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CEN/TS 15621:2007

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

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Animal feeding stuffs - Determination of calcium, sodium, phosphorus, magnesium, potassium, sulphur, iron, zinc, copper, manganese, cobalt and molybdenum after pressure digestion by ICP-AES

Withdrawn date

10-03-2023

Superseded by

EN 15621:2017

Published date

01-08-2007

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1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sampling
8 Preparation of the test sample
9 Procedure
10 Calculation and expression of the result
11 Precision
12 Test report
Annex A (informative) Results of the interlaboratory tests
Annex B (informative) Notes on the detection technique,
                      interferences and quantification, and
                      pressure digestion
Bibliography

This Technical Specification specifies a method for the determination of the minerals calcium, sodium, phosphorus, magnesium, potassium and sulphur and the elements iron, zinc, copper, manganese, cobalt, molybdenum in animal feeding stuffs by inductively coupled plasma atomic emission spectrometry (ICP-AES) after pressure digestion.The method limit of quantification for each element is dependent on the sample matrix as well as of the instrument. The method is not applicable for determination of low concentrations of elements. A limit of quantification of 1 mg/kg should normally be obtained.

Committee
CEN/TC 327
DocumentType
Technical Specification
PublisherName
Comite Europeen de Normalisation
Status
Withdrawn
SupersededBy

10/30199728 DC : 0 BS EN 16206 - ANIMAL FEEDING STUFFS - DETERMINATION OF ARSENIC BY HYDRIDE GENERATION ATOMIC ABSORPTION SPECTROMETRY (HGAAS) AFTER MICROWAVE PRESSURE DIGESTION (EXTRACTION WITH 65% NITRIC ACID AND 30% HYDROGEN PEROXIDE)
10/30199731 DC : 0 BS EN 16159 - ANIMAL FEEDING STUFFS - DETERMINATION OF SELENIUM BY HYDRIDE GENERATION ATOMIC ABSORPTION SPECTROMETRY (HGAAS) AFTER MICROWAVE DIGESTION (EXTRACTION WITH 65% NITRIC ACID AND 30% HYDROGEN PEROXIDE)
11/30199734 DC : 0 BS EN 16277 - ANIMAL FEEDING STUFFS - DETERMINATION OF MERCURY BY COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CVAAS) AFTER MICROWAVE PRESSURE DIGESTION (EXTRACTION WITH 65% NITRIC ACID AND 30% HYDROGEN PEROXIDE)

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
ISO 6497:2002 Animal feeding stuffs Sampling
EN 13805:2014 Foodstuffs - Determination of trace elements - Pressure digestion
EN ISO 6497:2005 Animal feeding stuffs - Sampling (ISO 6497:2002)
ISO 6498:2012 Animal feeding stuffs — Guidelines for sample preparation
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)

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