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ASTM D 7151 : 2015

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Determination of Elements in Insulating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

Available format(s)

Hardcopy , PDF

Superseded date

01-17-2024

Language(s)

English

Published date

06-18-2015

US$75.00
Excluding Tax where applicable

Committee
D 27
DocumentType
Test Method
Pages
8
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method describes the determination of metals and contaminants in insulating oils by inductively coupled plasma atomic emission spectrometry (ICP-AES). The specific elements are listed in Table 1. This test method is similar to Test Method D5185, but differs in methodology, which results in the greater sensitivity required for insulating oil applications.

(A)These wavelengths are only suggested and do not represent all possible choices.

1.2This test method uses oil-soluble metals for calibration and does not purport to quantitatively determine insoluble particulates. Analytical results are particle size dependent, and low results are obtained for particles larger than several micrometers.2

1.3This test method determines the dissolved metals (which can originate from overheating or arcing, or both) and a portion of the particulate metals (which generally originate from a wear mechanism). While this ICP method detects nearly all particles less than several micrometers, the response of larger particles decreases with increasing particle size because larger particles are less likely to make it through the nebulizer and into the sample excitation zone.

1.4This test method includes an option for filtering the oil sample for those users who wish to separately determine dissolved metals and particulate metals (and hence, total metals).

1.5Elements present at concentrations above the upper limit of the calibration curves can be determined with additional, appropriate dilutions and with no degradation of precision.

1.6The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

ASTM D 117 : 2018 Standard Guide for Sampling, Test Methods, and Specifications for Electrical Insulating Liquids
ASTM D 117 : 2022 Standard Guide for Sampling, Test Methods, and Specifications for Electrical Insulating Liquids

ASTM D 2864 : 2009 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM D 923 : 2015 : R2023 Standard Practices for Sampling Electrical Insulating Liquids
ASTM D 5185 : 1997 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM C 1109 : 2004 Standard Practice for Analysis of Aqueous Leachates from Nuclear Waste Materials Using Inductively Coupled Plasma-Atomic Emission Spectrometry
ASTM D 2864 : 2017 : REV A Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 5185 : 2005 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 5185 : 2002 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 5185 : 2018 Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 923 : 2015 Standard Practices for Sampling Electrical Insulating Liquids
ASTM D 4307 : 1999 : R2004 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 5185 : 2013 : EDT 1 Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 2864 : 2006 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 5185 : 2013 Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 4307 : 1999 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 2864 : 2010 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 2864 : 2002 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 2864 : 2000 : REV A Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 4307 : 2017 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 2864 : 2021 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 4307 : 2017 : R2021 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 4307 : 1999 : R2010 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 5185 : 2009 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 2864 : 2010 : EDT 1 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 5185 : 2002 : EDT 1 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 2864 : 2019 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 5185 : 2002 : EDT 2 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 2864 : 2007 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM C 1109 : 1998 Standard Test Method for Analysis of Aqueous Leachates from Nuclear Waste Materials Using Inductively Coupled Plasma-Atomic Emission Spectrometry
ASTM C 1109 : 2010 Standard Practice for Analysis of Aqueous Leachates from Nuclear Waste Materials Using Inductively Coupled Plasma-Atomic Emission Spectrometry
ASTM D 2864 : 2020 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM C 1109 : 2010 : R2015 Standard Practice for Analysis of Aqueous Leachates from Nuclear Waste Materials Using Inductively Coupled Plasma-Atomic Emission Spectroscopy
ASTM D 4307 : 1999 : R2015 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 2864 : 2017 Standard Terminology Relating to Electrical Insulating Liquids and Gases
ASTM D 2864 : 2021 : REV A Standard Terminology Relating to Electrical Insulating Liquids and Gases

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