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ASTM E 2594 : 2009 : R2014

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance-Based Method)

Available format(s)

Hardcopy , PDF

Superseded date

03-02-2020

Superseded by

ASTM E 2594 : 2020

Language(s)

English

Published date

06-24-2014

US$75.00
Excluding Tax where applicable

CONTAINED IN VOL. 03.05, 2014 Specifies the inductively coupled plasma atomic emission spectrometric analysis of nickel alloys.

Committee
E 01
DocumentType
Test Method
Pages
10
ProductNote
Reconfirmed 2014
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method describes the inductively coupled plasma atomic emission spectrometric analysis of nickel alloys, such as specified by Committee B02, and having chemical compositions within the following limits:

Element

Application
Range (%)

Aluminum

0.01–1.00

Boron

0.001–0.050

Calcium

0.001–0.05

Carbon

0.10–0.20

Chromium

0.01–33.0

Cobalt

0.10–20.0

Copper

0.01–3.00

Iron

0.01–50.0

Lead

0.001–0.01

Magnesium

0.0001–0.100

Manganese

0.01–3.0

Molybdenum

0.01–30.0

Niobium

0.01–6.0

Nickel

25.0–80.0

Nitrogen

0.001–0.20

Oxygen

0.0001–0.003

Phosphorous

0.001–0.030

Sulfur

0.0001–0.010

Silicon

0.01–1.50

Tantalum

0.005–0.10

Tin

0.001–0.020

Titanium

0.001–6.0

Tungsten

0.01–5.0

Vanadium

0.01–1.0

Zirconium

0.01–0.10


1.2The following elements may be determined using this test method. The test method user should carefully evaluate the precision and bias statements of this test method to determine applicability of the test method for the intended use.

Element

Quantification
Range (%)

Aluminum

0.060–1.40

Boron

0.002–0.020

Calcium

0.001–0.003

Copper

0.010–0.52

Magnesium

0.001–0.10

Manganese

0.002–0.65

Niobium

0.020–5.5

Phosphorous

0.004–0.030

Tantalum

0.010–0.050

Tin

0.002–0.018

Titanium

0.020–3.1

Tungsten

0.007–0.11

Vanadium

0.010–0.50

Zirconium

0.002–0.10


1.3This test method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this test method to other elements or different concentration ranges provided that method validation is performed that includes evaluation of method sensitivity, precision, and bias as described in this document. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials or spike recoveries, or both. The user is cautioned to carefully evaluate the validation data against the laboratory’s data quality objectives. Method validation of scope extensions is also a requirement of ISO/IEC 17025.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 8.2.6.3 and safety hazard statements are given in Section 9.

ASTM E 1473 : 2016 Standard Test Methods for Chemical Analysis of Nickel, Cobalt and High-Temperature Alloys
ASTM F 3049 : 2014 Standard Guide for Characterizing Properties of Metal Powders Used for Additive Manufacturing Processes

ASTM E 2027 : 2017 : EDT 1 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials (Withdrawn 2022)
ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
ASTM E 1479 : 2016 Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM E 1479 : 1999 : R2005 Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM E 50 : 2017 : REDLINE Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 1329 : 2000 : R2005 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 2027 : 2009 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 2027 : 2017 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 1479 : 2016 : REDLINE Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM E 1601 : 2019 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1601 : 1998 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1601 : 2010 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1329 : 2010 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
ASTM E 1479 : 1999 : R2011 Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
ASTM E 1329 : 2000 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 1601 : 2012 : REDLINE Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM E 1601 : 2012 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 2027 : 1999 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 2027 : 2005 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ISO Guide 31:2015 Reference materials — Contents of certificates, labels and accompanying documentation
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ISO Guide 34:2009 General requirements for the competence of reference material producers
ASTM E 1479 : 1999 Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
ISO/IEC Guide 98-3:2008 Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)

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