ASTM D 874 : 2013 : REV A : R2018
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
Standard Test Method for Sulfated Ash from Lubricating Oils and Additives
Hardcopy , PDF
07-12-2023
English
05-31-2018
Important note : All end users must be registered with an Account prior to user licenses being assigned.| Committee |
D 02
|
| DocumentType |
Test Method
|
| Pages |
5
|
| ProductNote |
THIS STANDARD IS ALSO REFERES TO EN 14213
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
1.1This test method covers the determination of the sulfated ash from unused lubricating oils containing additives and from additive concentrates used in compounding. These additives usually contain one or more of the following metals: barium, calcium, magnesium, zinc, potassium, sodium, and tin. The elements sulfur, phosphorus, and chlorine can also be present in combined form.
1.2Application of this test method to sulfated ash levels below 0.02 % by mass is restricted to oils containing ashless additives. The lower limit of the test method is 0.005 % by mass sulfated ash.
Note 1:This test method is not intended for the analysis of used engine oils or oils containing lead. Neither is it recommended for the analysis of nonadditive lubricating oils, for which Test Method D482 can be used.
Note 2:There is evidence that magnesium does not react the same as other alkali metals in this test. If magnesium additives are present, the data is interpreted with caution.
Note 3:There is evidence that samples containing molybdenum can give low results because molybdenum compounds are not fully recovered at the temperature of ashing.
1.3Fatty acid methyl ester (FAME) conforming to EN 14213 and EN 14214, when tested using this test method, were shown to meet its precision.
1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| ASTM D 7455 : 2019 | Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis |
| ASTM D 4485 : 2022 : EDT 1 | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 4310 : 2022 : REV A | Standard Test Method for Determination of Sludging and Corrosion Tendencies of Inhibited Mineral Oils |
| ASTM D 7876 : 2013 : R2018 | Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants |
| ASTM D 6751 : 2023 | Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels |
| ASTM D 4682 : 2018 | Standard Specification for Miscibility with Gasoline and Fluidity of Two-Stroke-Cycle Gasoline Engine Lubricants |
| ASTM D 482 : 2019 | Standard Test Method for Ash from Petroleum Products |
| ASTM E 2403 : 2006 : R2018 | Standard Test Method for Sulfated Ash of Organic Materials by Thermogravimetry |
| ASTM D 7578 : 2020 | Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants |
| ASTM D 4057 : 2019 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2013 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2017 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2017 : REV B | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2021 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6299 : 2022 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4057 : 1981 : EDT 2 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2000 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4177 : 2022 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2022 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4057 : 2022 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 1193 : 1970 | Standard Specification For Reagent Water |
| ASTM D 4177 : 2020 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6299 : 2020 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4177 : 2022 : EDT 1 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
Access your standards online with a subscription
Features
-
Simple online access to standards, technical information and regulations.
-
Critical updates of standards and customisable alerts and notifications.
-
Multi-user online standards collection: secure, flexible and cost effective.