ASTM E 200 : 2016 : REDLINE
Superseded
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Practice for Preparation, Standardization, and Storage of Standard and Reagent Solutions for Chemical Analysis
Available format(s)
PDF
Superseded date
17-07-2023
Superseded by
Language(s)
English
Published date
27-07-2018
Important note : All end users must be registered with an Account prior to user licenses being assigned.CONTAINED IN VOL. 15.05, 2017 Defines procedures for the preparation, standardization, and storage of the standard volumetric solutions and reagent testing solutions commonly used in chemical analysis.
| Committee |
D 16
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| DocumentType |
Redline
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| Pages |
16
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| PublisherName |
American Society for Testing and Materials
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| Status |
Superseded
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| SupersededBy |
1.1This practice covers procedures for the preparation, standardization, and storage of the standard volumetric solutions and reagent testing solutions commonly used in chemical analysis.
1.2The information in this practice is arranged as follows:
| Sections | |
| Referenced Documents | 2 |
| Terminology | 3 |
| Significance and Use | 4 |
| Apparatus | 5 |
| Temperature effects | 6 |
| Measurements | 7 |
| Reagents | 8 |
| Concentration of solutions | 9 |
| Mixing of solutions | 10 |
| Storage of solutions | 11 |
| Preparation and standardization of solutions | 12 |
| Precision and Bias | 13 |
| Sodium hydroxide solution, 0.02 to 1.0 meq/mL (N) | 14 to 19 |
| Hydrochloric acid, 0.02 to 1.0 meq/mL (N) | 20 to 28 |
| Sulfuric acid, 0.02 to 1.0 meq/mL (N) | 29 to 33 |
| Hydrochloric acid, special 1 meq/mL (N) | 34 to 38 |
| Sulfuric acid, special 1 meq/mL (N) | 39 to 43 |
| Silver nitrate solution, 0.1 meq/mL (N) | 44 to 48 |
| Ammonium thiocyanate solution, 0.1 meq/mL (N) | 49 to 53 |
| Iodine solution, 0.1 meq/mL (N) | 54 to 58 |
| Sodium thiosulfate solution, 0.1 meq/mL (N) | 59 to 63 |
| Potassium permanganate solution, 0.1 meq/mL (N) | 64 to 68 |
| Potassium dichromate solution, 0.1 meq/mL(N) | 69 to 73 |
| Methanolic sodium hydroxide solution, 0.5 meq/mL (N) | 74 to 79 |
| Ceric sulfate solution, 0.1 meq/mL (N) | 80 to 84 |
| Acetous perchloric acid, 0.1 meq/mL (N) | 85 to 89 |
| Disodium ethylenediaminetetraacetate solution, 0.05 mol/L(M) | 90 to 94 |
| Standard ion solutions | 95 |
| Nonstandardized reagent solutions and indicator solutions | 96 |
1.3The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given throughout this practice.
| Standards | Relationship |
| UNE 55539-8:1994 | Identical |
| UNE 55539-12:1995 | Identical |
| UNE 55539-9:1994 | Identical |
| UNE 55539-10:1994 | Identical |
| UNE 55539-13:1995 | Identical |
| UNE 55539-3:1994 | Identical |
| UNE 55539-11:1994 | Identical |
| UNE 55539-4:1994 | Identical |
| UNE 55539-5:1994 | Identical |
| UNE 55539-6:1994 | Identical |
| UNE 55539-7:1994 | Identical |
| UNE 55539-2:1994 | Identical |
| ASTM D 3566 : 2003 | Standard Practice for Rubber—Determination of Bromine in the Presence of Chlorine by Oxygen Combustion |
| ASTM D 5788 : 1995 : R2005 | Standard Guide for Spiking Organics into Aqueous Samples |
| ASTM E 1910/E1910M : 2015 : REDLINE | Standard Test Method for Agricultural pH Control Agents, Measurement of pH Change and Buffering Capacity |
| ASTM E 449:2008 | Standard Test Methods for Analysis of Calcium Chloride |
| ASTM D 297 : 2015 : REDLINE | Standard Test Methods for Rubber Products—Chemical Analysis |
| ASTM D 6363 : 1998 : R2003 : EDT 1 | Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method |
| ASTM D 3546 : 2005 : R2011 | Standard Test Method for Formic Acid in Glacial Acetic Acid |
| ASTM D 2790 : 1983 | Methods of Analysis of Solvent Systems Used for Removal of Water-Formed Deposits (Withdrawn 1993) |
| ASTM D 4274 : 2016 : REDLINE | Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols |
| ASTM E 271 : 1998 | Standard Test Methods for Analysis of Aqueous Hydrofluoric Acid (Withdrawn 2003) |
| ASTM D 2192 : 2006 : R2012 | Standard Test Method for Purity of Aldehydes and Ketones (Withdrawn 2021) |
| ASTM D 3316 : 2006 | Standard Test Method for Stability of Perchloroethylene with Copper |
| ASTM D 1614 : 2009 : R2017 | Standard Test Method for Alkalinity in Acetone |
| ASTM D 4856 : 2011 | Standard Test Method for Determination of Sulfuric Acid Mist in Workplace Atmospheres Collected on Mixed Cellulose Ester Filters (Ion Chromatographic Analysis) |
| ASTM D 888 : 2012-05 | TEST METHODS FOR DISSOLVED OXYGEN IN WATER |
| ASTM E 258 : 2007 : R2015 | Standard Test Method for Total Nitrogen in Organic Materials by Modified Kjeldahl Method (Withdrawn 2019) |
| ASTM D 3316 : 2006 : R2016 | Standard Test Method for Stability of Perchloroethylene with Copper |
| ASTM E 1584 : 2017 : REDLINE | Standard Test Method for Assay of Nitric Acid |
| ASTM C 574 : 1984 : R1988 | Method for Chemical Analyisis of Magnesite and Dolomite Refractories |
| ASTM E 1147 : 1992 : R2005 | Standard Test Method for Partition Coefficient (N-Octanol/Water) Estimation by Liquid Chromatography (Withdrawn 2013) |
| ASTM D 2106 : 2007 | Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents |
| ASTM D 5810 : 1996 : R2011 | Standard Guide for Spiking into Aqueous Samples |
| ASTM D 3249 : 1995 : R2000 | Standard Practice for General Ambient Air Analyzer Procedures |
| ASTM D 4252 : 1989 : R2017 | Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates |
| ASTM D 5788 : 1995 | Standard Guide for Spiking Organics into Aqueous Samples |
| ASTM D 3089 : 1997 : R2008 | Standard Practice for Determining the A-D Dimension of Aerosol Valve Dip Tubes |
| ASTM D 2086 : 2008 | Standard Test Method for Acidity in Vinyl Acetate and Acetaldehyde |
| ASTM D 6363 : 1998 : R2013 | Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method |
| ASTM D 1417 : 2016 : REDLINE | Standard Test Methods for Rubber Latices—Synthetic |
| ASTM D 2086 : 2008 : R2012 | Standard Test Method for Acidity in Vinyl Acetate and Acetaldehyde (Withdrawn 2021) |
| ASTM D 1942 : 1980 | Method of Test for Morpholine in Water |
| ASTM D 5788 : 1995 : R2017 | Standard Guide for Spiking Organics into Aqueous Samples |
| ASTM E 1547 : 2009 | Standard Terminology Relating to Industrial and Specialty Chemicals |
| ASTM D 5916 : 1996 : R2002 | Standard Test Method for Detection and Enumeration of <i>Clostridium perfringens</i> from Water and Extracted Sediments by Membrane Filtration (MF) (Withdrawn 2011) |
| ASTM D 6328 : 2012-11 | GUIDE FOR QUALITY ASSURANCE PROTOCOLS FOR CHEMICAL ANALYSIS OF ATMOSPHERIC WET DEPOSITION |
| ASTM D 3316 : 2006 : R2011 | Standard Test Method for Stability of Perchloroethylene with Copper |
| ASTM D 1141 : 1998 : R2013 | Standard Practice for the Preparation of Substitute Ocean Water |
| ASTM D 2912 : 1976 : R1983 | Test Method for Oxidant Content of the Atmosphere (Neutral KI) (Withdrawn 1990) |
| ASTM D 3228 : 2008 : R2014 | Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method |
| MIL H 6083 : E | HYDRAULIC FLUID, PETROLEUM BASE, FOR PRESERVATION AND OPERATION |
| ASTM D 4252 : 1989 : R1995 : EDT 1 | Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates |
| ASTM D 5788 : 1995 : R2001 | Standard Guide for Spiking Organics into Aqueous Samples |
| ASTM E 1788 : 2016 : REDLINE | Standard Test Method for Acidity in Acrylonitrile |
| ASTM D 512 : 2012 | Standard Test Methods for Chloride Ion In Water (Withdrawn 2021) |
| MIL-D-22346 Revision B:1973 | DI-NORMAL-PROPYL ADIPATE (DNPA) |
| ASTM E 442 : 1991 | Test Method for Chlorine, Bromine, or Iodine in Organic Compounds by Oxygen Flask Combustion (Withdrawn 1997) |
| ASTM D 3566 : 2003 : R2009 | Standard Practice for Rubber—Determination of Bromine in the Presence of Chlorine by Oxygen Combustion |
| ASTM D 5788 : 1995 : R2011 | Standard Guide for Spiking Organics into Aqueous Samples |
| ASTM D 4415 : 2005 | Standard Test Methods for Determination of Dimer in Acrylic Acid (Withdrawn 2011) |
| ASTM D 6363 : 1998 | Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method |
| ASTM D 4224 : 1989 | Test Method for Anionic Detergent by Para-Toluidine Hydrochloride (Withdrawn 1995) |
| ASTM D 3566 : 2003 : R2014 | Standard Practice for Rubber—Determination of Bromine in the Presence of Chlorine by Oxygen Combustion |
| ASTM D 2379 : 2009 | Standard Test Method for Acidity of Formaldehyde Solutions |
| ASTM D 6303 : 1998 | Standard Test Method for Formaldehyde in Water (Withdrawn 2007) |
| ASTM D 1387 : 1989 : R2002 | Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes |
| ASTM D 6470 : 1999 : R2015 | Standard Test Method for Salt in Crude Oils (Potentiometric Method) |
| ASTM D 3634 : 1999 : EDT 1 | Standard Test Method for Trace Chloride Ion in Engine Coolants |
| ASTM D 5810 : 1996 : R2006 | Standard Guide for Spiking into Aqueous Samples |
| ASTM D 3634 : 1999 : R2005 | Standard Test Method for Trace Chloride Ion in Engine Coolants |
| ASTM D 5810 : 1996 : R2015 | Standard Guide for Spiking into Aqueous Samples |
| ASTM E 257 : 1998 | Standard Test Method for Sulfur in Organic Compounds by Sodium Peroxide Bomb Ignition |
| ASTM D 345 : 2002 | Side bearings of the freight wagon bogies. General specifications |
| ASTM D 1387 : 1989 : R2007 | Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes |
| ASTM D 2942 : 2002 | Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods) |
| ASTM E 1615 : 2016 : REDLINE | Standard Test Method for Iron in Trace Quantities Using the FerroZine Method |
| ASTM E 223 : 2016 : REDLINE | Standard Test Methods for Analysis of Sulfuric Acid |
| ASTM D 2382 : 1988 | Test Method for Heat of Combustion of Hydrocarbon Fuels by Bomb Calorimeter (High-Precision Method) (Withdrawn 1994) |
| ASTM D 4266 : 2017 : REDLINE | Standard Test Methods for Precoat Capacity of Powdered Ion-Exchange Resins |
| ASTM E 1910 : 2004 | Test Method for Agricultural pH Control Agents |
| ASTM D 240 : 2017 : REDLINE | Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter |
| ASTM E 441 : 1990 | Test Method for Vinyl Unsaturation in Organic Compounds with Mercuric Acetate (Withdrawn 1996) |
| ASTM D 2106 : 2007 : R2017 | Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents |
| ASTM D 1067 : 2016 : REDLINE | Standard Test Methods for Acidity or Alkalinity of Water |
| ASTM D 1387 : 1989 : R2012 | Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes |
| ASTM D 2942 : 2002 : R2013 | Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods) |
| ASTM E 567 : 1991 | Test Method for Tertiary Hydroxyl Groups with Hydrogen Bromide (Withdrawn 1996) |
| ASTM D 3249 : 1995 : R2005 | Standard Practice for General Ambient Air Analyzer Procedures |
| ASTM D 3634 : 1999 : R2015 | Standard Test Method for Trace Chloride Ion in Engine Coolants |
| ASTM D 7389 : 2007 | Standard Test Method for Acid Number (Empirical) of Maleic Anhydride (MAH) Grafted Waxes |
| ASTM E 2677 : 2014 | Standard Test Method for Determining Limits of Detection in Explosive Trace Detectors |
| ASTM D 2195 : 2005 | Standard Test Methods for Pentaerythritol (Withdrawn 2011) |
| ASTM E 301 : 1994 | Standard Test Method for Total Acidity of Organic Acids (Withdrawn 2001) |
| ASTM D 5810 : 1996 | Standard Guide for Spiking into Aqueous Samples |
| ASTM D 7795 : 2015 : REDLINE | Standard Test Method for Acidity in Ethanol and Ethanol Blends by Titration |
| ASTM E 449 : 2008 : R2013 | Standard Test Methods for Analysis of Calcium Chloride |
| ASTM E 358 : 1995 | Test Methods for Analysis of Phosphoric Acid (Withdrawn 2000) |
| ASTM D 3634 : 1999 : R2009 | Standard Test Method for Trace Chloride Ion in Engine Coolants |
| AWWA B403 : 2016 | ALUMINUM SULFATE - LIQUID, GROUND, OR LUMP |
| ASTM D 2106 : 2007 : R2012 | Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents |
| ASTM E 819 : 1998 | Standard Test Method for Trace Amounts of Arsenic in Organic Industrial Chemicals (Withdrawn 2003) |
| ASTM E 234 : 1998 | Standard Test Method for Total Bromine Number of Unsaturated Aliphatic Chemicals |
| ASTM D 3546 : 2005 | Standard Test Method for Formic Acid in Glacial Acetic Acid |
| ASTM D 3546 : 2005 : R2019 | Standard Test Method for Formic Acid in Glacial Acetic Acid |
| ASTM D 1141 : 1998 : R2008 | Standard Practice for the Preparation of Substitute Ocean Water |
| ASTM D 3228 : 2008 | Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method |
| ASTM D 6470 : 1999 : R2010 | Standard Test Method for Salt in Crude Oils (Potentiometric Method) |
| ASTM D 1141 : 1998 : EDT 1 | Standard Practice for the Preparation of Substitute Ocean Water |
| ASTM E 1228 : 2017 : REDLINE | Standard Test Method for Assay of Peroxy Esters—Catalyzed Iodometric Procedure |
| ASTM D 513 : 2016 : REDLINE | Standard Test Methods for Total and Dissolved Carbon Dioxide in Water |
| ASTM D 1614 : 2009 | Standard Test Method for Alkalinity in Acetone |
| ASTM E 1547 : 2009 : R2017 | Standard Terminology Relating to Industrial and Specialty Chemicals |
| ASTM D 7389 : 2007 : R2012 | Standard Test Method for Acid Number (Empirical) of Maleic Anhydride (MAH) Grafted Waxes |
| ASTM D 2942 : 2002 : R2008 | Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods) |
| ASTM D 5318 : 1997 | Standard Test Method for Hydrolyzable Chloride in Peroxy Esters and Peroxy Dicarbonates (Withdrawn 2004) |
| ASTM D 3249 : 1995 : R2011 | Standard Practice for General Ambient Air Analyzer Procedures |
| ASTM E 394 : 2015 : REDLINE | Standard Test Method for Iron in Trace Quantities Using the 1,10-Phenanthroline Method |
| ASTM E 534 : 2013-11 | TEST METHODS FOR CHEMICAL ANALYSIS OF SODIUM CHLORIDE |
| ASTM D 4252 : 1989 : R2003 | Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates |
| ASTM D 4252 : 1989 : R2009 | Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates |
| ASTM E 224 : 2016 : REDLINE | Standard Test Methods for Analysis of Hydrochloric Acid |
| GOST 849:2018 | Primary nickel. SpecificationsE |
| ASTM D 2192 : 2006 | Standard Test Method for Purity of Aldehydes and Ketones |
| ASTM D 6363 : 1998 : R2009 : EDT 1 | Standard Test Method for Determination of Hydrogen Peroxide and Combined Organic Peroxides in Atmospheric Water Samples by Peroxidase Enzyme Fluorescence Method |
| ASTM D 4249 : 1983 : R1998 | Standard Test Method for Enumeration of <I>Candida albicans</I> in Water |
| ASTM E 222 : 2017 : REDLINE | Standard Test Methods for Hydroxyl Groups Using Acetic Anhydride Acetylation |
| ASTM E 326 : 1996 | Test Method for Hydroxyl Groups by Phthalic Anhydride Esterification (Withdrawn 2001) |
| ASTM D 4249 : 1983 : R2005 | Standard Test Method for Enumeration of <I>Candida albicans</I> in Water (Withdrawn 2013) |
| ASTM E 335 : 1996 | Standard Test Method for Hydroxyl Groups by Pyromellitic Dianhydride Esterification (Withdrawn 2003) |
| ASTM E 233 : 1990 | Test Method for Assay of N-Butyllithium Solutions (Withdrawn 1996) |
| ASTM D 5810 : 1996 : R2001 | Standard Guide for Spiking into Aqueous Samples |
| ASTM E 1147 : 1992 : R1997 | Standard Test Method for Partition Coefficient (N-Octanol/Water) Estimation by Liquid Chromatography |
| ASTM D 1613 : 2017 : REDLINE | Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products |
| ASTM C 500/C500M : 2007 : R2011 : EDT 1 | Standard Test Methods for Asbestos-Cement Pipe |
| ASTM D 3634 : 1999 : R2005 : EDT 1 | Standard Test Method for Trace Chloride Ion in Engine Coolants |
| ASTM E 778 : 2015 : REDLINE | Standard Test Methods for Nitrogen in Refuse-Derived Fuel Analysis Samples |
| ASTM D 1141 : 1998 : R2003 | Standard Practice for the Preparation of Substitute Ocean Water |
| ASTM E 258 : 2007 | Standard Test Method for Total Nitrogen in Organic Materials by Modified Kjeldahl Method |
| ASTM D 5058 : 2012 : REDLINE | Standard Practices for Compatibility of Screening Analysis of Waste |
| ASTM E 359 : 2017 : REDLINE | Standard Test Methods for Analysis of Soda Ash (Sodium Carbonate) |
| ASTM D 1387 : 1989 : R1995 : EDT 1 | Standard Test Method for Saponification Number (Empirical) of Synthetic and Natural Waxes |
| ASTM D 1386 : 2015 : REDLINE | Standard Test Method for Acid Number (Empirical) of Synthetic and Natural Waxes |
| ASTM D 6511/D6511M : 2011-07 | TEST METHODS FOR SOLVENT BEARING BITUMINOUS COMPOUNDS |
| ASTM D 6470 : 1999 | Standard Test Method for Salt in Crude Oils (Potentiometric Method) |
| ASTM D 5916 : 1996 | Standard Test Method for Detection and Enumeration of <i>Clostridium perfringens</i> from Water and Extracted Sediments by Membrane Filtration (MF) |
| ASTM C 25 : 2017 : REDLINE | TEST METHODS FOR CHEMICAL ANALYSIS OF LIMESTONE, QUICKLIME, AND HYDRATED LIME |
| ASTM D 2379 : 2009 : R2017 | Standard Test Method for Acidity of Formaldehyde Solutions |
| ASTM D 3875 : 2015 : REDLINE | Standard Test Method for Alkalinity in Brackish Water, Seawater, and Brines |
| ASTM D 2106 : 2007 : EDT 1 | Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents |
| ASTM D 6470 : 1999 : R2004 | Standard Test Method for Salt in Crude Oils (Potentiometric Method) |
| ASTM D 4856 : 2011 : R2016 | Standard Test Method for Determination of Sulfuric Acid Mist in Workplace Atmospheres Collected on Mixed Cellulose Ester Filters (Ion Chromatographic Analysis) |
| ASTM E 50 : 2017 : REDLINE | Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials |
| ASTM E 180 : 2003 | Standard Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Specialty Chemicals (Withdrawn 2009) |
| ASTM E 203 : 2016 : REDLINE | Standard Test Method for Water Using Volumetric Karl Fischer Titration |
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