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ASTM D 8127 : 2017 : EDT 1

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Coupled Particulate and Elemental Analysis using X-ray Fluorescence (XRF) for In-Service Lubricants

Available format(s)

Hardcopy , PDF

Superseded date

25-05-2023

Superseded by

ASTM D 8127 : 2023

Language(s)

English

Published date

01-05-2018

£57.59
Excluding VAT

CONTAINED IN VOL. 05.05, 2018 Defines particle analysis2 test method for in-service lubricants describes using a combination of pore blockage particle counting and energy dispersive X-ray fluorescence (EDXRF) spectrometry for the quantitative determination of solid particle counts larger than four (4) micrometres, and elemental content of suspended particulate of iron (Fe) and copper (Cu) in such lubricants.

Committee
D 02
DocumentType
Test Method
Pages
8
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This automatic wear particle analysis2 test method for in-service lubricants describes using a combination of pore blockage particle counting and energy dispersive X-ray fluorescence (EDXRF) spectrometry for the quantitative determination of solid particle counts larger than four (4) micrometres, and elemental content of suspended particulate of iron (Fe) and copper (Cu) in such lubricants.

1.2This test method provides for the determination of the elemental content of suspended particulate of Fe greater than 4 μm in the range of 6 mg/kg to 223 mg/kg. Suspended particulate of copper greater than 4 μm is determined in the range of 3.5 mg/kg to 92.4 mg/kg in the lubricant. Total particle count greater than 4 μm is determined in the range of 11 495 particles/mL greater than 4 μm to 2 169 500 particles/mL greater than 4 μm in the lubricant.

1.3This test method is applicable to all known in-service lubricants (API Groups I-V) at any stage of degradation.

1.4This test method uses an empirical inter-element correction methodology.

1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 7343 : 2018 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 7343 : 2020 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 7578 : 2020 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 7578 : 2018 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants

ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 7751 : 2014 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 4057 : 1995 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 7669 : 2011 Standard Guide for Practical Lubricant Condition Data Trend Analysis
ASTM D 7720:2011 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 7874 : 2013 : R2018 Standard Guide for Applying Failure Mode and Effect Analysis (FMEA) to In-Service Lubricant Testing
ASTM E 1621 : 2013 Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry
ASTM D 4177 : 1995 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 7720 : 2021 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
ASTM D 5854 : 1996 : R2010 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 7874 : 2013 : R2022 Standard Guide for Applying Failure Mode and Effect Analysis (FMEA) to In-Service Lubricant Testing
ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM E 1621 : 2005 Standard Guide for X-Ray Emission Spectrometric Analysis
ASTM D 5854 : 2019 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 7751 : 2014 : EDT 1 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 5854 : 1996 : R2005 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM D 7874 : 2013 Standard Guide for Applying Failure Mode and Effect Analysis (FMEA) to In-Service Lubricant Testing
ASTM D 7751 : 2012 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM E 1621 : 2022 Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry
ASTM D 4177 : 2015 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 7669 : 2015 Standard Guide for Practical Lubricant Condition Data Trend Analysis
ASTM E 1621 : 2021 Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry
ASTM D 7751 : 2011 : EDT 1 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 4177 : 2022 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 4177 : 1995 : R2010 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 4177 : 1995 : R2000 Standard Practice for Automatic Sampling of Peroleum and Petroleum Products
ASTM D 5854 : 1996 : R2000 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM E 1621 : 2013 : REDLINE Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry
ISO 21018-3:2008 Hydraulic fluid power — Monitoring the level of particulate contamination of the fluid — Part 3: Use of the filter blockage technique
ASTM D 7669 : 2015 : REDLINE Standard Guide for Practical Lubricant Condition Data Trend Analysis
ASTM D 7751 : 2011 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 7751 : 2016 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 4177 : 2016 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 4177 : 2020 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 4177 : 1995 : R2005 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 7720 : 2011 : R2017 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
ASTM D 5854 : 2019 : REV A Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
ASTM E 1621 : 1994 : R1999 Standard Guide for X-Ray Emission Spectrometric Analysis
ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 7751 : 2016 : REDLINE Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 4177 : 2022 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 4177 : 2015 : REV A Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 7751 : 2016 : R2021 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 5854 : 1996 : R2015 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products

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