ASTM E 2554 : 2018 : EDT 1
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques
Hardcopy , PDF
25-10-2024
English
01-04-2018
Committee |
E 11
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DocumentType |
Standard Practice
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Pages |
8
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ProductNote |
ε1 NOTE—Editorial corrections were made throughout in September 2019.
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PublisherName |
American Society for Testing and Materials
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Status |
Superseded
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SupersededBy | |
Supersedes |
1.1This practice describes techniques for a laboratory to estimate the uncertainty of a test result using data from test results on a control sample. This practice provides one method for a laboratory to estimate Measurement Uncertainty in accordance with Section A22.3 in Form and Style for ASTM Standards.
1.2Uncertainty as defined by this practice applies to the capabilities of a single laboratory. Any estimate of uncertainty determined through the use of this practice applies only to the individual laboratory for which the data are presented.
1.3The laboratory uses a well defined and established test method in determining a series of test results. The uncertainty estimated using this practice only applies when the same test method is followed. The uncertainty only applies for the material types represented by the control samples, and multiple control samples may be needed, especially if the method has different precision for different sample types or response levels.
1.4The uncertainty estimate determined by this practice represents the intermediate precision of test results. This estimate seeks to quantify the total variation expected within a single laboratory using a single established test method while incorporating as many known sources of variation as possible.
1.5This practice does not establish error estimates (error budget) attributed to individual factors that could influence uncertainty.
1.6This practice describes the use of control charts to evaluate the data obtained and presents a special type of control chart to monitor the estimate of uncertainty.
1.7The system of units for this standard is not specified. Dimensional quantities in the standard are presented only as illustrations of calculation methods. The examples are not binding on products or test methods treated.
1.8This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.9This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ASTM D 8018 : 2015 : R2020 | Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Soil by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS) |
ASTM E 2655 : 2014 : R2020 | Standard Guide for Reporting Uncertainty of Test Results and Use of the Term Measurement Uncertainty in ASTM Test Methods |
ASTM E 1488 : 2012 : R2018 | Standard Guide for Statistical Procedures to Use in Developing and Applying Test Methods |
ASTM D 7600 : 2016 : R2017 | Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry |
ASTM E 2655 : 2014 | Standard Guide for Reporting Uncertainty of Test Results and Use of the Term Measurement Uncertainty in ASTM Test Methods |
ASTM D 8018 : 2015 | Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Soil by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS) |
ASTM F 76 : 2008 : R2016 : EDT 1 | Standard Test Methods for Measuring Resistivity and Hall Coefficient and Determining Hall Mobility in Single-Crystal Semiconductors (Withdrawn 2023) |
ASTM E 903 : 2012 | Standard Test Method for Solar Absorptance, Reflectance, and Transmittance of Materials Using Integrating Spheres |
ASTM D 7742 : 2017 | Standard Practice for Determination of Nonylphenol Polyethoxylates (NPnEO, 3 ≤ n ≤ 18) and Octylphenol Polyethoxylates (OPnEO, 2 ≤ n ≤ 12) in Water by Single Reaction Monitoring (SRM) Liquid Chromatography/ Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 7448 : 2016 | Standard Practice for Establishing the Competence of Laboratories Using ASTM Procedures in the Sampling and Analysis of Coal and Coke (Withdrawn 2024) |
ASTM D 7599 : 2016 : R2017 | Standard Test Method for Determination of Diethanolamine, Triethanolamine, <emph type="ital">N</emph>-Methyldiethanolamine and <emph type="ital">N</emph >-Ethyldiethanolamine in Water by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS) |
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ASTM D 7968 : 2017 : REV A | Standard Test Method for Determination of Polyfluorinated Compounds in Soil by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS) |
ASTM E 384 : 2017 | Standard Test Method for Microindentation Hardness of Materials |
ASTM D 7979 : 2017 | Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances in Water, Sludge, Influent, Effluent and Wastewater by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 8024 : 2016 | Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Water by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS) |
ASTM E 1323 : 2015 | Standard Guide for Evaluating Laboratory Measurement Practices and the Statistical Analysis of the Resulting Data |
ASTM E 1125 : 2016 | Standard Test Method for Calibration of Primary Non-Concentrator Terrestrial Photovoltaic Reference Cells Using a Tabular Spectrum |
ASTM D 7644 : 2016 | Standard Test Method for Determination of Bromadiolone, Brodifacoum, Diphacinone and Warfarin in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 8064 : 2016 | Standard Test Method for Elemental Analysis of Soil and Solid Waste by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry Using Multiple Monochromatic Excitation Beams (Withdrawn 2024) |
ASTM C 1210 : 2018 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry |
ASTM D 5994/D5994M : 2010 : R2015 : EDT 1 | Standard Test Method for Measuring Core Thickness of Textured Geomembranes |
ASTM D 7597 : 2016 : R2017 | Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Hydrogen Dimethylamidophosphate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Water by Liquid Chromatography/Tandem Mass Spectrometry |
ASTM D 7645 : 2016 | Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl, and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 7466/D7466M : 2010 : R2015 : EDT 1 | Standard Test Method for Measuring Asperity Height of Textured Geomembranes |
ASTM D 8025 : 2016 | Standard Test Method for Determination of Select Pesticides in Water by Multiple Reaction Monitoring Liquid Chromatography Tandem Mass Spectrometry |
ASTM D 7598 : 2016 : R2017 | Standard Test Method for Determination of Thiodiglycol in Water by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry |
ASTM D 7979 : 2019 | Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances in Water, Sludge, Influent, Effluent, and Wastewater by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS) |
ASTM E 2866 : 2021 | Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid, and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid Chromatography/Tandem Mass Spectrometry |
ASTM E 2787 : 2021 | Standard Test Method for Determination of Thiodiglycol in Soil Using Pressurized Fluid Extraction Followed by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 8421 : 2024 | Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances (PFAS) in Aqueous Matrices by Co-solvation followed by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 7645 : 2023 | Standard Test Method for Determination of Aldicarb, Aldicarb Sulfone, Aldicarb Sulfoxide, Carbofuran, Methomyl, Oxamyl, and Thiofanox in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 7968 : 2023 | Standard Test Method for Determination of Polyfluorinated Compounds in Soil by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 7598 : 2016 : R2024 | Standard Test Method for Determination of Thiodiglycol in Water by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry |
ASTM D 8025 : 2023 | Standard Test Method for Determination of Select Pesticides in Water by Multiple Reaction Monitoring Liquid Chromatography Tandem Mass Spectrometry |
ASTM D 7466/D7466M : 2023 | Standard Test Method for Measuring Asperity Height of Textured Geomembranes |
ASTM E 1125 : 2016 : R2020 | Standard Test Method for Calibration of Primary Non-Concentrator Terrestrial Photovoltaic Reference Cells Using a Tabular Spectrum |
ASTM E 1323 : 2015 : R2020 | Standard Guide for Evaluating Laboratory Measurement Practices and the Statistical Analysis of the Resulting Data |
ASTM D 7599 : 2016 : R2024 | Standard Test Method for Determination of Diethanolamine, Triethanolamine, <emph type="ital">N</emph>-Methyldiethanolamine and <emph type="ital">N</emph >-Ethyldiethanolamine in Water by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 5994/D5994M : 2010 : R2021 | Standard Test Method for Measuring Core Thickness of Textured Geomembranes |
ASTM D 7644 : 2023 | Standard Test Method for Determination of Bromadiolone, Brodifacoum, Diphacinone and Warfarin in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS) |
ASTM E 903 : 2020 | Standard Test Method for Solar Absorptance, Reflectance, and Transmittance of Materials Using Integrating Spheres |
ASTM D 7597 : 2016 : R2024 | Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Hydrogen Dimethylamidophosphate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Water by Liquid Chromatography/Tandem Mass Spectrometry |
ASTM D 8024 : 2023 | Standard Test Method for Determination of (Tri-n-butyl)-n-tetradecylphosphonium chloride (TTPC) in Water by Multiple Reaction Monitoring Liquid Chromatography/Mass Spectrometry (LC/MS/MS) |
ASTM D 7979 : 2020 | Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances in Water, Sludge, Influent, Effluent, and Wastewater by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 7742 : 2017 : R2024 | Standard Practice for Determination of Nonylphenol Polyethoxylates (NPnEO, 3 ≤ n ≤ 18) and Octylphenol Polyethoxylates (OPnEO, 2 ≤ n ≤ 12) in Water by Single Reaction Monitoring (SRM) Liquid Chromatography/ Tandem Mass Spectrometry (LC/MS/MS) |
ASTM D 7600 : 2016 : R2024 | Standard Test Method for Determination of Aldicarb, Carbofuran, Oxamyl and Methomyl by Liquid Chromatography/Tandem Mass Spectrometry |
ASTM D 8535 : 2023 | Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances (PFAS) in Soil/Biosolid Matrices by Solvent Extraction, Filtering, and Followed by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS) |
ASTM E 2838 : 2021 | Standard Test Method for Determination of Thiodiglycol on Wipes by Solvent Extraction Followed by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS) |
ASTM E 1488 : 2023 | Standard Guide for Statistical Procedures to Use in Developing and Applying Test Methods |
ASTM C 1210 : 2021 | Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry |
ASTM C 1068 : 2021 | Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry |
ASTM E 177 : 1990 : REV A : R1996 | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
ASTM E 92 : 2023 | Standard Test Methods for Vickers Hardness and Knoop Hardness of Metallic Materials |
ASTM E 2587 : 2016 | Standard Practice for Use of Control Charts in Statistical Process Control |
ASTM E 456 : 2002 | Standard Terminology for Relating to Quality and Statistics |
ASTM D 5184 : 2012 : R2017 | Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry |
ASTM E 456 : 2013 : REV A : R2022 | Standard Terminology Relating to Quality and Statistics |
ASTM E 384 : 2022 | Standard Test Method for Microindentation Hardness of Materials |
ASTM E 456 : 2013 : REV A : R2022 : EDT 1 | Standard Terminology Relating to Quality and Statistics |
ASTM D 5184 : 2022 | Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry |
ASTM E 384 : 2011 | Standard Test Method for Knoop and Vickers Hardness of Materials |
ASTM E 456 : 2013 : REV A : R2017 : EDT 5 | Standard Terminology Relating to Quality and Statistics |
ASTM E 2282 : 2023 | Standard Guide for Defining the Test Result of a Test Method |
ASTM E 2587 : 2007 : EDT 1 | Standard Practice for Use of Control Charts in Statistical Process Control |
ASTM E 92 : 2017 | Standard Test Methods for Vickers Hardness and Knoop Hardness of Metallic Materials |
ASTM E 2587 : 2016 : R2021 : EDT 1 | Standard Practice for Use of Control Charts in Statistical Process Control |
ASTM E 456 : 2013 : REV A | Standard Terminology Relating to Quality and Statistics |
ASTM E 2282 : 2014 : R2019 | Standard Guide for Defining the Test Result of a Test Method |
ASTM E 2282 : 2014 : R2023 | Standard Guide for Defining the Test Result of a Test Method |
ASTM E 177 : 2014 | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
ASTM E 384 : 2016 | Standard Test Method for Microindentation Hardness of Materials |
ASTM E 92 : 1982 : R2003 : EDT 2 | Standard Test Method for Vickers Hardness of Metallic Materials (Withdrawn 2010) |
ASTM E 456 : 2013 : REV A : R2017 : EDT 4 | Standard Terminology Relating to Quality and Statistics |
ASTM E 456 : 2013 : REV A : R2017 : EDT 6 | Standard Terminology Relating to Quality and Statistics |
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