ASTM E 2787 : 2021
Current
The latest, up-to-date edition.
Standard Test Method for Determination of Thiodiglycol in Soil Using Pressurized Fluid Extraction Followed by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
Hardcopy , PDF
English
05-10-2021
Important note : All end users must be registered with an Account prior to user licenses being assigned.| Committee |
D 34
|
| DocumentType |
Test Method
|
| Pages |
9
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Current
|
| Supersedes |
1.1This procedure covers the determination of thiodiglycol (TDG) in soil using pressurized fluid extraction (PFE). A commercially available PFE system2 is used, followed by analysis using liquid chromatography (LC), and detected with tandem mass spectrometry (MS/MS). TDG is qualitatively and quantitatively determined by this method. This method adheres to single reaction monitoring (SRM) mass spectrometry.
1.2The method detection limit (MDL) and reporting range for TDG are listed in Table 1.
1.2.1The MDL is determined following the Code of Federal Regulations, 40 CFR Part 136, Appendix B.
1.2.2The reporting limit (RL) is calculated from the concentration of the Level 1 calibration standard as shown in Table 4. The RL for this method is 200 ppb. Reporting range concentrations are calculated from Table 4 concentrations assuming a 5 μL injection of the lowest level calibration standard, 5 g sample, and a 2 mL final extract volume.
1.3Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| ASTM E 2554 : 2018 : R2024 : EDT 1 | Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques |
| ASTM D 2777 : 2021 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
| ASTM D 2777 : 2013 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
| ASTM E 2554 : 2018 : EDT 1 | Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques |
| ASTM D 5681 : 2020 | Standard Terminology for Waste and Waste Management |
| ASTM D 5681 : 2022 | Standard Terminology for Waste and Waste Management |
| ASTM D 5681 : 2022 : EDT 1 | Standard Terminology for Waste and Waste Management |
| ASTM D 5681 : 2023 | Standard Terminology for Waste and Waste Management |
Access your standards online with a subscription
Features
-
Simple online access to standards, technical information and regulations.
-
Critical updates of standards and customisable alerts and notifications.
-
Multi-user online standards collection: secure, flexible and cost effective.