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AS 1038.16-1996

AS 1038.16-1996

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Coal and coke - Analysis and testing - Assessment and reporting of results

Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Superseded date

06-30-2017

Superseded by

AS 1038.16-2005

Language(s)

English

Published date

01-01-1996

Publisher

Standards Australia

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Hardcopy - English
PDF 1 User - English
PDF 3 Users - English
PDF 5 Users - English
PDF 9 Users - English
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1 - AS 1038.16-1996 COAL AND COKE - ANALYSIS AND TESTING - ASSESSMENT AND REPORTING OF RESULTS
4 - PREFACE
5 - CONTENTS
6 - 1 SCOPE
6 - 2 REFERENCED DOCUMENTS
8 - 3 TERMS, DEFINITIONS, NOTATION AND ABBREVIATIONS
10 - 4 INTEGRITY OF RESULTS
10 - 4.1 General
10 - 4.2 Sample integrity
11 - 4.3 Procedures
11 - 4.4 Process control
12 - 4.5 Data management and documentation
12 - 5 ASSESSING THE ACCURACY OF TEST RESULTS
12 - 5.1 General
12 - 5.2 Reference material
12 - 5.3 Accuracy of the reference result
12 - 5.4 Accuracy of the test result
12 - 5.5 Comparison of results with calculated values
13 - 6 ASSESSING THE PRECISION OF TEST RESULTS
13 - 6.1 Replicate test results
13 - 6.2 Test result replication
13 - 6.3 Reproducibility
13 - 7 REPORTING ANALYSES TO DIFFERENT BASES
13 - 7.1 General
14 - 7.2 Corrections applicable to analytical results
16 - 7.3 Reporting analysis to different bases
19 - 8 REPORTING OF TEST RESULT
19 - 8.1 General
19 - 8.2 Number of decimal places
19 - 8.3 Test report
21 - APPENDIX A - DERIVATION OF EQUATIONS USED FOR METHOD CALCULATIONS
21 - A1 GENERAL
21 - A2 TOTAL MOISTURE (AS 1038.1, AS 1038.2 and AS 2434.1)
21 - A3 CARBON AND HYDROGEN (AS 1038.6.1, AS 1038.7 and AS 2434.6.1)
21 - A3.1 Carbon
22 - A3.2 Hydrogen
22 - A4 NITROGEN (AS 1038.6. 2, AS 1038.7 and AS 2434.6.1)
22 - A5 TOTAL SULFUR (ESCHKA METHOD) (AS 1038.6.3.1, AS 1038.7 and AS 2434.6.1)
23 - A6 TOTAL SULFUR OR CHLORINE (HIGH TEMPERATURE COMBUSTION/ TITRATION METHOD) (AS 1038.6.3.2, AS 1038.7 and AS 2434.6.1)
24 - A7 CHLORINE (ESCHKA METHOD) (AS 1038.8.1)
24 - A8 PHOSPHORUS
24 - A8.1 Ash digestion/molybdenum blue method (AS 1038.9.1)
25 - A8.2 Coal extraction method (AS 1038.9.2)
25 - A8.3 Ash digestion method (AS 1038.9.3)
25 - A8.4 Phosphorus in ash (AS 1038.14.1 and AS 1038.14.2)
25 - A9 FORMS OF SULFUR (AS 1038.11)
25 - A9. 1 Sulfate sulfur
25 - A9. 2 Pyritic sulfur
27 - A10 RELATIVE DENSITY (AS 1038.21.1.1 and AS 1038.21.1.2)
27 - A11 CARBONATE CARBON (AS 1038.23)
28 - APPENDIX B - SUGGESTED HIERARCHY OF PARAMETERS FOR A TEST REPORT
30 - APPENDIX C - PRECISION OF TEST METHODS AND SCHEDULE FOR REPORTING OF RESULTS

Sets out procedures and information for the assessment and reporting of test results obtained by use of the AS 1038 and AS 2434 series of methods for the evaluation of both higher rank and lower rank coal and coke.

Committee
MN-001
DocumentType
Standard
ISBN
0 7337 0103 5
Pages
32
PublisherName
Standards Australia
Status
Superseded
SupersededBy
Supersedes
UnderRevision

This Standard provides procedures and information for the assessment and reporting of results obtained by the use of methods detailed in the AS 1038 series and associated Standards. Technical aspects relevant to the derivation of formulas required for calculation and to the acceptance of analytical results are also provided.

First published as part of AS CK2.3-1949.
Revised and redesignated in part as AS K152.16-1965.
Revised and redesignated AS 1038.16-1975.
Second edition 1981.
Third edition 1986.
Fourth edition 1996.

AS 1038.14.1-1995 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Borate fusion/flame atomic absorption spectrometric method
AS 4264.3-1996 Coal and coke - Sampling Lower rank coal - Sampling procedures
AS 2706-1984 Numerical values - Rounding and interpretation of limiting values
AS 2434.2-1983 Methods for the analysis and testing of brown coal and brown coal char Determination of the volatile matter in low rank coal
AS 1038.21.1.1-1994 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/density bottle method
AS 1038.10.3-1998 Coal and coke - Analysis and testing Determination of trace elements - Coal and coke - Determination of boron content - ICP-AES method (Reconfirmed 2013) (Reconfirmed 2023)
AS 4156.1-1994 Coal preparation Higher rank coal - Float and sink testing (Reconfirmed 2013)
AS 2617-1996 Sampling from coal seams (Reconfirmed 2013)
AS 1152-1993 Specification for test sieves
AS 1038.12.2-1999 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Determination of Gray-King coke type (Reconfirmed 2013) (Reconfirmed 2023)
AS 2850-1986 Chemical analysis - Interlaboratory test programs - For determining precision of analytical method(s) - Guide to the planning and conduct
AS 1038.6.3.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - Eschka method (Reconfirmed 2013)
AS 1038.5.1-1988 Coal and coke - Analysis and testing Gross specific energy of coal and coke - Adiabatic calorimeters
AS 1038.12.1-1993 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Crucible swelling number
AS 2434.8-1993 Methods for the analysis and testing of lower rank coal and its chars Lower rank coal - Determination of ash
AS 1038.6.2-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Nitrogen
AS 2434.4-1985 Methods for the analysis and testing of brown coal and brown coal char - Determination of the apparent density of dried lower rank coal and its chars (mercury displacement method)
AS 1038.20-1992 Coal and coke - Analysis and testing Higher rank coal - Hardgrove grindability index
AS 1038.10.4-1989 Coal and coke - Analysis and testing Determination of trace elements - Coal, coke and fly-ash - Determination of fluorine content - Pyrohydrolysis method
AS 1038.18-1996 Coal and coke - Analysis and testing Coke - Size analysis
AS 2434.3-1984 Methods for the analysis and testing of brown coal and brown coal char - Determination of the moisture holding capacity of lower rank coals
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.6.3.2-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method
AS 2434.5-1984 Methods for the analysis and testing of brown coal and brown coal char - Determination of moisture in bulk samples and in analysis samples of char from lower rank coal
AS 2434.7-1986 Methods for the analysis and testing of lower rank coal and its chars - Determination of moisture in the analysis sample of lower rank coal
AS 2137-1981 Hard coal - Determination of plastic properties by the Gieseler plastometer
AS 1038.9.1-1992 Coal and coke - Analysis and testing Coal and coke - Phosphorus - Ash digestion/molybdenum blue method
AS 1038.9.2-1992 Coal and coke - Analysis and testing Higher rank coal - Phosphorus - Coal extraction method
AS 1038.11-1993 Coal and coke - Analysis and testing Coal - Forms of sulfur
AS 1038.1-1992 Coal and coke - Analysis and testing Higher rank coal - Total moisture
AS 1038.12.3-1993 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Dilatation
AS 1038.14.2-1995 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Acid digestion/flame atomic absorption spectrometric method
AS 1038.6.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Carbon and hydrogen (Reconfirmed 2013)
AS 1038.7-1981 Coal and coke - Analysis and testing - Ultimate analysis of coke
AS 4264.2-1996 Coal and coke - Sampling Coke - Sampling procedures (Reconfirmed 2013)
AS 1038.21.1.2-1994 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/volumetric method
AS 1038.6.3.3-1997 Coal and coke - Analysis and testing Higher rank coal - Ultimate analysis - Total sulfur - Infrared method (Reconfirmed 2013)
AS 1038.2-1995 Coal and coke - Analysis and testing Coke - Total moisture
AS 2434.1-1999 Methods for the analysis and testing of lower rank coal and its chars Determination of the total moisture content of lower rank coal (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.17-1989 Coal and coke - Analysis and testing Determination of moisture-holding capacity (equilibrium moisture) of higher rank coal
AS 1038.13-1990 Methods for the analysis and testing of coal and coke Tests specific to coke (Reconfirmed 2013)
AS 2434.6.1-1986 Methods for the analysis and testing of lower rank coal and its chars - Ultimate analysis of lower rank coal - Classical methods
AS 1038.9.3-1991 Coal and coke - Analysis and testing Coal and coke - Phosphorus - Ash digestion method
AS 1038.8.1-1999 Coal and coke - Analysis and testing Coal and coke - Chlorine - Eschka method (Reconfirmed 2013)
AS 1038.3-1989 Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
AS 1038.22-1992 Coal and coke - Analysis and testing Higher rank coal - Mineral matter and water of constitution
AS 2434.9-1991 Methods for the analysis and testing of lower rank coal and its chars Determination of four acid-extractable inorganic ions in lower rank coal
AS 1038.23-1994 Coal and coke - Analysis and testing Higher rank coal - Carbonate carbon
AS 1038.21.2-1992 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Lump sample
AS 1038.10.1-1986 Coal and coke - Analysis and testing Determination of trace elements - Determination of eleven trace elements in coal, coke and fly-ash - Flame atomic absorption spectrometric method
AS 1038.5.2-1989 Coal and coke - Analysis and testing Gross specific energy of coal and coke - Automatic isothermal-type calorimeters
AS 1038.10.5-1993 Coal and coke - Analysis and testing Coal, coke and fly-ash - Trace elements - Determination of mercury content
AS 1038.4-1995 Coal and coke - Analysis and testing Coke - Proximate analysis
AS 1038.19-1989 Coal and coke - Analysis and testing - Determination of the abrasion index of higher rank coal
AS 1038.15-1995 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Ash fusibility
AS 4264.1-1995 Coal and coke - Sampling Higher rank coal - Sampling procedures

AS 1038.8.2-2003 Coal and coke - Analysis and testing Coal and coke - Chlorine - High-temperature combustion method (Reconfirmed 2013)
AS 1038.4-1995 Coal and coke - Analysis and testing Coke - Proximate analysis
AS 2434.6-2002 Methods for the analysis and testing of lower rank coal and its chars Lower rank coal - Ultimate analysis - Classical methods (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.6.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Carbon and hydrogen (Reconfirmed 2013)
AS 1038.11-2002 Coal and coke - Analysis and testing Coal - Forms of sulfur (Reconfirmed 2013)
AS 1038.12.1-1993 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Crucible swelling number
AS 1038.14.2-2003 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Acid digestion/flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 2434.8-2002 Methods for the analysis and testing of lower rank coal and its chars Lower rank coal - Determination of ash (Reconfirmed 2013) (Reconfirmed 2023)
AS 2519-1993 Guide to the technical evaluation of higher rank coal deposits (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.21.1.2-2002 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/volumetric method (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.14.1-1995 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Borate fusion/flame atomic absorption spectrometric method
AS 1038.9.1-1992 Coal and coke - Analysis and testing Coal and coke - Phosphorus - Ash digestion/molybdenum blue method
AS 1038.6.3.2-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method
AS 1038.12.2-1999 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Determination of Gray-King coke type (Reconfirmed 2013) (Reconfirmed 2023)
AS 2434.8-1993 Methods for the analysis and testing of lower rank coal and its chars Lower rank coal - Determination of ash
AS 1038.10.1-2003 Coal and coke - Analysis and testing Determination of trace elements - Coal, coke and fly-ash - Determination of eleven trace elements - Flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 1038.6.3.2-2003 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method (Reconfirmed 2013)
AS 1038.10.3-1998 Coal and coke - Analysis and testing Determination of trace elements - Coal and coke - Determination of boron content - ICP-AES method (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.10.5-1993 Coal and coke - Analysis and testing Coal, coke and fly-ash - Trace elements - Determination of mercury content
AS 1038.21.1.1-2002 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/density bottle method
AS 2434.3-2002 Methods for the analysis and testing of lower rank coal and its chars Lower rank coal - Determination of the moisture holding capacity (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.8.1-1992 Coal and coke - Analysis and testing Coal and coke - Chlorine - Eschka method
AS 1038.8.2-1996 Coal and coke - Analysis and testing Coal and coke - Chlorine - High-temperature combustion method
AS 1038.12.4.2-1996 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Plasticity - Discontinuous-torque Gieseler method
AS 2434.2-2002 Methods for the analysis and testing of lower rank coal and its chars Lower rank coal - Determination of volatile matter (Reconfirmed 2013)
AS 3980-1991 Guide to the determination of desorbable gas content of coal seams - Direct method
AS 1038.12.3-2002 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Dilatation
AS 2434.9-1991 Methods for the analysis and testing of lower rank coal and its chars Determination of four acid-extractable inorganic ions in lower rank coal
AS 1038.23-1994 Coal and coke - Analysis and testing Higher rank coal - Carbonate carbon
AS 1038.14.1-2003 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Borate fusion/flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 2434.5-2002 Methods for the analysis and testing of lower rank coal and its chars Lower rank coal and its chars - Determination of moisture in bulk samples of lower rank coal and in analysis samples of char (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.6.2-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Nitrogen
AS 1038.11-1993 Coal and coke - Analysis and testing Coal - Forms of sulfur
AS 1038.1-1992 Coal and coke - Analysis and testing Higher rank coal - Total moisture
AS 1038.23-2002 Coal and coke - Analysis and testing Higher rank coal and coke - Carbonate carbon (Reconfirmed 2013)
AS 1038.17-2000 Coal and coke - Analysis and testing Higher rank coal - Moisture-holding capacity (equilibrium moisture) (Reconfirmed 2013)
AS 1038.12.3-1993 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Dilatation
AS 1038.5-1998 Coal and coke - Analysis and testing - Gross calorific value
AS 1038.14.2-1995 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Acid digestion/flame atomic absorption spectrometric method
AS 1038.20-1992 Coal and coke - Analysis and testing Higher rank coal - Hardgrove grindability index
AS 1038.20-1992 Coal and coke - Analysis and testing Higher rank coal - Hardgrove grindability index
AS 4264.4-1996 Coal and coke - Sampling - Determination of precision and bias
AS 1038.22-1992 Coal and coke - Analysis and testing Higher rank coal - Mineral matter and water of constitution
AS 1038.9.2-1992 Coal and coke - Analysis and testing Higher rank coal - Phosphorus - Coal extraction method
AS 1038.1-2001 Coal and coke - Analysis and testing Higher rank coal - Total moisture
AS 1038.10.5.1-2003 Coal and coke - Analysis and testing Coal, coke and fly-ash - Trace elements - Determination of mercury content - Tube combustion method (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.21.1.2-1994 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/volumetric method
AS 1038.2-1995 Coal and coke - Analysis and testing Coke - Total moisture
AS 2434.7-2002 Methods for the analysis and testing of lower rank coal and its chars Lower rank coal - Determination of moisture in the analysis sample (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.10.2-1998 Coal and coke - Analysis and testing Determination of trace elements - Coal and coke - Determination of arsenic, antimony and selenium - Hydride generation method (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.21.1.1-1994 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/density bottle method
AS 1038.12.1-2002 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Crucible swelling number
AS 1038.12.4.1-1996 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Plasticity - Continuous-torque Gieseler method
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 4156.7-1999 Coal preparation Coal size classifying equipment - Performance evaluation (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.6.3.3-1997 Coal and coke - Analysis and testing Higher rank coal - Ultimate analysis - Total sulfur - Infrared method (Reconfirmed 2013)
AS 2434.9-2000 Method for the analysis and testing of lower rank coal and its chars Determination of four acid-extractable inorganic ions in lower rank coal (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.6.3.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - Eschka method (Reconfirmed 2013)
AS 1038.10.4-2001 Coal and coke - Analysis and testing Determination of trace elements - Coal, coke and fly-ash - Determination of fluorine content - Pyrohydrolysis method (Reconfirmed 2013)

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