ASTM E 2994 : 2016
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Analysis of Titanium and Titanium Alloys by Spark Atomic Emission Spectrometry and Glow Discharge Atomic Emission Spectrometry (Performance-Based Method)
Hardcopy , PDF
01-21-2022
English
05-12-2016
Important note : All end users must be registered with an Account prior to user licenses being assigned.CONTAINED IN VOL. 03.05, 2016 Specifies the analysis of titanium and its alloys by spark atomic emission spectrometry (Spark-AES) and glow discharge atomic emission spectrometry (GD-AES).
| Committee |
E 01
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| DocumentType |
Test Method
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| Pages |
15
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
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| SupersededBy |
1.1This test method describes the analysis of titanium and its alloys by spark atomic emission spectrometry (Spark-AES) and glow discharge atomic emission spectrometry (GD-AES). The titanium specimen to be analyzed may be in the form of a disk, casting, foil, sheet, plate, extrusion or some other wrought form or shape. The elements and ranges covered in the scope by spark-AES of this method are listed below.
| Element | Tested Mass Fraction Range (%) |
| Aluminum | 0.008 to 7.0 |
| Chromium | 0.006 to 0.1 |
| Copper | 0.014 to 0.1 |
| Iron | 0.043 to 0.3 |
| Manganese | 0.005 to 0.1 |
| Molybdenum | 0.014 to 0.1 |
| Nickel | 0.006 to 0.1 |
| Silicon | 0.018 to 0.1 |
| Tin | 0.02 to 0.1 |
| Vanadium | 0.015 to 5.0 |
| Zirconium | 0.013 to 0.1 |
1.1.1The elements oxygen, nitrogen, carbon, niobium, boron, yttrium, palladium, and ruthenium, were included in the ILS but the data did not contain the required six laboratories. Precision tables were provided for informational use only.
1.2The elements and ranges covered in the scope by GD-AES of this method are listed below.
| Element | Tested Mass Fraction Range (%) |
| Aluminum | 0.02 to 7.0 |
| Chromium | 0.006 to 0.1 |
| Copper | 0.028 to 0.1 |
| Iron | 0.09 to 0.3 |
| Molybdenum | 0.016 to 0.1 |
| Nickel | 0.006 to 0.1 |
| Silicon | 0.018 to 0.1 |
| Tin | 0.022 to 0.1 |
| Vanadium | 0.054 to 5.0 |
| Zirconium | 0.026 to 0.1 |
1.3The mass fractions given in the above scope tables are the ranges validated through the interlaboratory study. However, it is known that the techniques used in this standard allow the useable range to be extended higher or lower based on individual instrument and laboratory capabilities, and the spectral characteristics of the specific element wavelength being used. Laboratories must provide sufficient evidence of method validation when extending the analytical range as described in Guide E2857 Validating Analytical Methods.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.
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| SAE AMS 4959 : 2017 | TITANIUM ALLOY WIRE 13.5V - 11CR - 3AL SPRING TEMPER |
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| SAE AMS 2380 : 2017 | APPROVAL AND CONTROL OF PREMIUM-QUALITY TITANIUM ALLOYS |
| SAE AMS 4981 : 2017 | TITANIUM ALLOY BARS, WIRE, AND FORGINGS, 6.0AL - 2.0SN - 4.0ZR - 6.0MO, SOLUTION AND PRECIPITATION HEAT TREATED |
| SAE AMS 4935 : 2017 | TITANIUM ALLOY EXTRUSIONS AND FLASH WELDED RINGS, 6AL - 4V, ANNEALED, BETA PROCESSED |
| SAE AMS 4911 : 2018 | TITANIUM ALLOY, SHEET, STRIP, AND PLATE, 6AL - 4 V, ANNEALED |
| SAE AMS 4940 : 2017 | TITANIUM SHEET, STRIP, AND PLATE COMMERCIALLY PURE ANNEALED, 25.0 KSI (172 MPA) YIELD STRENGTH |
| SAE AMS 4939C : 2017 | TITANIUM ALLOY SHEET, STRIP, AND PLATE, 3AL - 8V - 6CR - 4MO - 4ZR, SOLUTION HEAT TREATED |
| SAE AMS 4978 : 2018 | TITANIUM ALLOY BARS, WIRE, FORGINGS, AND RINGS, 6AL - 6V - 2SN, ANNEALED |
| SAE AMS 4976 : 2017 | TITANIUM ALLOY, FORGINGS, 6.0AL - 2.0SN - 4.0ZR - 2.0MO - 08SI, SOLUTION AND PRECIPITATION HEAT TREATED |
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| SAE AMS 4917 : 2017 | TITANIUM ALLOY SHEET, STRIP, AND PLATE 13.5V - 11CR - 3.0AL - SOLUTION HEAT TREATED |
| SAE AMS 6931 : 2017 | TITANIUM ALLOY BARS, FORGINGS AND FORGING STOCK, 6.0AL - 4.0V, ANNEALED |
| SAE AMS 2249 : 2017 | CHEMICAL CHECK ANALYSIS LIMITS, TITANIUM AND TITANIUM ALLOYS |
| SAE AMS 4942 : 2018 | TITANIUM TUBING, SEAMLESS, ANNEALED, 40.0 KSI (275 MPA) YIELD STRENGTH |
| SAE AMS 4993F : 2017 | TITANIUM ALLOY, BLENDED POWDER COMPACTS, SINTERED, 6AL - 4V |
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| SAE AMS 6950 : 2017 | TITANIUM ALLOY BARS, FORGINGS, AND FORGING STOCK 4AL - 2.5V - 1.5 FE SINGLE HEARTH MELTED, ANNEALED |
| SAE AMS 6951 : 2017 | TITANIUM ALLOY, SHEET 5AL - 4V - 0.75MO - 0.5FE ANNEALED |
| SAE AMS 4915 : 2017 | TITANIUM ALLOY SHEET, STRIP, AND PLATE 8AL - 1V - 1MO SINGLE ANNEALED |
| SAE AMS4933F : 2017 | TITANIUM ALLOY EXTRUSIONS AND FLASH WELDED RINGS 8AL - 1MO - 1V SOLUTION HEAT TREATED AND STABILIZED |
| SAE AMS 4941 G : 2017 | TITANIUM TUBING, WELDED, 40 KSI (276 MPA) YIELD STRENGTH |
| SAE AMS 4954 : 2017 | TITANIUM ALLOY, WELDING WIRE 6AL - 4V |
| SAE AMS 4967 : 2014 | TITANIUM ALLOY, BARS, WIRE, FORGINGS, AND RINGS 6.0AL - 4.0V ANNEALED, HEAT TREATABLE |
| SAE AMS 4971L : 2017 | TITANIUM ALLOY, BARS, WIRE, FORGINGS, AND RINGS, 6AL - 6V - 2SN, ANNEALED, HEAT TREATABLE |
| SAE AMS 4991 : 2014 | TITANIUM ALLOY CASTINGS, INVESTMENT 6AL - 4V HOT ISOSTATIC PRESSED, ANNEAL OPTIONAL |
| SAE AMS 2368 : 2017 | SAMPLING AND TESTING OF WROUGHT TITANIUM RAW MATERIAL EXCEPT FORGINGS AND FORGING STOCK |
| SAE AMS 4945 : 2014 | TITANIUM ALLOY TUBING, SEAMLESS, HYDRAULIC 3AL - 2.5V, CONTROLLED CONTRACTILE STRAIN RATIO COLD WORKED, STRESS RELIEVED |
| ASTM B 348/B348M : 2021 | Standard Specification for Titanium and Titanium Alloy Bars and Billets |
| ASTM F 620 : 2020 | Standard Specification for Titanium Alloy Forgings for Surgical Implants in the Alpha Plus Beta Condition |
| ASTM B 863 : 2019 | Standard Specification for Titanium and Titanium Alloy Wire |
| ASTM F 1472 : 2020 : REV A | Standard Specification for Wrought Titanium-6Aluminum-4Vanadium Alloy for Surgical Implant Applications (UNS R56400) |
| ASTM F 2989 : 2021 | Standard Specification for Metal Injection Molded Unalloyed Titanium Components for Surgical Implant Applications |
| ASTM B 861 : 2019 | Standard Specification for Titanium and Titanium Alloy Seamless Pipe |
| ASTM B 862 : 2019 | Standard Specification for Titanium and Titanium Alloy Welded Pipe |
| ASTM B 1009 : 2020 | Standard Specification for Titanium Alloy Bars for Near Surface Mounts in Civil Structures |
| ASTM F 1108 : 2021 | Standard Specification for Titanium-6Aluminum-4Vanadium Alloy Castings for Surgical Implants (UNS R56406) |
| ASTM B 381 : 2021 | Standard Specification for Titanium and Titanium Alloy Forgings |
| ASTM F 3046 : 2021 | Standard Specification for Wrought Titanium-3Aluminum-2.5Vanadium Alloy for Surgical Implant Applications (UNS R56320) |
| ASTM E 177 : 1990 : REV A : R1996 | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
| ASTM E 177 : 2014 : REDLINE | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
| ASTM E 135 : 2021 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 1329 : 2000 : R2005 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis |
| ASTM E 691 : 2020 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 1507 : 1998 : R2003 | Standard Guide for Describing and Specifying the Spectrometer of an Optical Emission Direct-Reading Instrument (Withdrawn 2003) |
| ASTM E 691 : 2019 : EDT 1 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 135 : 2003 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 1601 : 2019 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 1601 : 1998 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 2972 : 2015 | Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials |
| ASTM E 1601 : 2010 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 1329 : 2010 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019) |
| ASTM E 1329 : 2000 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis |
| ASTM E 1601 : 2012 : REDLINE | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 305 : 2013 | Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves |
| ASTM E 691 : 2009 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 135 : 2002 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 305 : 2013 : REDLINE | Standard Practice for Establishing and Controlling Atomic Emission Spectrochemical Analytical Curves |
| ASTM E 1601 : 2012 | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
| ASTM E 2857 : 2011 : R2021 : EDT 1 | Standard Guide for Validating Analytical Methods |
| ASTM E 691 : 2021 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM E 2857 : 2011 : R2016 | Standard Guide for Validating Analytical Methods |
| ASTM E2972 : 2015(2019) | Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials |
| ASTM E 135 : 2021 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2003 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 135 : 2003 : REV C | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ASTM E 305 : 2021 | Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves |
| ASTM E 2857 : 2011 | Standard Guide for Validating Analytical Methods |
| ASTM E 1507 : 1998 | Standard Guide for Describing and Specifying the Spectrometer of an Optical Emission Direct-Reading Instrument |
| ASTM E 135 : 2020 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
| ISO/IEC Guide 98-3:2008 | Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995) |
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