ASTM D 6481 : 2014 : R2019
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Determination of Phosphorus, Sulfur, Calcium, and Zinc in Lubrication Oils by Energy Dispersive X-ray Fluorescence Spectroscopy
Hardcopy , PDF
03-22-2024
English
07-02-2019
Important note : All end users must be registered with an Account prior to user licenses being assigned.This test method covers the quantitative determination of additive elements in unused lubricating oils, as shown inTable 1.
| Committee |
D 02
|
| DocumentType |
Test Method
|
| Pages |
5
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
1.1This test method covers the quantitative determination of additive elements in unused lubricating oils, as shown in Table 1.
1.2This test method is limited to the use of energy dispersive X-ray fluorescence (EDXRF) spectrometers employing an X-ray tube for excitation in conjunction with the ability to separate the signals of adjacent elements.
1.3This test method uses interelement correction factors calculated from empirical calibration data.
1.4This test method is not suitable for the determination of magnesium and copper at the concentrations present in lubricating oils.
1.5This test method excludes lubricating oils that contain chlorine or barium as an additive element.
1.6This test method can be used by persons who are not skilled in X-ray spectrometry. It is intended to be used as a routine test method for production control analysis.
1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations to use.
1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| ASTM D 7455 : 2019 | Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis |
| ASTM D 6074 : 2015 | Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils |
| ASTM D 7578 : 2018 | Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants |
| ASTM D 7343 : 2018 | Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants |
| ASTM D 7343 : 2020 | Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants |
| ASTM D 7578 : 2020 | Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants |
| ASTM D 6074 : 2015 : R2022 | Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils |
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