DATA
BS EN 14213:2003 Heating fuels. Fatty acid methyl esters (FAME). Requirements and test methods
EN 14331:2004 Liquid petroleum products - Separation and characterisation of fatty acid methyl esters (FAME) from middle distillates - Liquid chromatography (LC)/gas chromatography (GC) method
EN 16300:2012 Automotive fuels - Determination of iodine value in fatty acid methyl esters (FAME) - Calculation method from gas chromatographic data
UNE-EN 14214:2013 Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods
I.S. EN 14331:2004 LIQUID PETROLEUM PRODUCTS - SEPARATION AND CHARACTERISATION OF FATTY ACID METHYL ESTERS (FAME) FROM MIDDLE DISTILLATES - LIQUID CHROMATOGRAPHY (LC)/GAS CHROMATOGRAPHY (GC) METHOD
BS EN 14331:2004 Liquid petroleum products. Separation and characterisation of fatty acid methyl esters (FAME) from middle distillates. Liquid chromatography (LC)/gas chromatography (GC) method
DIN EN 14331:2004-06 Liquid petroleum products - Separation and characterisation of fatty acid methyl esters (FAME) from middle distillate fuels - Liquid chromatography (LC)/gas chromatography (GC) method
DIN EN 14214:2003-11 LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
DIN EN 14213:2003-11 HEATING FUELS - FATTY ACID METHYL ESTERS (FAME) - REQUIREMENTS AND TEST METHODS

ISO 5555:2001 Animal and vegetable fats and oils — Sampling
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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