ASTM D 7756 : 2019
Current
The latest, up-to-date edition.
Standard Test Method for Residues in Liquefied Petroleum (LP) Gases by Gas Chromatography with Liquid, On-Column Injection
Hardcopy , PDF
English
06-18-2019
This test method covers the determination, by gas chromatography, of soluble hydrocarbon materials, sometimes called “oily residue,” which can be present in liquefied petroleum (LP) gases and which are substantially less volatile than the LPG product.
Committee |
D 02
|
DocumentType |
Test Method
|
Pages |
13
|
PublisherName |
American Society for Testing and Materials
|
Status |
Current
|
Supersedes |
1.1This test method covers the determination, by gas chromatography, of soluble hydrocarbon materials, sometimes called “oily residue,” which can be present in liquefied petroleum (LP) gases and which are substantially less volatile than the LPG product.
1.2This test method quantifies, in the range of 10 mg/kg to 600 mg/kg (ppm mass), the residue with a boiling point between 174 °C and 522 °C (C10 to C40) in LPG. Higher boiling materials, or materials that adhere permanently to the chromatographic column, will not be detected.
1.3Appendix X3, Appendix X4, and Appendix X6 describe additional applications which could be performed based on the hardware and procedures described in this test method. Appendix X3 describes a test procedure for expanding the analysis range to benzene, Appendix X4 describes a test procedure for the analysis of diisopropanolamine, and Appendix X6 describes a test procedure for the analysis of heavy residues or contaminants from C40 to about C60 in LPG.
1.4The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.
1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ASTM D 1265 : 1997 | Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method) |
ASTM D 6299 : 2013 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 2421 : 2002 : R2007 | Standard Practice for Interconversion of Analysis of C<i><inf>5</inf></i> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis |
ASTM D 2158 : 2016 | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases |
ASTM D 2421 : 2021 | Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis |
ASTM D 6667 : 2001 | Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence |
ASTM D 6299 : 2017 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
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ASTM D 6300 : 2017 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 6299 : 2009 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 1835 : 1997 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 2421 : 1995 | Standard Practice for Interconversion of Analysis of C<sub>5</sub> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Weight Basis |
ASTM D 2163 : 2023 : EDT 1 | Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography |
ASTM D 2158 : 2004 | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases |
ASTM D 6300 : 2017 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 2163 : 2014 : EDT 1 | Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography |
ASTM D 2163 : 2007 | Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography |
ASTM D 6299 : 2013 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 3700 : 2014 | Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder |
ASTM D 6299 : 2021 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6299 : 2010 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6667 : 2004 | Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence |
ASTM D 2158 : 2011 | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases |
ASTM D 2421 : 2018 | Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis |
ASTM D 6299 : 2022 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 1265 : 2023 : REV A | Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method |
ASTM D 6300 : 2016 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 2158 : 1989 | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases |
ASTM D 3700 : 1994 | Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder |
ASTM D 6300 : 2004 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 1835 : 2018 : REV A | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 1835 : 2012 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 6300 : 2019 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 6299 : 2023 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 2421 : 2001 | Standard Practice for Interconversion of Analysis of C<sub>5</sub> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Weight Basis |
ASTM D 2598 : 2012 | Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis |
ASTM D 6300 : 2021 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
ASTM D 6300 : 2019 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 6667 : 2004 : R2010 | Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence |
ASTM D 6300 : 2023 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
ASTM D 6300 : 2020 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
ASTM D 2421 : 2002 | Standard Practice for Interconversion of Analysis of C<sub>5</sub> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Weight Basis |
ASTM D 6299 : 2000 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 3700 : 2021 | Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder |
ASTM D 6299 : 2010 : EDT 2 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6299 : 2016 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 2598 : 2002 | Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis |
ASTM D 6300 : 2023 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
ASTM D 6299 : 2019 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 1835 : 2003 : REV A | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 6667 : 2010 | Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence |
ASTM D 6300 : 2020 : REV B | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
ASTM D 6299 : 2023 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6299 : 2000 : REV A | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6300 : 2006 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 6300 : 2014 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM E 355 : 1996 : R2021 : EDT 1 | Standard Practice for Gas Chromatography Terms and Relationships |
ASTM D 1835 : 2003 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 6300 : 2015 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 6667 : 2014 : R2019 | Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence |
ASTM D 6300 : 1999 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 1835 : 2013 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 2421 : 2013 | Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis |
ASTM D 6299 : 2023 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 1835 : 2020 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 6299 : 2020 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6299 : 2008 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6667 : 2014 : R2019 | Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence |
ASTM D 1835 : 2018 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 2158 : 2002 | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases |
ASTM D 2598 : 1996 : R2001 | Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis |
ASTM D 2421 : 2021 : EDT 1 | Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis |
ASTM D 1265 : 2004 | Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method) |
ASTM D 6300 : 2013 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 3700 : 2012 | Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder |
ASTM D 6299 : 2002 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 2158 : 2016 : REV A | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases |
ASTM D 2163 : 1991 : R1996 | Standard Test Method for Analysis of Liquefied Petroleum (LP) Gases and Propene Concentrates by Gas Chromatography (Withdrawn 2005) |
ASTM D 1835 : 2022 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 3700 : 2007 | Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder |
ASTM D 6667 : 2014 | Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence |
ASTM D 1835 : 2016 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 6300 : 2008 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 6300 : 2003 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 1265 : 2011 : R2017 : EDT 1 | Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method |
ASTM D 6300 : 2007 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 6299 : 2022 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 2158 : 1997 : EDT 1 | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases |
ASTM D 1835 : 2011 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 2598 : 2016 | Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis |
ASTM D 1265 : 2005 | Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method) |
ASTM D 6300 : 2002 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 2598 : 2002 : R2007 | Standard Practice for Calculation of Certain Physical Properties of Liquefied Petroleum (LP) Gases from Compositional Analysis |
ASTM D 1265 : 2004 : REV A | Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method) |
ASTM D 1265 : 2011 | Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method |
ASTM D 2158 : 2016 : REV A : EDT 1 | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases |
ASTM D 6300 : 2016 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 2163 : 2014 | Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography |
ASTM D 2163 : 2014 : R2019 | Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography |
ASTM D 3700 : 2016 | Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder |
ASTM E 355 : 1996 : R2014 | Standard Practice for Gas Chromatography Terms and Relationships |
ASTM D 6299 : 2007 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 1265 : 2023 | Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method |
ASTM D 6299 : 2007 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6299 : 2020 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 2163 : 2023 | Standard Test Method for Determination of Hydrocarbons in Liquefied Petroleum (LP) Gases and Propane/Propene Mixtures by Gas Chromatography |
ASTM D 1265 : 2022 | Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method |
ASTM D 6299 : 2017 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6300 : 2014 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
ASTM D 1835 : 2005 | Standard Specification for Liquefied Petroleum (LP) Gases |
ASTM D 2158 : 2021 | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases |
ASTM D 2421 : 2019 | Standard Practice for Interconversion of Analysis of C<emph type="ital"><inf>5</inf ></emph> and Lighter Hydrocarbons to Gas-Volume, Liquid-Volume, or Mass Basis |
ASTM D 6299 : 2002 | Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance |
ASTM D 6300 : 2024 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
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