EN 16694 : 2015
Current
The latest, up-to-date edition.
WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS)
23-09-2015
European foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
9 Calibration
10 Quantification
11 Expression of results
12 Test report
Annex A (informative) - Suitable gas chromatographic
conditions and example chromatograms
Annex B (informative) - Repeatability and reproducibility data
Annex C (informative) - Examples of suitable solid phase
extraction disks
Annex D (informative) - Clean up procedure
Bibliography
This European Standard specifies a method for the determination of six selected polybrominated diphenyl ethers (PBDEs) listed in Table 1, representative for technical BDEs in water samples in mass concentrations ≥ 0,025 ng/l (for each individual congener).
Committee |
CEN/TC 230
|
DevelopmentNote |
Supersedes PREN 16694. (09/2015)
|
DocumentType |
Standard
|
PublisherName |
Comite Europeen de Normalisation
|
Status |
Current
|
Standards | Relationship |
SN EN 16694 : 2015 | Identical |
BS EN 16694:2015 | Identical |
NEN EN 16694 : 2015 | Identical |
NBN EN 16694 : 2015 | Identical |
I.S. EN 16694:2015 | Identical |
NF EN 16694 : 2015 | Identical |
DIN EN 16694:2015-12 | Identical |
UNI EN 16694 : 2015 | Identical |
PN EN 16694 : 2016 | Identical |
NS EN 16694 : 2015 | Identical |
UNE-EN 16694:2016 | Identical |
EN 16377:2013 | Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste |
ISO/TS 13530:2009 | Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis |
ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
ISO 5667-3:2012 | Water quality Sampling Part 3: Preservation and handling of water samples |
ISO 5667-1:2006 | Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques |
EN ISO 22032:2009 | Water quality - Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge - Method using extraction and gas chromatography/mass spectrometry (ISO 22032:2006) |
ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
ISO 22032:2006 | Water quality — Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge — Method using extraction and gas chromatography/mass spectrometry |
EN ISO 5667-3:2012 | Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012) |
ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
EN ISO 22892:2011 | Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006) |
EN ISO 5667-1 : 2006 COR 2007 | WATER QUALITY - SAMPLING - PART 1: GUIDANCE ON THE DESIGN OF SAMPLING PROGRAMMES AND SAMPLING TECHNIQUES |
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