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ASTM C 114 : 2022

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Methods for Chemical Analysis of Hydraulic Cement

Available format(s)

Hardcopy , PDF

Superseded date

06-14-2024

Superseded by

ASTM C 114 : 2023

Language(s)

English

Published date

12-21-2022

US$108.00
Excluding Tax where applicable

Committee
C 01
DocumentType
Test Method
Pages
32
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1These test methods cover the chemical analyses of hydraulic cements. Any test methods of demonstrated acceptable precision and bias may be used for analysis of hydraulic cements, including analyses for referee and certification purposes, as explained in Section 4. Specific chemical test methods are provided for ease of reference for those desiring to use them. They are grouped as Reference Test Methods and Alternative Test Methods. The reference test methods are long accepted classical chemical test methods which provide a reasonably well-integrated basic scheme of analysis for hydraulic cements. The alternative test methods generally provide individual determination of specific analytes and may be used alone or as alternates and determinations within the basic scheme at the option of the analyst and as indicated in the individual method.

1.2Contents:

Section

Subject

2

Referenced Documents

4

Description of Referee Analyses

4.1

Referee Analyses

5

Qualification for Different Analyses

5.1

Certified Reference Materials

5.2

Requirements for Qualification Testing

5.3

Alternative Analyses

5.4

Performance Requirements for Rapid Test Methods

6

General

6.1

Interferences and Limitations

6.2

Apparatus and Materials

6.3

Reagents

6.4

Sample Preparation

6.5

General Procedures

6.6

Recommended Order for Reporting Analyses

Reference Test Methods

7

Insoluble Residue

8

Silicon Dioxide

8.2

Cements with Insoluble Residue Less Than 1 %

8.3

Cements with Insoluble Residue Greater Than 1 %

9

Ammonium Hydroxide Group

10

Ferric Oxide

11

Phosphorus Pentoxide

12

Titanium Dioxide

13

Zinc Oxide

14

Aluminum Oxide

15

Calcium Oxide

16

Magnesium Oxide

17

Sulfur

17.1

Sulfur Trioxide

17.2

Sulfide

18

Loss On Ignition

18.1

Portland Cement

18.2

Portland Blast-Furnace Slag Cement and Slag Cement

19

Sodium and Potassium Oxides

19.1

Total Alkalis

19.2

Water-Soluble Alkalis

20

Manganic Oxide

21

Chloride

22

Chloroform-Soluble Organic Substances

Alternative Test Methods

23

Calcium Oxide

24

Carbon Dioxide

25

Magnesium Oxide

26

Loss on Ignition

26.1

Portland Blast-Furnace Slag Cement and Slag Cement

27

Titanium Dioxide

28

Phosphorus Pentoxide

29

Manganic Oxide

30

Free Calcium Oxide

Appendices

Appendix X1

Example of Determination of Equivalence Point
 for the Chloride Determination

Appendix X2

CO2 Determinations in Hydraulic Cements

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM C 465 : 2023 Standard Specification for Processing Additions for Use in the Manufacture<brk/> of Hydraulic Cements
ASTM C 1905/C1905M : 2023 Standard Specification for Cements that Require Carbonation Curing
ASTM C 183/C183M : 2023 Standard Practice for Sampling and the Amount of Testing of Hydraulic Cement
ASTM C 1600/C1600M : 2023 Standard Specification for Rapid Hardening Hydraulic Cement
ASTM C 331/C331M : 2023 Standard Specification for Lightweight Aggregates for Concrete Masonry Units
ASTM C 595/C595M : 2023 Standard Specification for Blended Hydraulic Cements
ASTM C 188 : 2017 : R2023 Standard Test Method for Density of Hydraulic Cement
ASTM C 1222 : 2023 Standard Practice for Evaluation of Laboratories Testing Hydraulic Cement
ASTM C 1761/C1761M : 2023 Standard Specification for Lightweight Aggregate for Internal Curing of Concrete
ASTM C 1709 : 2022 Standard Guide for Evaluation of Alternative Supplementary Cementitious Materials (ASCM) for Use in Concrete
ASTM F 412 : 2023 Standard Terminology Relating to Plastic Piping Systems
ASTM C 330/C330M : 2023 Standard Specification for Lightweight Aggregates for Structural Concrete
ASTM C 845/C845M : 2018 Standard Specification for Expansive Hydraulic Cement
ASTM C 1875 : 2018 Standard Practice for Determination of Major and Minor Elements in Aqueous Pore Solutions of Cementitious Pastes by Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES)
ASTM C 330/C330M : 2017 : REV A Standard Specification for Lightweight Aggregates for Structural Concrete
ASTM C 1707 : 2018 Standard Specification for Pozzolanic Hydraulic Lime for Structural Purposes
ASTM C 1012/C1012M : 2018 : REV B Standard Test Method for Length Change of Hydraulic-Cement Mortars Exposed to a Sulfate Solution
ASTM C 1038/C1038M : 2019 Standard Test Method for Expansion of Hydraulic Cement Mortar Bars Stored in Water
ASTM D 806 : 2019 Standard Test Method for Cement Content of Hardened Soil-Cement Mixtures
ASTM C 1600/C1600M : 2019 Standard Specification for Rapid Hardening Hydraulic Cement
ASTM C 1084 : 2019 Standard Test Method for Portland-Cement Content of Hardened Hydraulic-Cement Concrete
ASTM C 10/C10M : 2019 Standard Specification for Natural Cement
ASTM C 1240 : 2020 Standard Specification for Silica Fume Used in Cementitious Mixtures
ASTM C 563 : 2020 Standard Guide for Approximation of Optimum SO<inf>3</inf> in Hydraulic Cement
ASTM D 5759 : 2012 : R2020 Standard Guide for Characterization of Coal Fly Ash and Clean Coal Combustion Fly Ash for Potential Uses
ASTM C 1872 : 2018 : EDT 2 Standard Test Method for Thermogravimetric Analysis of Hydraulic Cement
ASTM C 1218/C1218M : 2020 Standard Test Method for Water-Soluble Chloride in Mortar and Concrete
ASTM C 219 : 2020 : REV A Standard Terminology Relating to Hydraulic and Other Inorganic Cements
ASTM C 1365 : 2018 Standard Test Method for Determination of the Proportion of Phases in Portland Cement and Portland-Cement Clinker Using X-Ray Powder Diffraction Analysis
ASTM C 1709 : 2018 Standard Guide for Evaluation of Alternative Supplementary Cementitious Materials (ASCM) for Use in Concrete
ASTM C 1152/C1152M : 2020 Standard Test Method for Acid-Soluble Chloride in Mortar and Concrete
ASTM C 1324 : 2020 : REV A Standard Test Method for Examination and Analysis of Hardened Masonry Mortar
ASTM C 1005 : 2020 Standard Specification for Reference Masses and Devices for Determining Mass and Volume for Use in Physical Testing of Hydraulic Cements
ASTM C 1524 : 2020 Standard Test Method for Water-Extractable Chloride in Aggregate (Soxhlet Method)
ASTM C 1580 : 2020 Standard Test Method for Water-Soluble Sulfate in Soil
ASTM C 1157/C1157M : 2020 : REV A Standard Performance Specification for Hydraulic Cement
ASTM C 1222 : 2021 Standard Practice for Evaluation of Laboratories Testing Hydraulic Cement
ASTM C 595/C595M : 2021 Standard Specification for Blended Hydraulic Cements
ASTM C 109/C109M : 2021 Standard Test Method for Compressive Strength of Hydraulic Cement Mortars (Using 2-in. or [50mm] Cube Specimens)
ASTM C 1697 : 2021 Standard Specification for Blended Supplementary Cementitious Materials
ASTM F 412 : 2021 Standard Terminology Relating to Plastic Piping Systems
ASTM C 311/C311M : 2022 Standard Test Methods for Sampling and Testing Fly Ash or Natural Pozzolans for Use in Portland-Cement Concrete
ASTM C 1778 : 2022 Standard Guide for Reducing the Risk of Deleterious Alkali-Aggregate Reaction in Concrete
ASTM C 1602/C1602M : 2022 Standard Specification for Mixing Water Used in the Production of Hydraulic Cement Concrete
ASTM C 465 : 2022 Standard Specification for Processing Additions for Use in the Manufacture<brk/> of Hydraulic Cements
ASTM C 150/C150M : 2022 Standard Specification for Portland Cement
ASTM C 989/C989M : 2022 Standard Specification for Slag Cement for Use in Concrete and Mortars
ASTM C 226 : 2022 Standard Specification for Air-Entraining Additions for Use in the Manufacture of Air-Entraining Hydraulic Cement
ASTM C 183/C183M : 2022 Standard Practice for Sampling and the Amount of Testing of Hydraulic Cement
ASTM E 2060 : 2022 Standard Guide for Use of Coal Combustion Products for Solidification/Stabilization of Inorganic Wastes
ASTM C 188 : 2017 Standard Test Method for Density of Hydraulic Cement
ASTM D 5298 : 2016 Standard Test Method for Measurement of Soil Potential (Suction) Using Filter Paper
ASTM C 1608 : 2017 Standard Test Method for Chemical Shrinkage of Hydraulic Cement Paste
ASTM C 786/C786M : 2017 Standard Test Method for Fineness of Hydraulic Cement and Raw Materials by the 300-μm (No. 50), 150-μm (No. 100), and 75-μm (No. 200) Sieves by Wet Methods
ASTM C 331/C331M : 2017 Standard Specification for Lightweight Aggregates for Concrete Masonry Units
ASTM C 1761/C1761M : 2017 Standard Specification for Lightweight Aggregate for Internal Curing of Concrete

ASTM E 617 : 2013 Standard Specification for Laboratory Weights and Precision Mass Standards
ASTM C 25 : 2019 Standard Test Methods for Chemical Analysis of Limestone, Quicklime, and Hydrated Lime

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