ASTM D 4483 : 2005
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
Hardcopy , PDF
11-11-2014
English
02-23-2005
Committee |
D 11
|
DocumentType |
Standard Practice
|
Pages |
60
|
ProductNote |
Reconfirmed 2005
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy | |
Supersedes |
1.1 This practice covers guidelines for evaluating precision and serves as the governing practice for interlaboratory test programs (ITP) used to evaluate precision for test methods as used in the rubber manufacturing and the carbon black industries. This practice uses the basic one way analysis of variance calculation algorithms of Practice E 691. Although bias is not evaluated in this practice, it is an essential concept in understanding precision evaluation.
1.2 This practice applies to test methods that have test results expressed in terms of a quantitative continuous variable. Although exceptions may occur, it is in general limited to test methods that are fully developed and in routine use in a number of laboratories.
1.3 Two precision evaluation methods are given that are described as robust statistical procedures that attempt to eliminate or substantially decrease the influence of outliers. The first is a General Precision procedure intended for all test methods in the rubber manufacturing industry, and the second is a specific variation of the general precision procedure designated as Special Precision, that applies to carbon black testing. Both of these procedures use the same uniform level experimental design and the Mandel h and k statistics to review the precision database for potential outliers. However, they use slight modifications in the procedure for rejecting incompatible data values as outliers. The Special Precision procedure is specific as to the number of replicates per database cell or material-laboratory combination.
1.4 This practice is divided into the following sections:
1.5 Six annexes are presented; these serve as supplements to the main body of this practice. are given mainly as background information that is important for a full understanding of precision evaluation. contain detailed instructions and procedures needed to perform the operations as called for in various parts of the practice. The use of these annexes in this capacity avoids long sections of involved instruction in the main body of this practice. This allows for a better presentation and understanding of the central concepts involved in the evaluation of precision. is also important; it gives a complete example of precision evaluation that illustrates all of the procedures and options likely to be encountered in any precision evaluation, from the simple to the most complex.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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ASTM D 2240 : 2015 : EDT 1 | Standard Test Method for Rubber Property—Durometer Hardness |
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ASTM D 1414 : 2015 | Standard Test Methods for Rubber O-Rings |
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ASTM D 7662 : 2015 | Standard Test Method for Carbon Content in Carbon Black Feedstock Oils |
ASTM D 5668 : 2009 : R2014 | Standard Test Methods for Rubber From Synthetic Sources—Volatile Matter |
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ASTM D 6370 : 1999 : R2019 | Standard Test Method for Rubber—Compositional Analysis by Thermogravimetry (TGA) |
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ASTM D 3189 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of Solution BR (Polybutadiene Rubber) |
ASTM D 1329 : 2016 | Standard Test Method for Evaluating Rubber Property—Retraction at Lower Temperatures (TR Test) |
ASTM D 1509 : 2018 | Standard Test Methods for Carbon Black—Heating Loss |
ASTM D 4004 : 2006 : R2017 | Standard Test Methods for Rubber—Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis |
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ASTM D 5670 : 1995 : R2019 | Standard Test Method for Rubber—Determination of Residual Unsaturation in Hydrogenated Nitrile Rubber (HNBR) by Infrared Spectrophotometry |
ASTM D 3190 : 2006 : R2016 | Standard Test Method for Rubber—Evaluation of Chloroprene Rubber (CR) |
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ASTM D 1619 : 2016 : REV A | Standard Test Methods for Carbon Black—Sulfur Content |
ASTM D 4571 : 2006 : R2017 | Standard Test Methods for Rubber Compounding Materials—Determination of Volatile Material |
ASTM D 623 : 2007 : R2014 | Standard Test Methods for Rubber Property—Heat Generation and Flexing Fatigue In Compression |
ASTM D 7558 : 2009 : R2019 | Standard Test Method for Colorimetric/Spectrophotometric Procedure to Quantify Extractable Chemical Dialkyldithiocarbamate, Thiuram, and Mercaptobenzothiazole Accelerators in Natural Rubber Latex and Nitrile Gloves |
ASTM F 414 : 2015 | Standard Test Method for Energy Absorbed by a Tire When Deformed by Slow-Moving Plunger |
ASTM D 3187 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of NBR (Acrylonitrile-Butadiene Rubber) |
ASTM D 624 : 2000 : R2012 | Standard Test Method for Tear Strength of Conventional Vulcanized Rubber and Thermoplastic Elastomers |
ASTM D 6924 : 2003 : R2017 | Standard Specification for Preformed Thermoplastic Vulcanizate Elastomeric Joint Seals for Bridges |
ASTM D 6600 : 2000 : R2017 | Standard Practice for Evaluating Test Sensitivity for Rubber Test Methods |
ASTM D 4937 : 1996 : R2017 | Standard Test Method for <emph type="ital">p</emph>-Phenylenediamine Antidegradants Purity by Gas Chromatography |
ASTM D 378 : 2010 : R2016 | Standard Test Methods for Rubber (Elastomeric) Conveyor Belting, Flat Type |
ASTM D 6281 : 2015 | Standard Test Method for Airborne Asbestos Concentration in Ambient and Indoor Atmospheres as Determined by Transmission Electron Microscopy Direct Transfer (TEM) |
ASTM D 3265 : 2019 | Standard Test Method for Carbon Black—Tint Strength |
ASTM D 5230 : 2014 : EDT 1 | Standard Test Method for Carbon Black—Automated Individual Pellet Hardness |
ASTM D 7679 : 2016 | Standard Test Method for Sulfur Content in Carbon Black Feedstock Oils |
ASTM D 6085 : 1997 : R2016 | Standard Practice for Sampling in Rubber Testing—Terminology and Basic Concepts |
ASTM D 5297 : 1995 : R2019 | Standard Test Methods for Rubber Chemical Accelerator—Purity by High Performance Liquid Chromatography |
ASTM D 412 : 2016 | Standard Test Methods for Vulcanized Rubber and Thermoplastic Elastomers—Tension |
ASTM D 573 : 2004 : R2015 | Standard Test Method for Rubber—Deterioration in an Air Oven |
ASTM D 1417 : 2016 | Standard Test Methods for Rubber Latices—Synthetic |
ASTM D 1506 : 2015 | Standard Test Methods for Carbon Black—Ash Content |
ASTM D 3346 : 2017 | Standard Test Methods for Rubber Property—Processability of Emulsion SBR (Styrene-Butadiene Rubber) With the Mooney Viscometer (Delta Mooney) |
ASTM D 6915 : 2017 : EDT 1 | Standard Practice for Carbon Black—Evaluation of Standard Reference Blacks |
ASTM D 2414 : 2018 : REV A | Standard Test Method for Carbon Black—Oil Absorption Number (OAN) |
ASTM D 4026 : 2006 : R2017 | Standard Test Method for Rubber Latex—Styrene-Butadiene Copolymer—Determination of Residual Styrene |
ASTM D 4572 : 1989 : R2017 | Standard Test Method for Rubber Chemicals—Wet Sieve Analysis of Sulfur |
ASTM D 3958 : 2006 : R2016 | Standard Test Methods for Rubber—Evaluation of BIIR and CIIR (Halogenated Isobutene—Isoprene Rubber) |
ASTM D 2663 : 2014 : R2019 | Standard Test Methods for Carbon Black—Dispersion in Rubber |
ASTM D 297 : 2015 | Standard Test Methods for Rubber Products—Chemical Analysis |
ASTM D 572 : 2004 : R2015 | Standard Test Method for Rubber—Deterioration by Heat and Oxygen |
ASTM D 6601 : 2019 | Standard Test Method for Rubber Properties—Measurement of Cure and After-Cure Dynamic Properties Using a Rotorless Shear Rheometer |
ASTM D 7771 : 2017 : REV A | Standard Test Method for Determination of Benzo-α-Pyrene (BaP) Content in Carbon Black |
ASTM D 1229 : 2003 : R2015 | Standard Test Method for Rubber Property—Compression Set at Low Temperatures |
ASTM D 1076 : 2015 | Standard Specification for Rubber—Concentrated, Ammonia Preserved, Creamed, and Centrifuged Natural Latex |
ASTM D 531 : 2015 | Standard Test Method for Rubber Property—Pusey and Jones Indentation |
ASTM D 1278 : 1991 : REV A : R2015 | Standard Test Methods for Rubber from Natural Sources—Chemical Analysis |
ASTM D 395 : 2018 | Standard Test Methods for Rubber Property—Compression Set |
ASTM D 4569 : 2006 : R2017 | Standard Test Method for Rubber Compounding Materials—Determination of Acidity in Sulfur |
ASTM D 4482 : 2011 : R2017 | Standard Test Method for Rubber Property—Extension Cycling Fatigue |
ASTM D 454 : 2004 : R2015 | Standard Test Method for Rubber Deterioration by Heat and Air Pressure |
ASTM D 6556 : 2019 | Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption |
ASTM D 3492 : 2016 | Standard Specification for Rubber Contraceptives (Male Condoms) |
ASTM D 3186 : 2007 : R2016 | Standard Test Methods for Rubber—Evaluation of SBR (Styrene-Butadiene Rubber) Mixed With Carbon Black or Carbon Black and Oil |
ASTM D 7772 : 2015 | Standard Test Method for Carbon Black Extractables – Absorbance of Cyclohexane Extract |
ASTM D 813 : 2007 : R2014 | Standard Test Method for Rubber Deterioration—Crack Growth |
ASTM D 6047 : 2017 | Standard Test Methods for Rubber, Raw—Determination of 5-Ethylidenenorbornene (ENB) or Dicyclopentadiene (DCPD) in Ethylene-Propylene-Diene (EPDM) Terpolymers |
ASTM D 4527 : 2018 | Standard Test Method for Carbon Black—Solvent Extractables |
ASTM D 751 : 2019 | Standard Test Methods for Coated Fabrics |
ASTM D 5099 : 2008 : R2017 | Standard Test Methods for Rubber—Measurement of Processing Properties Using Capillary Rheometry |
ASTM D 5712 : 2015 | Standard Test Method for Analysis of Aqueous Extractable Protein in Latex, Natural Rubber, and Elastomeric Products Using the Modified Lowry Method |
ASTM D 3493 : 2018 : REV A | Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN) |
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