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ASTM E 202 : 2018

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Methods for Analysis of Ethylene Glycols and Propylene Glycols

Available format(s)

Hardcopy , PDF

Superseded date

03-06-2024

Superseded by

ASTM E 202 : 2024

Language(s)

English

Published date

15-03-2018

£63.73
Excluding VAT

Committee
D 16
DocumentType
Test Method
Pages
14
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1These test methods cover the chemical and physical analysis of the commonly available grades of ethylene glycol, diethylene glycol, triethylene glycol, propylene glycol, and dipropylene glycol. The key sections appear in the following order:

Sections

Purity of Reagents

4

Specific Gravity

6 – 8

Distillation Range

10 – 12

Acidity

14 – 16

Water

18 – 20

Iron

22 – 24

Color

26 – 28

Gas Chromatographic Analysis

30 – 32

Alternative Test Methods

Appendix X1

1.2Review the current appropriate Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid procedures, and safety precautions.

1.3In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard with the exception of foot-pound for apparatus descriptions.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D 268 : 2022 Standard Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and Material
ASTM D 2694 : 2005 : R2019 Standard Specification for Diethylene Glycol<sup>,</sup>
ASTM D 7713 : 2018 : R2023 Standard Specification for Aqueous Engine Coolant Grade Glycol (53 % by Volume Nominal)
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ASTM D 3585 : 2024 Standard Specification for ASTM Reference Fluid for Coolant Tests
ASTM D 2693 : 2022 Standard Specification for Ethylene Glycol
ASTM D 7583 : 2016 : R2023 Standard Test Method for John Deere Coolant Cavitation Test
ASTM D 4669 : 2024 Standard Test Method for Polyurethane Raw Materials: Determination of Specific Gravity of Polyols
ASTM D 5164 : 2005 : R2019 Standard Specification for Propylene Glycol and Dipropylene Glycol

ASTM E 611 : 1992 Test Methods for Low Concentrations of Diethylene Glycol in Ethylene Glycol by Gas Chromatography (Withdrawn 1996)
ASTM E 1615 : 2000 Standard Test Method for Iron in Trace Quantities Using the FerroZine Method
ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 2409 : 2004 Standard Test Method for Glycol Impurities in Mono-, Di-, Tri- and Tetraethylene Glycol (Gas Chromatographic Method)
ASTM E 2679 : 2022 Standard Test Method for Acidity in Mono-, Di-, Tri- and Tetraethylene Glycol by <brk />Non-Aqueous Potentiometric Titration
ASTM D 1078 : 1999 Standard Test Method for Distillation Range of Volatile Organic Liquids
ASTM E 1510 : 1995 : R2013 : EDT 1 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM D 4052 : 2018 : REV A Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 1209 : 2000 Standard Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
ASTM E 1064 : 2000 Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
ASTM E 29 : 2002 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 394 : 2015 Standard Test Method for Iron in Trace Quantities Using the 1,10-Phenanthroline Method
ASTM D 1613 : 1996 : R1999 Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 2409 : 2020 : REV A Standard Test Method for Glycol Impurities in Mono-, Di-, Tri- and Tetraethylene Glycol and in Mono- and Dipropylene Glycol<brk/>(Gas Chromatographic Method)
ASTM E 1615 : 2022 Standard Test Method for Determination of Trace Quantities of Iron by Visible Spectrophotometry
ASTM E 2679 : 2009 Standard Test Method for Acidity in Mono-, Di-, Tri- and Tetraethylene Glycol by<br> Non-Aqueous Potentiometric Titration
ASTM E 203 : 2023 Standard Test Method for Water Using Volumetric Karl Fischer Titration
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 1064 : 2024 Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
ASTM E 1510 : 1995 : R2021 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 5386 : 2024 Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
ASTM E 1510 : 1995 Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
ASTM D 4052 : 1996 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 5386 : 1993 : REV B : R2000 : EDT 1 Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
ASTM D 6809 : 2002 Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials
ASTM E 394 : 2000 Standard Test Method for Iron in Trace Quantities Using the 1,10-Phenanthroline Method
ASTM D 1613 : 2017 : R2023 Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM D 5386 : 2016 Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
ASTM E 1064 : 2023 Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
ASTM D 4052 : 2022 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM E 394 : 2022 Standard Test Method for Iron in Trace Quantities Using the 1,10-Phenanthroline Method
ASTM D 1613 : 2017 Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
ASTM E 203 : 2024 Standard Test Method for Water Using Volumetric Karl Fischer Titration
ASTM E 1064 : 2016 Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
ASTM E 2679 : 2009 : R2016 : EDT 1 Standard Test Method for Acidity in Mono-, Di-, Tri- and Tetraethylene Glycol by<brk />Non-Aqueous Potentiometric Titration
ASTM E 1615 : 2016 Standard Test Method for Iron in Trace Quantities Using the FerroZine Method
ASTM E 203 : 2016 Standard Test Method for Water Using Volumetric Karl Fischer Titration
ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

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