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ASTM D 5453 : 2019 : REV A

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence

Available format(s)

Hardcopy , PDF

Superseded date

11-01-2024

Superseded by

ASTM D 5453 : 2024

Language(s)

English

Published date

07-01-2019

US$83.00
Excluding Tax where applicable

Committee
D 02
DocumentType
Test Method
Pages
12
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the determination of total sulfur in liquid hydrocarbons, boiling in the range from approximately 25 °C to 400 °C, with viscosities between approximately 0.2 cSt and 20 cSt (mm2/s) at room temperature.

1.2Three separate interlaboratory studies (ILS) on precision, and three other investigations that resulted in an ASTM research report, have determined that this test method is applicable to naphthas, distillates, engine oil, ethanol, Fatty Acid Methyl Ester (FAME), and engine fuel such as gasoline, oxygen enriched gasoline (ethanol blends, E-85, M-85, RFG), diesel, biodiesel, diesel/biodiesel blends, and jet fuel. Samples containing 1.0 mg/kg to 8000 mg/kg total sulfur can be analyzed (Note 1).

Note 1:Estimates of the pooled limit of quantification (PLOQ) for the precision studies were calculated. Values ranged between less than 1.0 mg/kg and less than 5.0 mg/kg (see Section 9 and 16.1).

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For warning statements, see 3.1, 7.3, 7.4, Section 8, and 9.1.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 7578 : 2018 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 1405/D1405M : 2008 : R2013 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels (Withdrawn 2019)
ASTM D 3338/D3338M : 2009 : R2014 : EDT 2 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 7166 : 2010 : R2015 Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous Fuels
ASTM D 7620 : 2010 : R2015 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbon Based Fuels by Continuous Injection, Air Oxidation and Ultraviolet Fluorescence Detection
ASTM D 6615 : 2015 : REV A Standard Specification for Jet B Wide-Cut Aviation Turbine Fuel
ASTM D 7422 : 2017 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
ASTM D 910 : 2017 : REV A Standard Specification for Leaded Aviation Gasolines
ASTM D 4809 : 2018 Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)
ASTM D 3699 : 2018 : REV A Standard Specification for Kerosine
ASTM D 4806 : 2019 Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 1655 : 2019 Standard Specification for Aviation Turbine Fuels
ASTM D 7566 : 2019 Standard Specification for Aviation Turbine Fuel Containing Synthesized Hydrocarbons
ASTM D 6227 : 2018 Standard Specification for Unleaded Aviation Gasoline Containing a Non-hydrocarbon Component
ASTM D 7547 : 2018 : REV A Standard Specification for Hydrocarbon Unleaded Aviation Gasoline
ASTM D 8047 : 2018 Standard Test Method for Evaluation of Engine Oil Aeration Resistance in a Caterpillar C13 Direct-Injected Turbocharged Automotive Diesel Engine
ASTM D 5797 : 2018 Standard Specification for Methanol Fuel Blends (M51–M85) for Methanol-Capable Automotive Spark-Ignition Engines
ASTM D 4814 : 2019 Standard Specification for Automotive Spark-Ignition Engine Fuel
ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 7862 : 2019 Standard Specification for Butanol for Blending with Gasoline for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 4054 : 2019 Standard Practice for Evaluation of New Aviation Turbine Fuels and Fuel Additives
ASTM D 7826 : 2019 Standard Guide for Evaluation of New Aviation Gasolines and New Aviation Gasoline Additives
ASTM D 6751 : 2019 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
ASTM D 7467 : 2019 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
ASTM D 396 : 2019 Standard Specification for Fuel Oils
ASTM D 8048 : 2019 Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
ASTM D 8111 : 2019 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIH, Spark-Ignition Engine
ASTM D 2880 : 2018 : REV A Standard Specification for Gas Turbine Fuel Oils
ASTM D 8114 : 2019 : REV A Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VIE Spark Ignition
ASTM D 8275 : 2019 Standard Specification for Gasoline-like Test Fuel for Compression-Ignition Engines
ASTM D 7320 : 2018 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 6984 : 2018 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIF, Spark-Ignition Engine
ASTM D 8011 : 2018 Standard Specification for Natural Gasoline as a Blendstock in Ethanol Fuel Blends or as a Denaturant for Fuel Ethanol
ASTM D 6334 : 2012 : R2017 : EDT 1 Standard Test Method for Sulfur in Gasoline by Wavelength Dispersive X-Ray Fluorescence (Withdrawn 2022)
ASTM D 4529 : 2017 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 4868 : 2017 Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels
ASTM D 240 : 2017 Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter
ASTM D 5967 : 2017 Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine
ASTM D 6074 : 2015 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
ASTM D 7156 : 2017 Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine
ASTM D 7223 : 2017 Standard Specification for Aviation Certification Turbine Fuel
ASTM D 7589 : 2016 Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VID Spark Ignition Engine<rangeref></rangeref >
ASTM D 7666 : 2012 Standard Specification for Triglyceride Burner Fuel
ASTM D 8074 : 2018 Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine
ASTM D 8076 : 2018 Standard Specification for 100 Research Octane Number Test Fuel for Automotive Spark-Ignition Engines
ASTM D 8147 : 2017 Standard Specification for Special-Purpose Test Fuels for Aviation Compression-Ignition Engines
ASTM D 8235 : 2021 Standard Specification for Ethyl Tertiary-Butyl Ether (ETBE) for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 8111 : 2023 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIH, Spark-Ignition Engine
ASTM D 4054 : 2024 Standard Practice for Evaluation of New Aviation Turbine Fuels and Fuel Additives
ASTM D 8011 : 2019 Standard Specification for Natural Gasoline as a Blendstock in Ethanol Fuel Blends or as a Denaturant for Fuel Ethanol
ASTM D 7223 : 2021 Standard Specification for Aviation Certification Turbine Fuel
ASTM D 7422 : 2023 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
ASTM D 7826 : 2024 Standard Guide for Evaluation of New Aviation Gasolines and New Aviation Gasoline Additives
ASTM D 8076 : 2024 Standard Specification for 95, 98, and 100 Research Octane Number Test Fuels for Automotive Spark-Ignition Engines
ASTM D 4806 : 2021 : REV A Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 6074 : 2015 : R2022 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
ASTM D 5797 : 2021 Standard Specification for Methanol Fuel Blends (M51–M85) for Methanol-Capable Automotive Spark-Ignition Engines
ASTM D 7166 : 2023 Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous Fuels
ASTM D 240 : 2019 Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter
ASTM D 7468 : 2022 Standard Test Method for Cummins ISM Test
ASTM D 8226 : 2021 : REV A : EDT 1 Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VIF Spark Ignition Engine<rangeref></rangeref >
ASTM D 8291 : 2024 : REV A Standard Test Method for Evaluation of Performance of Automotive Engine Oils in the Mitigation of Low-Speed, Preignition in the Sequence IX Gasoline Turbocharged Direct-Injection, Spark-Ignition Engine
ASTM D 6984 : 2018 : EDT 1 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIF, Spark-Ignition Engine
ASTM D 910 : 2024 Standard Specification for Leaded Aviation Gasolines
ASTM D 8275 : 2022 Standard Specification for Gasoline-like Test Fuel for Compression-Ignition Engines
ASTM D 3699 : 2019 Standard Specification for Kerosine
ASTM D 6227 : 2024 Standard Specification for Unleaded Aviation Gasoline Containing a Non-hydrocarbon Component
ASTM D 7666 : 2012 : R2019 Standard Specification for Triglyceride Burner Fuel
ASTM D 7467 : 2023 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
ASTM D 3338/D3338M : 2020 : REV A Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 7566 : 2024 : REV B Standard Specification for Aviation Turbine Fuel Containing Synthesized Hydrocarbons
ASTM D 7620 : 2010 : R2020 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbon Based Fuels by Continuous Injection, Air Oxidation and Ultraviolet Fluorescence Detection
ASTM D 2880 : 2023 Standard Specification for Gas Turbine Fuel Oils
ASTM D 7547 : 2023 Standard Specification for Hydrocarbon Unleaded Aviation Gasoline
ASTM D 6751 : 2024 Standard Specification for Biodiesel Fuel Blendstock (B100) for Middle Distillate Fuels
ASTM D 4814 : 2024 : REV A Standard Specification for Automotive Spark-Ignition Engine Fuel
ASTM D 7484 : 2023 : REV A Standard Test Method for Evaluation of Automotive Engine Oils for Valve-Train Wear Performance in Cummins ISB Medium-Duty Diesel Engine
ASTM D 8114 : 2023 : REV A Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VIE Spark Ignition
ASTM D 7455 : 2024 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 8048 : 2024 Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
ASTM D 8074 : 2023 Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine
ASTM D 7589 : 2016 : EDT 1 Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VID Spark Ignition Engine<rangeref></rangeref >
ASTM D 6593 : 2018 : EDT 1 Standard Test Method for Evaluation of Automotive Engine Oils for Inhibition of Deposit Formation in a Spark-Ignition Internal Combustion Engine Fueled with Gasoline and Operated Under Low-Temperature, Light-Duty Conditions
ASTM D 7862 : 2021 Standard Specification for Butanol for Blending with Gasoline for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 5967 : 2021 Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine
ASTM D 1655 : 2024 Standard Specification for Aviation Turbine Fuels
ASTM D 7156 : 2024 Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine
ASTM D 8147 : 2024 Standard Specification for Special-Purpose Test Fuels for Aviation Compression-Ignition Engines
ASTM D 396 : 2024 Standard Specification for Fuel Oils
ASTM D 975 : 2024 : REV A Standard Specification for Diesel Fuel
ASTM D 7320 : 2018 : EDT 1 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 8434 : 2021 Standard Specification for Unleaded Aviation Gasoline Test Fuel Containing Organo-metallic Additive
ASTM D 4529 : 2024 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 7549 : 2024 Standard Test Method for Evaluation of Heavy-Duty Engine Oils under High Output Conditions—Caterpillar C13 Test Procedure
ASTM D 6615 : 2022 Standard Specification for Jet B Wide-Cut Aviation Turbine Fuel
ASTM D 7578 : 2020 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 5798 : 2021 Standard Specification for Ethanol Fuel Blends for Flexible-Fuel Automotive Spark-Ignition Engines

ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 6299 : 2013 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2017 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2017 : REV B Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1250 : 2019 : EDT 1 Standard Guide for the Use of the Joint API and ASTM Adjunct for Temperature and Pressure Volume Correction Factors for Generalized Crude Oils, Refined Products, and Lubricating Oils: API MPMS Chapter 11.1
ASTM D 4052 : 2018 : REV A Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 1298 : 2012 : REV B : R2017 : EDT 1 Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 6299 : 2021 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2022 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 1298 : 2012 : REV B : R2017 Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 6299 : 2023 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2000 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1250 : 1980 : R1997 : EDT 1 Standard Guide for Petroleum Measurement Tables
ASTM D 6299 : 2023 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4177 : 2022 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 6299 : 2023 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4052 : 1996 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
ASTM D 6299 : 2022 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 4052 : 2022 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 4177 : 2020 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 1298 : 1985 : R1990 : EDT 1 Standard Practice for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 6299 : 2020 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 4177 : 2022 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products

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