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ASTM D 4951 : 2014 : REDLINE

Current

Current

The latest, up-to-date edition.

Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry

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English

Published date

10-01-2014

US$75.00
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CONTAINED IN VOL. 05.02, 2015 Defines the quantitative determination of barium, boron, calcium, copper, magnesium, molybdenum, phosphorus, sulfur, and zinc in unused lubricating oils and additive packages.

Committee
D 02
DocumentType
Redline
Pages
9
PublisherName
American Society for Testing and Materials
Status
Current

1.1This test method covers the quantitative determination of barium, boron, calcium, copper, magnesium, molybdenum, phosphorus, sulfur, and zinc in unused lubricating oils and additive packages.

1.2The precision statements are valid for dilutions in which the mass % sample in solvent is held constant in the range of 1 to 5 mass % oil.

1.3The precision tables define the concentration ranges covered in the interlaboratory study. However, both lower and higher concentrations can be determined by this test method. The low concentration limits are dependent on the sensitivity of the ICP instrument and the dilution factor. The high concentration limits are determined by the product of the maximum concentration defined by the linear calibration curve and the sample dilution factor.

1.4Sulfur can be determined if the instrument can operate at a wavelength of 180 nm.

1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

MIL-PRF-17331 Revision K:2013 LUBRICATING OIL, STEAM TURBINE AND GEAR, MODERATE SERVICE
MIL PRF 009000 : K LUBRICATING OIL, SHIPBOARD INTERNAL COMBUSTION ENGINE, HIGH-OUTPUT DIESEL
MIL-PRF-46167 Revision D:2005 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, ARCTIC
MIL-PRF-9000 Revision L:2014 Lubricating Oil, Shipboard Internal Combustion Engine, High-Output Diesel
API 1509 : 2002 ENGINE OIL LICENSING AND CERTIFICATION SYSTEM
SAE MS 1005 : 2017 LUBRICANTS, INDUSTRIAL OILS, AND RELATED PRODUCTS TYPE HF FIRE-RESISTANT HYDRAULIC FLUIDS - SPECIFICATION
ASTM D 7040 :2004 Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 7578 : 2015-06 GUIDE FOR CALIBRATION REQUIREMENTS FOR ELEMENTAL ANALYSIS OF PETROLEUM PRODUCTS AND LUBRICANTS
ASTM D 7040 : 2004 : R2010 Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM E 2097 : 2000 : R2014 Standard Guide for Determining the Impact of Extractables from Non-Metallic Materials on the Safety of Biotechnology Products (Withdrawn 2022)
ASTM D 4485 : 2017-03 SPECIFICATION FOR PERFORMANCE OF ACTIVE API SERVICE CATEGORY ENGINE OILS
BS EN ISO 4263-4:2006 Petroleum and related products. Determination of the ageing behaviour of inhibited oils and fluids. TOST test Procedure for industrial gear oils
A-A-52306 Revision A:1995 LUBRICATING OIL, HEAVY-DUTY DIESEL ENGINE
NF ISO 24254 : 2008 LUBRICANTS, INDUSTRIAL OILS AND RELATED PRODUCTS (CLASS L) - FAMILY E (INTERNAL COMBUSTION ENGINE OILS) - SPECIFICATIONS FOR OILS FOR USE IN FOUR-STROKE CYCLE MOTORCYCLE GASOLINE ENGINES AND ASSOCIATED DRIVE TRAINS (CATEGORIES EMA AND EMB)
ASTM E 2097 : 2000 Standard Guide for Determining the Impact of Extractables from Non-Metallic Materials on the Safety of Biotechnology Products
MIL-DTL-32353 Revision A:2012 HYDRAULIC & LUBRICATING OIL, SYNTHETIC HYDROCARBON BASE
SAE MS 1004 : 2017 LUBRICANTS, INDUSTRIAL OILS, AND RELATED PRODUCTS TYPE H (HYDRAULIC FLUIDS) - SPECIFICATION
SAE J 357 : 2016 PHYSICAL AND CHEMICAL PROPERTIES OF ENGINE OILS
ASTM D 7876 : 2013 Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants
BIS IS 13656 : 2014 INTERNAL COMBUSTION ENGINE CRANKCASE OILS FOR AUTOMOTIVE APPLICATION (DIESEL AND GASOLINE) - SPECIFICATION
ASTM D 4857 : 2012 : REDLINE Standard Test Method for Determination of the Ability of Lubricants to Minimize Ring Sticking and Piston Deposits in Two-Stroke-Cycle Gasoline Engines Other Than Outboards
ASTM D 6074 : 2015 : REDLINE Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
ASTM D 7040 : 2004 : R2015 Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
SAE J 2359 : 1998 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, MILITARY COMBAT/TACTICAL SERVICE
SAE J 183 : 2017 ENGINE OIL PERFORMANCE AND ENGINE SERVICE CLASSIFICATION (OTHER THAN 'ENERGY CONSERVING')
06/30159746 DC : 0 BS EN 50503 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - STANDARD FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
MIL-PRF-21260 Revision E:1998 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATIVE BREAK-IN
SAE J 2361 : 1998 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATION BREAK-IN
DIN EN ISO 4263-4:2006-05 Petroleum and related products - Determination of the ageing behaviour of inhibited oils and fluids - TOST test - Part 4: Procedure for industrial gear oils (ISO 4263-4:2006)
ASTM D 8110 : 2017 Standard Test Method for Elemental Analysis of Distillate Products by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
ASTM D 6443 : 2014 : REDLINE TEST METHOD FOR DETERMINATION OF CALCIUM, CHLORINE, COPPER, MAGNESIUM, PHOSPHORUS, SULFUR, AND ZINC IN UNUSED LUBRICATING OILS AND ADDITIVES BY WAVELENGTH DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY (MATHEMATICAL CORRECTION PROCEDURE)
ASTM D 7303 : 2017 : REDLINE Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry
SAE J 1260 : 2012 STANDARD OIL FILTER TEST OIL
ASTM E 2097 : 2000 : R2006 Standard Guide for Determining the Impact of Extractables from Non-Metallic Materials on the Safety of Biotechnology Products
EN ISO 4263-4:2006 Petroleum and related products - Determination of the ageing behaviour of inhibited oils and fluids - TOST test - Part 4: Procedure for industrial gear oils (ISO 4263-4:2006)
BS ISO 24254:2007 Lubricants, industrial oils and related products (class L). Family E (internal combustion engine oils). Specifications for oils for use in four-stroke cycle motorcycle gasoline engines and associated drivetrains (categories EMA and EMB)
API 1525A : 1ED 2012 BULK ENGINE OIL CHAIN OF CUSTODY AND QUALITY DOCUMENTATION
SAE MS 1002 : 2017 LUBRICANTS, INDUSTRIAL OILS, AND RELATED PRODUCTS TYPE C (GEARS) SPECIFICATION
MIL L 2104 : F LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, COMBAT TACTICAL SERVICE
SAE MS 1000 : 2013 LUBRICANTS, INDUSTRIAL OILS, AND RELATED PRODUCTS - CLASSIFICATION
ISO 24254:2007 Lubricants, industrial oils and related products (class L) Family E (internal combustion engine oils) Specifications for oils for use in four-stroke cycle motorcycle gasoline engines and associated drivetrains (categories EMA and EMB)
ISO 4263-4:2006 Petroleum and related products Determination of the ageing behaviour of inhibited oils and fluids TOST test Part 4: Procedure for industrial gear oils
SAE J 311 : 2000 FLUID FOR PASSENGER CAR TYPE AUTOMATIC TRANSMISSIONS

ASTM D 4628 : 2016 : REDLINE Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry
ASTM D 4307 : 2017 : REDLINE Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards

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