ASTM D 4307 : 2017 : REDLINE
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The latest, up-to-date edition.
Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
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Published date
05-01-2017
Important note : All end users must be registered with an Account prior to user licenses being assigned.CONTAINED IN VOL. 05.02, 2015 Defines a laboratory procedure for the preparation of small volumes of multicomponent liquid blends for use as analytical standards.
| Committee |
D 02
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| DocumentType |
Redline
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| Pages |
4
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| PublisherName |
American Society for Testing and Materials
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| Status |
Current
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1.1This practice covers a laboratory procedure for the preparation of small volumes of multicomponent liquid blends for use as analytical standards.
1.2This practice is applicable to components that are normally liquids at ambient temperature and pressure, or solids that will form a solution when blended with liquids. Butanes can be included if precaution is used in blending them.
1.3This practice is limited to those components that fulfill the following conditions:
1.3.1They are completely soluble in the final blend.
1.3.2They are not reactive with other blend components or with blend containers.
1.3.3The combined vapor pressure of the blended components is such that there is no selective evaporation of any of the components.
1.3.3.1The butane content of the blend is not to exceed 10 %. (Warning—Extremely flammable liquefied gas under pressure. Vapor reduces oxygen available for breathing.) Components with a vapor pressure higher than butanes are not to be blended.
1.4The values stated in SI units are to be regarded as the standard.
1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| ASTM D 5623 : 1994 : R2009 | Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection |
| ASTM D 6296 : 1998 | Standard Test Method for Total Olefins in Spark-Ignition Engine Fuels by Multi-dimensional Gas Chromatography |
| ASTM D 6142 : 2016 : REDLINE | Standard Test Method for Analysis of Phenol by Capillary Gas Chromatography |
| ASTM D 7151 : 2015 : REDLINE | Standard Test Method for Determination of Elements in Insulating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM U 01 : 2013 | Normal Paraffins by Subtractive GC |
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| ASTM D 7578 : 2015-06 | GUIDE FOR CALIBRATION REQUIREMENTS FOR ELEMENTAL ANALYSIS OF PETROLEUM PRODUCTS AND LUBRICANTS |
| ASTM D 7040 :2004 | Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry |
| ASTM D 7040 : 2004 : R2010 | Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry |
| ASTM U 00 : 2013 | C<sub>8</sub> and Lower Boiling Paraffins and Naphthenes in Low-Olefin Hydrocarbons by GC |
| ASTM UOP 980 : 2007 | C<sub>5</sub> and Lower Boiling Dienes, Olefins, and Paraffins in Naphthas by GC |
| ASTM UOP 555 : 2010 | Trace Impurities in Benzene by GC |
| ASTM UOP 621 : 1998 | Boiling Point Distribution of Hydrocarbons by Gas Chromatography |
| ASTM D 5623 : 1994 : R1999 : EDT 1 | Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection |
| ASTM UOP 976 : 2002 | Trace C<sub>4</sub>-C<sub>9</sub> Saturates in High Purity Aromatics by GC |
| ASTM D 7754 : 2016 : REDLINE | Standard Test Method for Determination of Trace Oxygenates in Automotive Spark-Ignition Engine Fuel by Multidimensional Gas Chromatography |
| ASTM D 7920 : 2015 | Standard Test Method for Determination of Fuel Methanol (M99) and Methanol Fuel Blends (M10 to M99) by Gas Chromatography |
| ASTM D 7776 : 2012 | Standard Guide for Self-Assessment of Quality System Practices in Petroleum Products and Lubricant Testing Laboratories (Withdrawn 2017) |
| ASTM UOP 931 : 2010 | Trace Impurities in Mixed Xylenes by GC |
| ASTM D 5441 : 1998 : R2003 : EDT 1 | Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography |
| ASTM D 5986 : 1996 : R2011 | Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C<sub>8</sub>-C<sub> 12</sub> Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy |
| ASTM D 6296 : 1998 : R2003 : EDT 1 | Standard Test Method for Total Olefins in Spark-Ignition Engine Fuels by Multi-dimensional Gas Chromatography |
| ASTM D 7059 : 2009 : R2013 | Standard Test Method for Determination of Methanol in Crude Oils by Multidimensional Gas Chromatography |
| ASTM D 7806 : 2012 | Standard Test Method for Determination of the Fatty Acid Methyl Ester (FAME) Content of a Blend of Biodiesel and Petroleum-Based Diesel Fuel Oil Using Mid-Infrared Spectroscopy |
| ASTM UOP 688 : 2009 | Normal Olefins and Normal Paraffins by GC |
| ASTM D 5442 : 2017 : REDLINE | Standard Test Method for Analysis of Petroleum Waxes by Gas Chromatography |
| ASTM D 6293 : 1998 | Standard Test Method for Oxygenates and Paraffin, Olefin, Naphthene, Aromatic (O-PONA) Hydrocarbon Types in Low-Olefin Spark Ignition Engine Fuels by Gas Chromatography |
| ASTM U 09 : 2011 | Trace Hydrocarbons in Udex Solvent by GC |
| ASTM D 7740 : 201 | Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants |
| ASTM D 4626 : 1995 : R2000 | Standard Practice for Calculation of Gas Chromatographic Response Factors |
| ASTM UOP 551 : 2008 | C<sub>6</sub> and Lower Boiling Hydrocarbons in Olefin Free Naphthas by GC |
| ASTM D 7266 : 2013 : R2018 : EDT 1 | Standard Test Method for Analysis of Cyclohexane by Gas Chromatography (External Standard) |
| EN 13405:2002 | Surface active agents - Determination of dialkyl-tetralins content in linear alkylbenzene by high performance liquid chromatography (HPLC) |
| ASTM D 4951 : 2014 : REDLINE | Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry |
| ASTM D 5845 : 2001 : R2016 | Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and <emph type="ital">tert</emph>-Butanol in Gasoline by Infrared Spectroscopy |
| ASTM D 5845 : 2001 : R2011 | Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and <span class="italic">tert</span>-Butanol in Gasoline by Infrared Spectroscopy |
| ASTM UOP 968 : 2000 | Foots Oil in Methyl Isobutyl Ketone by GC |
| ASTM UOP 720 : 2008 | Impurities in, and Purity of, High Purity p-Xylene by GC |
| ASTM D 4626 : 1995 : R2005 | Standard Practice for Calculation of Gas Chromatographic Response Factors |
| ASTM D 5986 : 1996 : R2001 | Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C<sub>8</sub>-C<sub>12</sub> Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy |
| ASTM D 7059 : 2009 : R2017 | Standard Test Method for Determination of Methanol in Crude Oils by Multidimensional Gas Chromatography |
| ASTM D 7920 : 2015 : EDT 1 | Standard Test Method for Determination of Fuel Methanol (M99) and Methanol Fuel Blends (M10 to M99) by Gas Chromatography |
| ASTM D 7807 : 2012 | Standard Test Method for Determination of Boiling Range Distribution of Hydrocarbon and Sulfur Components of Petroleum Distillates by Gas Chromatography and Chemiluminescence Detection |
| ASTM D 6144 : 2017 : REDLINE | Standard Test Method for Analysis of AMS (α-Methylstyrene) by Capillary Gas Chromatography |
| ASTM D 5501 : 2012 | Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography |
| ASTM D 6277 : 2007 : R2012 | Standard Test Method for Determination of Benzene in Spark-Ignition Engine Fuels Using Mid Infrared Spectroscopy |
| ASTM D 7040 : 2004 : R2015 | Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry |
| ASTM D 6296 : 1998 : R2013 | Standard Test Method for Total Olefins in Spark-ignition Engine Fuels by Multidimensional Gas Chromatography |
| ASTM D 7371 : 2014 : REDLINE | Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method) |
| ASTM D 5769 : 2015 : REDLINE | Standard Test Method for Determination of Benzene, Toluene, and Total Aromatics in Finished Gasolines by Gas Chromatography/Mass Spectrometry |
| ASTM UOP 733 : 2010 | Residual Triglycerides in Deoxygenated Feedstocks by GC |
| ASTM D 5845 : 2001 : R2006 | Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and <i>tert</i>-Butanol in Gasoline by Infrared Spectroscopy |
| ASTM D 8071 : 2017 | Standard Test Method for Determination of Hydrocarbon Group Types and Select Hydrocarbon and Oxygenate Compounds in Automotive Spark-Ignition Engine Fuel Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV) |
| ASTM D 7691 : 2016 : REDLINE | Standard Test Method for Multielement Analysis of Crude Oils Using Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
| ASTM D 7576 : 2016 : REDLINE | Standard Test Method for Determination of Benzene and Total Aromatics in Denatured Fuel Ethanol by Gas Chromatography |
| ASTM UOP303 : 2007 | Impurities in Catalysts by ICP-OES |
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| ASTM D 7740 : 2011 : R2016 | Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants |
| ASTM UOP744 : 2006 | Aromatics in Hydrocarbons by GC |
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| ASTM D 5060 : 2012 : REDLINE | Standard Test Method for Determining Impurities in High-Purity Ethylbenzene by Gas Chromatography |
| ASTM D 7266 : 2013 | Standard Test Method for Analysis of Cyclohexane by Gas Chromatography (External Standard) |
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| ASTM D 6277 : 2007 | Standard Test Method for Determination of Benzene in Spark-Ignition Engine Fuels Using Mid Infrared Spectroscopy |
| ASTM D 7861 : 2014 : EDT 1 | Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy |
| ASTM D 7861 : 2014 | Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy |
| ASTM D 5441 : 1998 : R2013 | Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography |
| ASTM UOP 863 : 2001 | Trace Desorbent in C10-C18 Molex Products by GC |
| ASTM UOP 702 : 2009 | Impurities in Distilled High Purity Cumene by GC |
| ASTM D 5501 : 2012 : R2016 | Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography |
| ASTM UOP 934 : 1994 | Diolefins in C5 Olefinic Hydrocarbon Streams by GC (Withdrawn 2011) |
| ASTM D 8110 : 2017 | Standard Test Method for Elemental Analysis of Distillate Products by Inductively Coupled Plasma Mass Spectrometry (ICP-MS) |
| ASTM UOP 543 : 2011 | Trace Non-Aromatic Hydrocarbons in High-Purity Aromatics by GC |
| ASTM D 5501 : 2012 : EDT 1 | Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography |
| ASTM D 4735 : 2015 : REDLINE | TEST METHOD FOR DETERMINATION OF TRACE THIOPHENE IN REFINED BENZENE BY GAS CHROMATOGRAPHY |
| ASTM U 00 : 2006 | Trace Oxygenated Hydrocarbons in Liquid Hydrocarbon Streams by GC |
| ASTM D 6730 : 2001 : R2016 | Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100–Metre Capillary (with Precolumn) High-Resolution Gas Chromatography |
| ASTM D 6839 : 2017-06 | TEST METHOD FOR HYDROCARBON TYPES, OXYGENATED COMPOUNDS, AND BENZENE IN SPARK IGNITION ENGINE FUELS BY GAS CHROMATOGRAPHY |
| ASTM D 6296 : 1998 : R2008 | Standard Test Method for Total Olefins in Spark-ignition Engine Fuels by Multidimensional Gas Chromatography |
| ASTM D 7360 : 2016 : REDLINE | Standard Test Method for Analysis of Benzene by Gas Chromatography with External Calibration |
| ASTM D 4626 : 1995 : R2010 | Standard Practice for Calculation of Gas Chromatographic Response Factors |
| ASTM D 5623 : 1994 : R2014 | Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection |
| ASTM D 6730 : 2001 : R2006 : EDT 1 | Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100–Metre Capillary (with Precolumn) High-Resolution Gas Chromatography |
| ASTM D 7266 : 2013 : EDT 1 | Standard Test Method for Analysis of Cyclohexane by Gas Chromatography (External Standard) |
| ASTM D 5441 : 1998 : R2017 | Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography |
| ASTM D 8003 : 2015 | Standard Test Method for Determination of Light Hydrocarbons and Cut Point Intervals in Live Crude Oils and Condensates by Gas Chromatography |
| ASTM UOP 868 : 1988 | Trace Saturates in High Purity Aromatics by GC |
| BS EN 13405:2002 | Surface active agents. Determination of dialkyl-tetralins content in linear alkylbenzene by high performance liquid chromatography (HPLC) |
| ASTM D 6293 : 1998 : R2003 : EDT 1 | Standard Test Method for Oxygenates and Paraffin, Olefin, Naphthene, Aromatic (O-PONA) Hydrocarbon Types in Low-Olefin Spark Ignition Engine Fuels by Gas Chromatography (Withdrawn 2009) |
| ASTM D 4626 : 1995 : R2015 | Standard Practice for Calculation of Gas Chromatographic Response Factors |
| ASTM D 6730 : 2001 | Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100-Metre Capillary (with Precolumn) High-Resolution Gas Chromatography |
| GOST R 52256 : 2004 ERRATA 2009 | GASOLINE - DETERMINATION OF MTBE, ETBE, TAME, DIPE, METHANOL, ETHANOL AND TRET-BUTANOL BY METHOD OF INFRA-RED SPECTROSCOPY |
| ASTM D 6730 : 2001 : R2006 | Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100-Metre Capillary (with Precolumn) High-Resolution Gas Chromatography |
| ASTM D 5441 : 1998 : R2008 : EDT 1 | Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography |
| ASTM UOP 870 : 1990 | Carbon Number Distribution of Paraffins, Naphthenes and Aromatics by GC |
| ASTM D 5986 : 1996 : R2006 | Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C<inf>8</inf>-C<inf> 12</inf> Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy |
| ASTM D 5441 : 1998 | Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography |
| ASTM D 5845 : 2001 | Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and <i>tert-</i>Butanol in Gasoline by Infrared Spectroscopy |
| ASTM UOP 725 : 1986 | Pentenes and Lower Boiling Hydrocarbons in Olefinic Gasolines by GC (Withdrawn 2013) |
| ASTM UOP 537 : 1991 | Alcohol and Ketone Mixtures by GC |
| ASTM D 7974 : 2015 | Standard Test Method for Determination of Farnesane, Saturated Hydrocarbons, and Hexahydrofarnesol Content of Synthesized Iso-Paraffins (SIP) Fuel for Blending with Jet Fuel by Gas Chromatography |
| ASTM D 5986 : 1996 : R2015 | Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C<inf>8</inf >–C<inf> 12</inf> Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy |
| ASTM UOP 732 : 2009 | Analysis of Distillate Fuels Derived from Oxygenated (Bio) Feedstocks by GC |
| ASTM D 6584 : 2017 : REDLINE | Standard Test Method for Determination of Total Monoglycerides, Total Diglycerides, Total Triglycerides, and Free and Total Glycerin in B-100 Biodiesel Methyl Esters by Gas Chromatography |
| ASTM D 7796 : 2017 : REDLINE | Standard Test Method for Analysis of Ethyl tert-Butyl Ether (ETBE) by Gas Chromatography |
| ASTM D 4420 : 1994 | Standard Test Method for Determination of Aromatics in Finished Gasoline by Gas Chromatography) |
| ASTM D 3797 : 2005 | Standard Test Method for Analysis of <i>o</i>-Xylene by Gas Chromatography (Withdrawn 2014) |
| ASTM D 7845 : 2017 : REDLINE | Standard Test Method for Determination of Chemical Species in Marine Fuel Oil by Multidimensional Gas Chromatography/Mass Spectrometry |
| ASTM D 7057 : 2018 : REDLINE | Standard Test Method for Analysis of Isopropylbenzene (Cumene) by Gas Chromatography (External Standard) |
| ASTM D 5986 : 1996 | Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C<sub>8</sub>-C<sub>12</sub> Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy |
| ASTM D 6730 : 2001 : R2011 | Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100–Metre Capillary (with Precolumn) High-Resolution Gas Chromatography |
| ASTM D 5623 : 1994 : R2004 : EDT 1 | Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection |
| ASTM UOP 799 : 2008 | Chloride in Liquid Hydrocarbons by Dry Colorimetry |
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