UNI CEN/TS 16182 : 2012
Current
The latest, up-to-date edition.
SLUDGE TREATED BIOWASTE AND SOIL - DETERMINATION OF NONYLPHENOLS (NP) AND NONYLPHENOL-MONO- AND DIETHOXYLATES USING GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GCMS)
05-04-2012
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sample storage and sample pretreatment
8 Procedure
9 Calculation and expression of results
10 Precision
11 Test report
Annex A (informative) - Repeatability and reproducibility
data
Annex B (informative) - Example of chromatographic
conditions and example of a chromatogram
Bibliography
This Technical Specification specifies a method for the determination of nonylphenols (NP), nonylphenolmonoethoxylates (NP1EO) and nonylphenol-diethoxylates (NP2EO) in sludge, treated waste and soil, by using GC-MS.
| Committee |
CT 4
|
| DocumentType |
Technical Specification
|
| PublisherName |
Ente Nazionale Italiano di Unificazione (UNI)
|
| Status |
Current
|
| Standards | Relationship |
| CEN/TS 16182:2012 | Identical |
| ISO 18857-1:2005 | Water quality — Determination of selected alkylphenols — Part 1: Method for non-filtered samples using liquid-liquid extraction and gas chromatography with mass selective detection |
| EN ISO 18857-1:2006 | Water quality - Determination of selected alkylphenols - Part 1: Method for non-filtered samples using liquid-liquid extraction and gas chromatography with mass selective detection (ISO 18857-1:2005) |
| ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| ISO 18857-2:2009 | Water quality Determination of selected alkylphenols Part 2: Gas chromatographic-mass spectrometric determination of alkylphenols, their ethoxylates and bisphenol A in non-filtered samples following solid-phase extraction and derivatisation |
| ISO 16720:2005 | Soil quality Pretreatment of samples by freeze-drying for subsequent analysis |
| EN ISO 18857-2:2011 | Water quality - Determination of selected alkylphenols - Part 2: Gas chromatographic-mass spectrometric determination of alkylphenols, their ethoxylates and bisphenol A in non-filtered samples following solid-phase extraction and derivatisation (ISO 18857-2:2009) |
| EN ISO 16720:2007 | Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005) |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
| EN ISO 22892:2011 | Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006) |
| EN 15934:2012 | Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content |
| EN 16179:2012 | Sludge, treated biowaste and soil - Guidance for sample pretreatment |
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