ASTM D 8127 : 2017 : EDT 1
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Coupled Particulate and Elemental Analysis using X-ray Fluorescence (XRF) for In-Service Lubricants
Hardcopy , PDF
05-25-2023
English
05-01-2018
CONTAINED IN VOL. 05.05, 2018 Defines particle analysis2 test method for in-service lubricants describes using a combination of pore blockage particle counting and energy dispersive X-ray fluorescence (EDXRF) spectrometry for the quantitative determination of solid particle counts larger than four (4) micrometres, and elemental content of suspended particulate of iron (Fe) and copper (Cu) in such lubricants.
Committee |
D 02
|
DocumentType |
Test Method
|
Pages |
8
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy | |
Supersedes |
1.1This automatic wear particle analysis2 test method for in-service lubricants describes using a combination of pore blockage particle counting and energy dispersive X-ray fluorescence (EDXRF) spectrometry for the quantitative determination of solid particle counts larger than four (4) micrometres, and elemental content of suspended particulate of iron (Fe) and copper (Cu) in such lubricants.
1.2This test method provides for the determination of the elemental content of suspended particulate of Fe greater than 4 μm in the range of 6 mg/kg to 223 mg/kg. Suspended particulate of copper greater than 4 μm is determined in the range of 3.5 mg/kg to 92.4 mg/kg in the lubricant. Total particle count greater than 4 μm is determined in the range of 11 495 particles/mL greater than 4 μm to 2 169 500 particles/mL greater than 4 μm in the lubricant.
1.3This test method is applicable to all known in-service lubricants (API Groups I-V) at any stage of degradation.
1.4This test method uses an empirical inter-element correction methodology.
1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ASTM D 7751 : 2012 | Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis |
ASTM D 4057 : 2006 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
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ASTM D 4177 : 2015 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
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ASTM E 1621 : 2021 | Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry |
ASTM D 7751 : 2011 : EDT 1 | Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis |
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ASTM D 7751 : 2011 | Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis |
ASTM D 7751 : 2016 | Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis |
ASTM D 4057 : 2022 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
ASTM D 4177 : 2016 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
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ASTM D 4177 : 1995 : R2005 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
ASTM D 7720 : 2011 : R2017 | Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination |
ASTM D 5854 : 2019 : REV A | Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products |
ASTM E 1621 : 1994 : R1999 | Standard Guide for X-Ray Emission Spectrometric Analysis |
ASTM D 4057 : 1995 : R2000 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
ASTM D 7751 : 2016 : REDLINE | Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis |
ASTM D 4177 : 2022 : EDT 1 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
ASTM D 4177 : 2015 : REV A | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
ASTM D 4057 : 2006 : R2011 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
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ASTM D 5854 : 1996 : R2015 | Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products |
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