ASTM D 3524 : 2014
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Diesel Fuel Diluent in Used Diesel Engine Oils by Gas Chromatography
Hardcopy , PDF
11-25-2020
English
05-15-2014
Important note : All end users must be registered with an Account prior to user licenses being assigned.CONTAINED IN VOL. 05.02, 2015 Describes the use of gas chromatography to determine the amount of diesel fuel in used engine lubricating oil.
| Committee |
D 02
|
| DocumentType |
Test Method
|
| Pages |
6
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
1.1This test method covers the use of gas chromatography to determine the amount of diesel fuel in used engine lubricating oil. This test is limited to SAE 30 oil. The diesel fuel diluent is analyzed at concentrations up to 12 mass %.
1.2This test method is limited to gas chromatographs equipped with flame ionization detectors and temperature programmable ovens.
1.3There is some overlap of the boiling ranges of diesel fuel and SAE 30 engine oils. Moreover, the boiling range of SAE 30 oils from various sources can vary appreciably. As a result, the calibration can be altered by as much as 2 %, in terms of fuel dilution. When testing unknown or mixed brands of used engine oil, it should be realized that the precision of the method may be poorer than the precision obtained when calibrating with a new oil representative of the used oil being tested.
1.4The values stated in SI units are to be regarded as the standard. The values stated in inch-pound units are for information only.
1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to use.
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| SAE J 357 : 2016 | PHYSICAL AND CHEMICAL PROPERTIES OF ENGINE OILS |
| ASTM D 6681 : 2017 | Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test Procedure |
| ASTM D 8048 : 2019 | Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine |
| ASTM D 6224 : 2016 | Standard Practice for In-Service Monitoring of Lubricating Oil for Auxiliary Power Plant Equipment |
| ASTM D 7593 : 2014 : REDLINE | Standard Test Method for Determination of Fuel Dilution for In-Service Engine Oils by Gas Chromatography |
| ASTM D 6681 : 2017 : REDLINE | Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test Procedure |
| ASTM D 7156 : 2017 : REDLINE | Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine |
| ASTM D 7593 : 2014 | Standard Test Method for Determination of Fuel Dilution for In-Service Engine Oils by Gas Chromatography |
| ASTM D 6750 : 2019 | Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur) |
| ASTM D 8047 : 2018 | Standard Test Method for Evaluation of Engine Oil Aeration Resistance in a Caterpillar C13 Direct-Injected Turbocharged Automotive Diesel Engine |
| ASTM D 8074 : 2018 | Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine |
| ASTM D 7156 : 2017 | Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine |
| ASTM D 6923 : 2018 | Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1R Test Procedure |
| 08/30190684 DC : DRAFT OCT 2008 | BS ISO 18436-5 - CONDITION MONITORING AND DIAGNOSTICS OF MACHINES - REQUIREMENTS FOR QUALIFICATION AND ASSESSMENT OF PERSONNEL - PART 5: LUBRICANT LABORATORY TECHNICIAN/ANALYST |
| BS ISO 18436-5:2012 | Condition monitoring and diagnostics of machines. Requirements for qualification and assessment of personnel Lubricant laboratory technician/analyst |
| UNI ISO 18436-5 : 2013 | CONDITION MONITORING AND DIAGNOSTICS OF MACHINES - REQUIREMENTS FOR QUALIFICATION AND ASSESSMENT OF PERSONNEL - PART 5: LUBRICANT LABORATORY TECHNICIAN/ANALYST |
| ASTM D 8074 : 2016 | Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine |
| ASTM D 6224 : 2016 : REDLINE | Standard Practice for In-Service Monitoring of Lubricating Oil for Auxiliary Power Plant Equipment |
| ISO 18436-5:2012 | Condition monitoring and diagnostics of machines — Requirements for qualification and assessment of personnel — Part 5: Lubricant laboratory technician/analyst |
| ASTM E 1510 : 1995 : R2013 : EDT 1 | Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs |
| ASTM E 260 : 1996 | Standard Practice for Packed Column Gas Chromatography |
| ASTM D 4626 : 1995 : R2005 | Standard Practice for Calculation of Gas Chromatographic Response Factors |
| ASTM E 1510 : 1995 : R2000 | Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs |
| ASTM E 1510 : 1995 : R2005 | Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs |
| ASTM E 1510 : 1995 | Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs |
| ASTM D 4626 : 1995 : R2019 | Standard Practice for Calculation of Gas Chromatographic Response Factors |
| ASTM D 4626 : 1995 : R2015 | Standard Practice for Calculation of Gas Chromatographic Response Factors |
| ASTM D 4626 : 1995 : R2000 | Standard Practice for Calculation of Gas Chromatographic Response Factors |
| ASTM D 4626 : 1995 : R2010 | Standard Practice for Calculation of Gas Chromatographic Response Factors |
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