EN ISO 6498:2012
Current
Current
The latest, up-to-date edition.
Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)
Published date
01-06-2012
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Foreword
1 Scope
2 Terms and definitions
3 Principle
4 Consideration of sample preparation errors
5 Safety precautions
6 Apparatus
7 Procedure
8 Performance tests (quality control)
9 Categories of feeds - Special remarks and flow charts
Annex A (informative) - Calculations, examples and
tables for minimum mass
Bibliography
ISO 6498:2012 specifies guidelines for the preparation of test samples from laboratory samples of animal feeding stuffs, including pet foods.The guidelines are overruled by special instructions and regulations for sample preparation demanded by specific analysis methods.
| Committee |
CEN/TC 327
|
| DevelopmentNote |
Supersedes PREN ISO 6498. (07/2012)
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Standards | Relationship |
| I.S. EN ISO 6498:2012 | Identical |
| UNE-EN ISO 6498:2012 | Identical |
| BS EN ISO 6498:2012 | Identical |
| UNI EN ISO 6498 : 2012 | Identical |
| DIN EN ISO 6498:2012-09 | Identical |
| NBN EN ISO 6498 : 2012 | Identical |
| NEN EN ISO 6498 : 2012 | Identical |
| ISO 6498:2012 | Identical |
| NF EN ISO 6498 : 2012 | Identical |
| PN EN ISO 6498 : 2012 | Identical |
| SN EN ISO 6498:2012 | Identical |
| NS EN ISO 6498 : 2012 | Identical |
| I.S. EN 15621:2017 | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, SULPHUR, IRON, ZINC, COPPER, MANGANESE AND COBALT AFTER PRESSURE DIGESTION BY ICP-AES |
| UNE-EN 16278:2012 | Animal feeding stuffs - Determination of inorganic arsenic by hydride generation atomic absorption spectrometry (HG-AAS) after microwave extraction and separation by solid phase extraction (SPE) |
| I.S. EN 17053:2018 | ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF TRACE ELEMENTS, HEAVY METALS AND OTHER LEMENTS IN FEED BY ICP-MS (MULTI-METHOD) |
| 15/30330813 DC : 0 | BS EN 16939 - ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETECTION OF TYLOSIN, SPIRAMYCIN AND VIRGINIAMYCIN - THINLAYER CHROMATOGRAPHY AND BIOAUTOGRAPHY |
| BS EN 16278:2012 | Animal feeding stuffs. Determination of inorganic arsenic by hydride generation atomic absorption spectrometry (HG-AAS) after microwave extraction and separation by solid phase extraction (SPE) |
| 16/30342876 DC : 0 | BS EN 15550 - ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CADMIUM AND LEAD BY GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS) AFTER PRESSURE DIGESTION |
| UNE-EN 16877:2017 | Animal feeding stuffs: Methods of sampling and analysis - Determination of T-2 and HT-2 toxins, Deoxynivalenol and Zearalenone, in feed materials and compound feed by LC-MS |
| I.S. EN 16277:2012 | ANIMAL FEEDING STUFFS - DETERMINATION OF MERCURY BY COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CVAAS) AFTER MICROWAVE PRESSURE DIGESTION (EXTRACTION WITH 65% NITRIC ACID AND 30% HYDROGEN PEROXIDE) |
| UNI EN 16279 : 2012 | ANIMAL FEEDING STUFFS - DETERMINATION OF FLUORIDE CONTENT AFTER HYDROCHLORIC ACID TREATMENT BY ION-SENSITIVE ELECTRODE METHOD (ISE) |
| BS EN 15510:2017 | Animal feeding stuffs. Methods of sampling and analysis. Determination of calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum and lead by ICP-AES |
| I.S. EN 15510:2017 | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, IRON, ZINC, COPPER, MANGANESE, COBALT, MOLYBDENUM AND LEAD BY ICP-AES |
| DIN EN 16877:2017-03 | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF T-2 AND HT-2 TOXINS, DEOXYNIVALENOL AND ZEARALENONE, IN FEED MATERIALS AND COMPOUND FEED BY LC-MS |
| EN 15621:2017 | Animal feeding stuffs: Methods of sampling and analysis - Determination of calcium, sodium, phosphorus, magnesium, potassium, sulphur, iron, zinc, copper, manganese and cobalt after pressure digestion by ICP-AES |
| DIN EN 15510:2017-10 | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, IRON, ZINC, COPPER, MANGANESE, COBALT, MOLYBDENUM AND LEAD BY ICP-AES |
| BS EN 15621:2017 | Animal feeding stuffs: Methods of sampling and analysis. Determination of calcium, sodium, phosphorus, magnesium, potassium, sulphur, iron, zinc, copper, manganese and cobalt after pressure digestion by ICP-AES |
| I.S. EN 17049:2018 | ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - IDENTIFICATION OF TYLOSIN, SPIRAMYCIN, VIRGINIAMYCIN, CARBADOX AND OLAQUINDOX AT SUB-ADDITIVE LEVELS IN COMPOUND FEED - CONFIRMATORY ANALYSIS BY LC-MS |
| I.S. EN 17050:2017 | ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF IODINE IN ANIMAL FEED BY ICP-MS |
| PREN 15550 : DRAFT 2016 | ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CADMIUM AND LEAD BY GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS) AFTER PRESSURE DIGESTION |
| BS EN 16939:2017 | Animal feeding stuffs. Methods of sampling and analysis. Detection of tylosin, spiramycin and virginiamycin. Thin Layer Chromatography and bioautography |
| UNI EN 16278 : 2012 | ANIMAL FEEDING STUFFS - DETERMINATION OF INORGANIC ARSENIC BY HYDRIDE GENERATION ATOMIC ABSORPTION SPECTROMETRY (HG-AAS) AFTER MICROWAVE EXTRACTION AND SEPARATION BY SOLID PHASE EXTRACTION (SPE) |
| BS EN 16877:2016 | Animal feeding stuffs. Methods of sampling and analysis. Determination of T-2 and HT-2 toxins, Deoxynivalenol and Zearalenone, in feed materials and compound feed by LCMS |
| PREN 15621 : DRAFT 2016 | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, SULPHUR, IRON, ZINC, COPPER, MANGANESE AND COBALT AFTER PRESSURE DIGESTION BY ICP-AES |
| I.S. EN 16877:2016 | ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF T-2 AND HT-2 TOXINS, DEOXYNIVALENOL AND ZEARALENONE, IN FEED MATERIALS AND COMPOUND FEED BY LC-MS |
| I.S. EN 16939:2017 | ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETECTION OF TYLOSIN, SPIRAMYCIN AND VIRGINIAMYCIN - THIN LAYER CHROMATOGRAPHY AND BIOAUTOGRAPHY |
| 17/30337117 DC : 0 | BS EN 17212 - ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF MELAMINE AND CYANURIC ACID CONTENT BY LIQUID CHROMATOGRAPHIC METHOD WITH MASS SPECTROMETRIC DETECTION (LC-MS/MS) |
| DIN EN 16930:2015-12 (Draft) | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CARBADOX AND OLAQUINDOX BY HPLC/UV |
| UNE-EN 15510:2018 | Animal feeding stuffs: Methods of sampling and analysis - Determination of calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum and lead by ICP-AES |
| BS EN 15550:2017 | Animal feeding stuffs: Methods of sampling and analysis. Determination of cadmium and lead by graphite furnace atomic absorption spectrometry (GF-AAS) after pressure digestion |
| I.S. EN 15550:2017 | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CADMIUM AND LEAD BY GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS) AFTER PRESSURE DIGESTION |
| 16/30341249 DC : 0 | BS EN 17050 - ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF IODINE IN ANIMAL FEED BY ANION-EXCHANGE ICP-MS |
| 14/30288021 DC : 0 | BS EN ISO 11085 - CEREALS, CEREALS-BASED PRODUCTS AND ANIMAL FEEDING STUFFS - DETERMINATION OF CRUDE FAT AND TOTAL FAT CONTENT BY THE RANDALL EXTRACTION METHOD |
| BS EN 16279:2012 | Animal feeding stuffs. Determination of fluoride content after hydrochloric acid treatment by ion-sensitive electrode method (ISE) |
| PREN 15510 : DRAFT 2016 | ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, IRON, ZINC, COPPER, MANGANESE, COBALT, MOLYBDENUM AND LEAD BY ICP-AES |
| PREN 17212 : DRAFT 2017 | ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALSYSIS - DETERMINATION OF MELAMINE AND CYANURIC ACID CONTENT BYLIQUID CHROMATOGRAPHIC METHOD WITH MASS SPECTROMETRIC DETECTION (LC-MS/MS) |
| BS EN 16930:2017 | Animal feeding stuffs. Methods of sampling and analysis. Determination of carbadox and olaquindox by HPLC/UV |
| BS EN 16277:2012 | Animal feeding stuffs. Determination of mercury by cold-vapour atomic absorption spectrometry (CVAAS) after microwave pressure digestion (extraction with 65% nitric acid and 30% hydrogen peroxide) |
| UNI EN 16277 : 2012 | ANIMAL FEEDING STUFFS - DETERMINATION OF MERCURY BY COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CVAAS) AFTER MICROWAVE PRESSURE DIGESTION (EXTRACTION WITH 65% NITRIC ACID AND 30% HYDROGEN PEROXIDE) |
| DIN EN 16278:2012-09 | ANIMAL FEEDING STUFFS - DETERMINATION OF INORGANIC ARSENIC BY HYDRIDE GENERATION ATOMIC ABSORPTION SPECTROMETRY (HG-AAS) AFTER MICROWAVE EXTRACTION AND SEPARATION BY SOLID PHASE EXTRACTION (SPE) |
| I.S. EN 16279:2012 | ANIMAL FEEDING STUFFS - DETERMINATION OF FLUORIDE CONTENT AFTER HYDROCHLORIC ACID TREATMENT BY ION-SENSITIVE ELECTRODE METHOD (ISE) |
| DIN EN 16877:2015-07 (Draft) | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF T-2 AND HT-2 TOXINS, DEOXYNIVALENOL AND ZEARALENONE, IN FEED MATERIALS AND COMPOUND FEED BY LC-MS |
| UNE-EN 16277:2012 | Animal feeding stuffs - Determination of mercury by cold-vapour atomic absorption spectrometry (CVAAS) after microwave pressure digestion (extraction with 65 % nitric acid and 30 % hydrogen peroxide) |
| EN 17053:2018 | Animal feeding stuffs: Methods of sampling and analysis - Determination of trace elements, heavy metals and other elements in feed by ICP-MS (multi-method) |
| DIN EN 16939:2015-12 (Draft) | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETECTION OF TYLOSIN, SPIRAMYCIN AND VIRGINIAMYCIN - THIN LAYER CHROMATOGRAPHY AND BIOAUTOGRAPHY |
| DIN EN 16279:2012-09 | Animal feeding stuffs - Determination of fluoride content after hydrochloric acid treatment by ion-sensitive electrode method (ISE) |
| DIN EN 15621:2016-11 (Draft) | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, SULPHUR, IRON, ZINC, COPPER, MANGANESE AND COBALT AFTER PRESSURE DIGESTION BY ICP-AES |
| 16/30342879 DC : 0 | BS EN 15621 - ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, SULPHUR, IRON, ZINC, COPPER, MANGANESE AND COBALT AFTER PRESSURE DIGESTION BY ICP-AES |
| 16/30342873 DC : 0 | BS EN 15510 - ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, IRON, ZINC, COPPER, MANGANESE, COBALT, MOLYBDENUM AND LEAD BY ICP-AES |
| I.S. EN 16930:2017 | ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CARBADOX AND OLAQUINDOX BY HPLC/UV |
| UNE-EN 16279:2012 | Animal feeding stuffs - Determination of fluoride content after hydrochloric acid treatment by ion-sensitive electrode method (ISE) |
| I.S. EN 16278:2012 | ANIMAL FEEDING STUFFS - DETERMINATION OF INORGANIC ARSENIC BY HYDRIDE GENERATION ATOMIC ABSORPTION SPECTROMETRY (HG-AAS) AFTER MICROWAVE EXTRACTION AND SEPARATION BY SOLID PHASE EXTRACTION (SPE) |
| UNE-EN 16930:2018 | Animal feeding stuffs: Methods of sampling and analysis - Determination of carbadox and olaquindox by HPLC/UV |
| UNE-EN 15550:2018 | Animal feeding stuffs: Methods of sampling and analysis - Determination of cadmium and lead by graphite furnace atomic absorption spectrometry (GF-AAS) after pressure digestion |
| DIN EN 15550:2016-11 (Draft) | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CADMIUM AND LEAD BY GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS) AFTER PRESSURE DIGESTION |
| DIN EN 15510:2016-11 (Draft) | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, IRON, ZINC, COPPER, MANGANESE, COBALT, MOLYBDENUM AND LEAD BY ICP-AES |
| EN 16277:2012 | Animal feeding stuffs - Determination of mercury by cold-vapour atomic absorption spectrometry (CVAAS) after microwave pressure digestion (extraction with 65 % nitric acid and 30 % hydrogen peroxide) |
| EN 16930:2017 | Animal feeding stuffs: Methods of sampling and analysis - Determination of carbadox and olaquindox by HPLC/UV |
| EN 17050:2017 | Animal feeding stuffs: Methods of sampling and analysis - Determination of iodine in animal feed by ICP-MS |
| EN 16279:2012 | Animal feeding stuffs - Determination of fluoride content after hydrochloric acid treatment by ion-sensitive electrode method (ISE) |
| EN 16939:2017 | Animal feeding stuffs: Methods of sampling and analysis - Detection of tylosin, spiramycin and virginiamycin - Thin Layer Chromatography and bioautography |
| EN 16877:2016 | Animal feeding stuffs: Methods of sampling and analysis - Determination of T-2 and HT-2 toxins, Deoxynivalenol and Zearalenone, in feed materials and compound feed by LC-MS |
| EN 16278:2012 | Animal feeding stuffs - Determination of inorganic arsenic by hydride generation atomic absorption spectrometry (HG-AAS) after microwave extraction and separation by solid phase extraction (SPE) |
| EN 15510:2017 | Animal feeding stuffs: Methods of sampling and analysis - Determination of calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum and lead by ICP-AES |
| EN 15550:2017 | Animal feeding stuffs: Methods of sampling and analysis - Determination of cadmium and lead by graphite furnace atomic absorption spectrometry (GF-AAS) after pressure digestion |
| 16/30330807 DC : 0 | BS EN 17049 - IDENTIFICATION OF TYLOSIN, SPIRAMYCIN, VIRGINIAMYCIN, CARBADOX AND OLAQUINDOX AT SUB-ADDITIVE LEVELS IN COMPOUND FEED - CONFIRMATORY ANALYSIS BY LCMS |
| DIN EN 16277:2012-09 | ANIMAL FEEDING STUFFS - DETERMINATION OF MERCURY BY COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CVAAS) AFTER MICROWAVE PRESSURE DIGESTION (EXTRACTION WITH 65% NITRIC ACID AND 30% HYDROGEN PEROXIDE) |
| BS EN 17050:2017 | Animal feeding stuffs: Methods of sampling and analysis. Determination of iodine in animal feed by ICP-MS |
| EN 17049:2018 | Animal feeding stuffs: Methods of sampling and analysis - Identification of tylosin, spiramycin, virginiamycin, carbadox and olaquindox at sub-additive levels in compound feed - Confirmatory analysis by LC-MS |
| DIN EN 16939:2017-10 | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETECTION OF TYLOSIN, SPIRAMYCIN AND VIRGINIAMYCIN - THIN LAYER CHROMATOGRAPHY AND BIOAUTOGRAPHY |
| DIN EN 15621:2017-10 | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CALCIUM, SODIUM, PHOSPHORUS, MAGNESIUM, POTASSIUM, SULPHUR, IRON, ZINC, COPPER, MANGANESE AND COBALT AFTER PRESSURE DIGESTION BY ICP-AES |
| DIN EN 15550:2017-10 | ANIMAL FEEDING STUFFS - METHODS OF SAMPLING AND ANALYSIS - DETERMINATION OF CADMIUM AND LEAD BY GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS) AFTER PRESSURE DIGESTION |
| ISO 664:2008 | Oilseeds Reduction of laboratory sample to test sample |
| ISO 6497:2002 | Animal feeding stuffs Sampling |
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