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ASTM D 7574 : 2016

ASTM D 7574 : 2016

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Determination of Bisphenol A in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry

Available format(s)

Hardcopy , PDF

Superseded date

09-06-2023

Superseded by

ASTM D 7574 : 2023

Language(s)

English

Published date

03-06-2016

Publisher

American Society for Testing and Materials

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Hardcopy - English
PDF - English
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This procedure covers the determination of bisphenol A (BPA) extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS).

Committee
D 19
DocumentType
Test Method
Pages
10
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This procedure covers the determination of bisphenol A (BPA) extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). BPA is qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry.

1.2The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3The method detection limit (MDL) and reporting limit (RL) for BPA are listed in Table 1.

(A)MDL determined following the Code of Federal Regulations, 40CFR Part 136, Appendix B.
(B)Lowest point of the reporting range, reporting limit, is calculated from the LV 1 concentration calibration standard in Table 4. Fig. 1 displays the signal/noise ratio at the reporting limit.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D 3694 : 1996 : R2011 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 5905 : 1998 : R2013 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 1129 : 2003 Standard Terminology Relating to Water
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM D 5847 : 1999 : REV A : EDT 1 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 3694 : 1996 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 2777 : 2012 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 5905 : 1998 : R2018 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 5847 : 2002 : R2007 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1129 : 2006 Standard Terminology Relating to Water
ASTM D 2777 : 2003 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
ASTM D 2777 : 2021 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 2777 : 2013 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 5847 : 2002 : R2012 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 5905 : 1998 : R2008 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 2777 : 1998 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
ASTM D 3694 : 1996 : R2017 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 1129 : 2013 : R2020 : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM D 3856 : 2011 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 5847 : 2002 : R2020 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
ASTM D 3694 : 1996 : R2004 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 1129 : 2002 Standard Terminology Relating to Water
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 5905 : 1998 : EDT 1 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 3856 : 1995 : R2006 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 1129 : 2004 Standard Terminology Relating to Water
ASTM D 5847 : 2022 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 2777 : 2008 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024)
ASTM D 2777 : 2006 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
ASTM D 3856 : 1995 : R2000 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
ASTM D 5847 : 2002 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 5905 : 1998 : R2003 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1129 : 2010 Standard Terminology Relating to Water
ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 2001 Standard Terminology Relating to Water
ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM D 2777 : 2008 : EDT 1 Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water

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