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AS 2503.5-2003

AS 2503.5-2003

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Refractories and refractory materials - Chemical analysis Chrome-bearing materials

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Language(s)

English

Published date

11-24-2003

Publisher

Standards Australia

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Hardcopy - English
PDF 1 User - English
PDF 3 Users - English
PDF 5 Users - English
PDF 9 Users - English
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This Standard has been reconfirmed. To view or download the Reconfirmation Notice please click here.

1 - AS 2503.5-2003 REFRACTORIES AND REFRACTORY MATERIALS-CHEMICAL ANALYSIS - CHROME-BEARING MATERIALS
4 - PREFACE
5 - CONTENTS
6 - SECTION 1 SCOPE AND GENERAL
6 - 1.1 SCOPE
6 - 1.2 REFERENCED DOCUMENTS
6 - 1.3 DEFINITIONS
6 - 1.3.1 Chrome-alumina refractory
7 - 1.3.2 Chrome-dolomite refractory
7 - 1.3.3 Chrome refractory
7 - 1.3.4 Chrome-silica refractory
7 - 1.3.5 Chrome-sillimanite refractory
7 - 1.4 PRINCIPLE
8 - 1.5 REPEATABILITY
8 - 1.6 SAFETY
9 - SECTION 2 SAMPLING AND SAMPLE PREPARATION
9 - 2.1 SCOPE
9 - 2.2 GROSS SAMPLING
9 - 2.2.1 Shaped materials
9 - 2.2.2 Bulk or ground materials
9 - 2.3 PREPARATION OF SAMPLE
9 - 2.3.1 Crushing
10 - 2.3.2 Test samples
11 - SECTION 3 DETERMINATION OF LOSS ON IGNITION
11 - 3.1 SCOPE
11 - 3.2 APPARATUS
11 - 3.2.1 Drying oven
11 - 3.2.2 Muffle furnace
11 - 3.2.3 Platinum crucible
11 - 3.2.4 Weighing balance
11 - 3.3 PROCEDURE
12 - SECTION 4 DETERMINATION OF SILICON
12 - 4.1 SCOPE
12 - 4.2 REAGENTS
12 - 4.2.1 General
12 - 4.2.2 Solid reagents
12 - 4.2.3 Solutions
13 - 4.3 APPARATUS
13 - 4.3.1 Glassware
13 - 4.3.2 Hot water bath
13 - 4.3.3 Platinum dish
13 - 4.3.4 Sintered glass crucible (porosity 5 µm to 15 µm)
13 - 4.3.5 Common apparatus
13 - 4.4 PROCEDURE
13 - 4.4.1 Blank test
13 - 4.4.2 Continuity of analysis
13 - 4.4.3 Determination
16 - SECTION 5 DETERMINATION OF CHROMIUM
16 - 5.1 SCOPE OF SECTION
16 - 5.2 REAGENTS
16 - 5.2.1 Introduction
16 - 5.2.2 Solid reagents
16 - 5.2.3 General solutions
16 - 5.2.4 Standard solutions
17 - 5.2.5 Indicator-barium diphenylamine sulfonate solution
17 - 5.3 APPARATUS
17 - 5.4 PROCEDURE
17 - 5.4.1 Blank test
17 - 5.4.2 Determination
19 - SECTION 6 DETERMINATION OF TITANIUM, IRON, ALUMINIUM, MANGANESE, CALCIUM AND MAGNESIUM
19 - 6.1 SCOPE
19 - 6.2 REAGENTS
19 - 6.2.1 Introduction
19 - 6.2.2 Solid reagents
19 - 6.2.3 General solutions
21 - 6.2.4 Standard solutions
23 - 6.2.5 Indicators
23 - 6.3 APPARATUS
23 - 6.3.1 Steam bath
23 - 6.3.2 UV-visible spectrophotometer
23 - 6.3.3 Common apparatus
24 - 6.4 PROCEDURE
24 - 6.4.1 Blank test
24 - 6.4.2 Preparation of test solution (Solution A)
25 - 6.4.3 Determination of titanium dioxide
26 - 6.4.4 Determination of iron as iron (III) oxide
26 - 6.4.5 Determination of manganese oxide
27 - 6.4.6 Determination of aluminium oxide
29 - 6.4.7 Determination of calcium oxide
29 - 6.4.8 Determination of magnesium oxide
32 - SECTION 7 DETERMINATION OF SODIUM, POTASSIUM AND LITHIUM OXIDES
32 - 7.1 SCOPE OF SECTION
32 - 7.2 REAGENTS
32 - 7.2.1 General
32 - 7.2.2 Solutions
32 - 7.3 APPARATUS
32 - 7.3.1 Flame photometer
32 - 7.3.2 Common apparatus
33 - 7.4 PROCEDURE
33 - 7.4.1 Preliminary procedures
33 - 7.4.2 Determination of sodium, potassium and lithium oxides
34 - SECTION 8 TEST REPORT
35 - APPENDIX A - STANDARDIZATION OF CDTA AND EGTA SOLUTIONS
35 - A1 SCOPE
35 - A2 REPEATABILITY
35 - A3 REAGENTS AND SOLUTIONS
35 - A4 PROCEDURE
35 - A4.1 Standardization of CDTA against magnesium
36 - A4.2 Standardization of CDTA against zinc
36 - A4.3 Standardization of EGTA against calcium
38 - APPENDIX B - STANDARDIZATION OF AMMONIUM IRON(II) SULFATE SOLUTION
38 - B1 SCOPE
38 - B2 REPEATABILITY
38 - B3 REAGENTS AND SOLUTIONS
38 - B4 PROCEDURE
40 - APPENDIX C - SCHEME OF ANALYSIS FOR CHROME-BEARING MATERIALS

Sets out methods for the sampling, sample preparation, and analysis of chrome-bearing materials.

Committee
MN-007
DocumentType
Standard
ISBN
0 7337 5576 3
Pages
35
ProductNote
Reconfirmed 05-07-2013
PublisherName
Standards Australia
Status
Current
Supersedes

This Standard sets out methods for the sampling, sample preparation, and analysis of chrome-bearing refractories and refractory materials. Procedures are described for the determination of—(a) the loss on ignition*; and (b) the chemical composition*, viz the amount of silicon, chromium, titanium, iron, aluminium, manganese, calcium, magnesium, sodium, potassium and lithium present in chrome-bearing materials, expressed as the oxides of these elements. NOTE: Appendix C provides an overview of these test procedures in flowchart form. This Standard applies to chrome-bearing materials represented by those defined in Clause 1.3, whose composition is typified by Table 1.1. It may be applicable to materials which fall outside these ranges, but if used for such cases, it is necessary to exercise caution when interpreting the results as it cannot be assumed the limits cited in Clause 1.5 apply.

Originated as part of AS R28-1965.
Revised and redesignated in part as AS 2503.5-1989.
Second edition 2003.

AS 2508.6.020-1991 Safe storage and handling information card - Selenious acid, selenates and selenites
AS 2508.2.011-1984 Safe storage and handling information card - Butadiene (inhibited)
AS 2508.8.010-1990 Safe storage and handling information cards for hazardous materials - Sulfuric acid (up to 98% m/m)
AS 2508.6.009-1990 Safe storage and handling information card - 1,1,1-trichloroethane (Methylchloroform)
AS 2508.3.033-1984 Safe storage and handling information card - Isoprene, inhibited
AS 2508.6.002-1985 Safe storage and handling information card - Cyanides (sodium and potassium)
AS 2508.3.032-1984 Safe storage and handling information card - Glycol ether acetates
AS 2508.8.005-1992 Safe storage and handling information card - Acetic acid (containing more than 10 percent but not more than 80 percent acid, by mass, in water)
AS 2508.3.005-1995 Safe storage and handling information card - Benzene
AS 2508.2.007-2001 Safe storage and handling information card - Liquefied petroleum gas
AS 2243.3-1991 Safety in laboratories Microbiology
AS 2508.8.009-1990 Safe storage and handling information card - Sulfuric acid (Oleum)
AS 2508.2.013-1992 Safe storage and handling information card - Ethylene (ethene)
AS 2508.4.001-1982 Safe storage and handling information card - Calcium carbide
AS 2243.7-1991 Safety in laboratories - Electrical aspects
AS 2508.3.009-1982 Safe storage and handling information card - Hydrocarbon solvents
AS 2508.6.024-1984 Safe storage and handling information card - Pentachlorophenol
AS 2508.8.017-1988 Safe storage and handling information card - Aluminium chloride (Anhydrous)
AS 2508.6.022-1986 Safe storage and handling information card - Copper-chrome-arsenic
AS 2508.3.025-1983 Safe storage and handling information cards for hazardous materials - Chlorobenzene (monochlorobenzene)
AS 2508.3.029-1983 Safe storage and handling information card - Glycol ethers (flammable)
AS 2508.6.001-1988 Safe storage and handling information card - Carbon tetrachloride (tetrachloromethane)
AS 2508.3.026-1995 Safe storage and handling information card - Propylene oxide
AS 2508.3.004-1982 Safe storage and handling information card - Acrylates (methyl, ethyl)
AS 2508.8.002-1986 Safe storage and handling information card - Hydrochloric acid (muriatic acid, spirits of salts)
AS 2243.9-1991 Safety in laboratories - Recirculating fume cabinets
AS 2508.5.001-1989 Safe storage and handling information card - Hydrogen peroxide
AS 2508.2.009-1984 Safe storage and handling information card - Oxygen (refrigerated liquid)
AS 2508.6.018-1989 Safe storage and handling information card - Lead arsenate and Lead aresenite
AS 2508.3.017-1983 Safe storage and handling information card - Ethanol/methylated spirits
AS 2508.2.001-1992 Safe storage and handling information card - Acetylene (Dissolved) (Ethyne)
AS 2508.2.012-1985 Safe storage and handling information card - Non-flammable, inert, compressed gases (includes: argon, helium, krypton, neon, nitrogen and xenon)
AS 2508.8.008-1992 Safe storage and handling information card - Maleic anhydride
AS 2508.8.007-1990 Safe storage and handling information card - Nitric acid
AS 2508.3.016-1982 Safe storage and handling information card - Methyl isobutyl ketone (MIBK)
AS 2243.6-1990 Safety in laboratories - Mechanical aspects
AS 2508.10.001-2000 Safe storage and handling information card - Agricultural and veterinary chemicals (Packaged products only)
AS 2508.8.012-1991 Safe storage and handling information card - Hydrogen fluoride (Anhydrous)(Anhydrous hydrofluoric acid)
AS 2508.6.008-1989 Safe storage and handling information card - Ammonium thioglycolate
AS 2508.3.027-1983 Safe storage and handling information card - Diacetone alcohol
AS 2780-2003 Refractories and refractory materials - Glossary of terms (Reconfirmed 2013)
AS 2508.8.015-1988 Safe storage and handling information card - Dilute ammonia solution containing 10 percent up to 35 percent m/m ammonia
AS 2508.3.007-1995 Safe storage and handling information card - Carbon disulphide
AS 2508.3.030-1983 Safe storage and handling information card - Cyclohexane
AS 2508.6.003-1984 Safe storage and handling information card - Aniline (aminobenzene)
AS 2508.6.015-1983 Safe storage and handling information card - Methylene chloride (Dichloromethane)
AS 2508.3.031-1983 Safe storage and handling information card - Tetrahydrofuran (THF)
AS 2508.3.002-1982 Safe storage and handling information card - Acetates (ethyl acetate, propyl acetates, butyl acetates, amyl acetate)
AS 2243.2-1990 Safety in laboratories - Chemical aspects
AS 2508.8.003-1990 Safe storage and handling information card - Sodium hypochlorite Hypochlorite solutions
AS 2508.2.005-1984 Safe storage and handling information card - Chlorine (compressed)
AS 2243.8-1992 Safety in laboratories Fume cupboards
AS 2508.6.013-1991 Safe storage and handling information card - Trichloroethylene
AS 2508.6.010-1983 Safe storage and handling information card - Toluene diisocyanate (TDI)
AS 2508.5.003-1990 Safe storage and handling information card - Calcium hypochlorite
AS 2508.3.024-1995 Safe storage and handling information card - Dimethylamine solution
AS 2508.6.028-1988 Safe storage and handling information card - Chloropicrin
AS 2508.3.003-1982 Safe storage and handling information card - Acrylates (butyl, isobutyl)
AS 2508.6.005-1984 Safe storage and handling information card - Fluorides (ammonium, potassium, magnesium or sodium fluoride)
AS 2508.3.008-1983 Safe storage and handling information cards for hazardous materials - Acrylonitrile (inhibited)
AS 2508.3.001-1982 Safe storage and handling information card - Acetone
AS 2508.3.014-1992 Safe storage and handling information card - Xylenes (xylols)
AS 2508.6.016-1995 Safe storage and handling information card - Phenol (carbolic acid), cresols and cresylic acid
AS 2508.3.034-1984 Safe storage and handling information card - Pentanes
AS 2508.3.011-1992 Safe storage and handling information card - Methanol (methyl alcohol)
AS 2508.2.004-1995 Safe storage and handling information card - Ammonia (anhydrous)
AS 2508.5.004-1991 Safe storage and handling information card - Benzoyl peroxide
AS 2243.1-1990 Safety in laboratories General
AS 2508.6.023-1989 Safe storage and handling information card - Phenylmercuric compounds
AS 2508.5.002-1990 Safe storage and handling information card - Ammonium nitrate
AS 2508.8.013-1991 Safe storage and handling information card - Hydrofluoric acid (aqueous)
AS 2508.6.004-1984 Safe storage and handling information card - Cadmium compounds (other than selenide and sulphide)
AS 2508.6.007-1995 Safe storage and handling information card - Epichlorohydrin (Ech or 1-Chloro-2,3-epoxypropane)
AS 2508.6.006-1982 Safe storage and handling information card - Beryllium and compounds
AS 2508.8.016-1988 Safe storage and handling information card - Phosphoric acid (Orthophosphoric acid)
AS 2508.3.028-1983 Safe storage and handling information card - Ethylene dichloride (1,2-dichloroethane, ethylene chloride (EDC))
AS 2508.8.001-1995 Safe storage and handling information card - Acetic anhydride
AS 2508.6.012-1988 Safe storage and handling information card - Diphenyl methane-4, 4-Diisocyanate [Methylene bis-(Phenylene) Diisocyanate] (MDI)
AS 2508.2.006-1995 Safe storage and handling information card - Ethylene oxide
AS 2497.1-2001 Procedures for acceptance testing of refractory products Batch procedure (Reconfirmed 2013)
AS 2243.10-1993 Safety in laboratories - Storage of chemicals
AS 2508.6.019-1995 Safe storage and handling information card - Lead alkyls
AS 2243.4-1998 Safety in laboratories - Ionizing radiations
AS 2508.6.027-1984 Safe storage and handling information card - Tributyltin-oxide
AS 2508.6.011-1988 Safe storage and handling information card - Tetrachloroethylene (Perchloroethylene, Per or Perc)
AS 2508.8.011-1995 Safe storage and handling information card - Methacrylic acid (inhibited)
AS 2508.6.021-1984 Safe storage and handling information card - Sodium pentachlorophenate
AS 2508.3.013-1984 Safe storage and handling information card - Methyl ethyl ketone (MEK)
AS 2508.2.010-1984 Safe storage and handling information card - Sulphur dioxide (liquefied)
AS 2508.6.026-1984 Safe storage and handling information card - Formaldehyde solutions - Flashpoint above 61 degrees Celsius
AS 2162.1-1996 Verification and use of volumetric apparatus General - Volumetric glassware
AS 2508.3.021-1983 Safe storage and handling information card - Cyclohexanone
AS 2508.8.018-1995 Safe storage and handling information card - Formaldehyde solutions (with not less than 25 percent formaldehyde)
AS 2508.8.004-1992 Safe storage and handling information card - Acetic acid (containing more than 80 percent acid, by mass, in water)
AS 2508.3.012-1982 Safe storage and handling information card - Styrene (vinyl benzene, styrene monomer)
AS 2508.6.017-1989 Safe storage and handling information card - Lead acetate
AS 2508.2.002-1992 Safe storage and handling information card - Hydrogen (compressed)
AS 2508.3.018-1983 Safe storage and handling information card - Methyl isobutyl carbinol
AS 2508.5.005-1992 Safe storage and handling information card - Methyl ethyl ketone peroxide (MEKP) (not more than 50% in solution with not more than 10% available oxygen)
AS 2508.2.008-1984 Safe storage and handling information card - Oxygen (compressed)
AS 2508.8.006-1992 Safe storage and handling information card - Sodium hydroxide (solid and solution) (caustic soda)
AS 2508.3.015-1992 Safe storage and handling information card - Toluene (toluol)
AS 2508.3.010-1995 Safe storage and handling information card - Amines (isopropylamine, diethylamine, triethylamine)
AS 2508.3.006-1995 Safe storage and handling information card - Butanols, propanols, amyl alcohols
AS 2508.6.025-1984 Safe storage and handling information card - Arsenic acid
AS 2508.8.014-1985 Safe storage and handling information card - Mercury metal
AS 2508.2.003-1995 Safe storage and handling information card - Vinyl chloride (inhibited)
AS 2508.3.020-1983 Safe storage and handling information card - Ethyl benzene
AS 2508.3.023-1983 Safe storage and handling information card - Vinyl acetate (vinyl acetate monomer)
AS 2508.3.022-1983 Safe storage and handling information card - Cumene (isopropyl-benzene)
AS 2508.6.014-1989 Safe storage and handling information card - Cyanides, inorganic (other than Sodium and Potassium Cyanides for which refer to AS 2508.6.002)
AS 2508.3.019-1983 Safe storage and handling information card - Methacrylates, HFP
AS 2243.5-1993 Safety in laboratories Non-ionizing radiations

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