BS 2000-367(2006) : 2006
Current
The latest, up-to-date edition.
PETROLEUM PRODUCTS - DETERMINATION AND APPLICATION OF PRECISION DATA IN RELATION TO METHODS OF TEST
01-12-2013
Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Stages in the planning of an inter-laboratory test
programme for the determination of the precision of
a test method
4.1 General
4.2 Preparing a draft method of test
4.3 Planning a pilot programme with at least two
laboratories
4.4 Planning the inter-laboratory programme
4.5 Executing the inter-laboratory programme
5 Inspection of inter-laboratory results for uniformity
and for outliers
5.1 General
5.2 Transformation of data
5.3 Tests for outliers
5.4 Rejection of complete data from a sample
5.5 Estimating missing or rejected values
5.6 Rejection test for outlying laboratories
5.7 Confirmation of selected transformation
6 Analysis of variance, calculation and expression of
precision estimates
6.1 General
6.2 Analysis of variance
6.3 Expectation of mean squares and calculation of
precision estimates
6.4 Expression of precision estimates of a method of test
7 Significance of repeatability (r) and reproducibility (R)
7.1 General
7.2 Repeatability, r
7.3 Reproducibility, R
8 Specifications
8.1 Aim of specifications
8.2 Construction of specifications limits in relation
to precision
9 Quality control against specifications
9.1 General
9.2 Testing margin at the supplier
9.3 Testing margin at the recipient
10 Dispute procedure
Annex A (normative) Determination of number of samples
required
Annex B (informative) Derivation of equation for calculating
the number of samples required
Annex C (normative) Notation and tests
Annex D (normative) Example results of test for determination
of bromine number and statistical tables
Annex E (normative) Types of dependence and corresponding
transformations
Annex F (normative) Weighted linear regression analysis
Annex G (normative) Rules for rounding off results
Annex H (informative) Explanation of equations given in Clause 7
Annex I (informative) Specifications that relate to a specified
degree of criticality
Bibliography
Describes calculation of precision estimates and application to specifications, also contains definitions of relevant statistical terms, procedures for adoption in planning of an inter-laboratory test programme for determination of precision of a test method, calculation method for precision for results of programme and procedure for interpreting laboratory results relating to precision of methods and to limits laid down by specifications.
Committee |
PTI/13
|
DevelopmentNote |
Also numbered as BS EN ISO 4259 Supersedes BS 2000-367(1996) & BS 2000-0.3(1996). (02/2007) Also numbered as IP 367. (05/2007)
|
DocumentType |
Standard
|
PublisherName |
Energy Institute (formerly Institute of Petroleum - IP)
|
Status |
Current
|
SupersededBy | |
Supersedes |
Standards | Relationship |
EN ISO 4259:2006 | Identical |
ISO 4259:2006 | Identical |
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DEFSTAN 91-38/2(2015) : 2015 | PETROLATUM, TECHNICAL JOINT SERVICE DESIGNATION: PX-6 PETROLATUM, TECHNICAL NATO CODE NO: S-743 JOINT SERVICE DESIGNATION: PX-7 |
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ISO 3534-2:2006 | Statistics — Vocabulary and symbols — Part 2: Applied statistics |
ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
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