ASTM D 7578 : 2020
Current
The latest, up-to-date edition.
Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
Hardcopy , PDF
English
01-05-2020
Committee |
D 02
|
DocumentType |
Guide
|
Pages |
13
|
PublisherName |
American Society for Testing and Materials
|
Status |
Current
|
Supersedes |
1.1This guide covers different ways by which the test methods used for elemental analysis of petroleum product and lubricant samples are calibrated before the sample analysis.
1.2Uniform practice for test method calibration is beneficial in standardizing the procedures, and obtaining consistent results across different laboratories.
1.3This guide includes only the basic steps for generally encountered instrument types. Anything out of the ordinary may require special procedures. See individual test methods for instructions to handle such situations.
1.4This guide is not a substitute for a thorough understanding of the actual test method to be used, caveats it contains, and additional instrument preparation that may be required.
1.5The user should not expand the scope of the test methods to materials or concentrations outside the scope of the test methods being used.
1.6This guide should also be applicable to sample preparation of non-petroleum based bio-fuels for elemental analysis. Work is underway on these aspects in Subcommittee D02.03. As more information becomes available, it will be added to this standard.
1.7The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.8This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.9This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D 8056 : 2018 | Standard Guide for Elemental Analysis of Crude Oil |
ASTM D 7961 : 2017 | Standard Practice for Calibrating U-tube Density Cells over Large Ranges of Temperature and Pressure |
ASTM D 5863 : 2022 | Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry |
ASTM D 129 : 2018 | Standard Test Method for Sulfur in Petroleum Products (General High Pressure Decomposition Device Method) (Withdrawn 2023) |
ASTM D 5291 : 2021 | Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants |
ASTM D 4929 : 2024 | Standard Test Method for Determination of Organic Chloride Content in Crude Oil |
ASTM D 6792 : 2021 : REV A | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 3341 : 2016 | Standard Test Method for Lead in Gasoline—Iodine Monochloride Method (Withdrawn 2022) |
ASTM D 874 : 2013 : REV A : R2018 | Standard Test Method for Sulfated Ash from Lubricating Oils and Additives |
ASTM D 6667 : 2021 | Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence |
ASTM D 7328 : 2022 | Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection |
ASTM D 5762 : 2024 | Standard Test Method for Nitrogen in Liquid Hydrocarbons, Petroleum and Petroleum Products by Boat-Inlet Chemiluminescence |
ASTM D 3120 : 1996 | Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry |
ASTM D 7757 : 2022 | Standard Test Method for Silicon in Gasoline and Related Products by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry |
ASTM D 5056 : 2017 | Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption |
ASTM D 7111 : 2016 | Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
ASTM D 7303 : 2017 | Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry |
ASTM D 5800 : 2018 : REV A | Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method |
ASTM D 7220 : 2012 : R2017 | Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry |
ASTM D 6728 : 2016 : R2021 | Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry |
ASTM D 1018 : 2011 : R2016 | Standard Test Method for Hydrogen In Petroleum Fractions (Withdrawn 2021) |
ASTM D 482 : 2013 | Standard Test Method for Ash from Petroleum Products |
ASTM D 892 : 2018 | Standard Test Method for Foaming Characteristics of Lubricating Oils |
ASTM D 5184 : 2012 : R2017 | Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry |
ASTM D 4628 : 2023 | Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry |
ASTM D 4929 : 2019 : REV A | Standard Test Method for Determination of Organic Chloride Content in Crude Oil |
ASTM D 3605 : 2022 | Standard Test Method for Trace Metals in Gas Turbine Fuels by Atomic Absorption and Flame Emission Spectroscopy |
ASTM D 808 : 2016 | Standard Test Method for Chlorine in New and Used Petroleum Products (High Pressure Decomposition Device Method) (Withdrawn 2021) |
ASTM D 4929 : 2022 | Standard Test Method for Determination of Organic Chloride Content in Crude Oil |
ASTM D 5184 : 2022 | Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry |
ASTM D 3230 : 2013 : R2018 | Standard Test Method for Salts in Crude Oil (Electrometric Method) |
ASTM D 7041 : 2016 : R2021 | Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbons and Hydrocarbon-Oxygenate Blends by Gas Chromatography with Flame Photometric Detection |
ASTM D 6443 : 2024 | Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure) |
ASTM D 3605 : 2017 | Standard Test Method for Trace Metals in Gas Turbine Fuels by Atomic Absorption and Flame Emission Spectroscopy |
ASTM D 5622 : 2017 | Standard Test Methods for Determination of Total Oxygen in Gasoline and Methanol Fuels by Reductive Pyrolysis |
ASTM D 445 : 2021 : EDT 2 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
ASTM D 3348 : 2012 : R2017 | Standard Test Method for Rapid Field Test for Trace Lead in Unleaded Gasoline (Colorimetric Method) (Withdrawn 2022) |
ASTM D 7328 : 2023 | Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection |
ASTM D 3231 : 2024 | Standard Test Method for Phosphorus in Gasoline |
ASTM D 6792 : 2021 : REV B | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 6792 : 2023 : REV C | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 5800 : 2019 | Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method |
ASTM D 445 : 2017 : REV A | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
ASTM D 6334 : 2012 : R2017 : EDT 1 | Standard Test Method for Sulfur in Gasoline by Wavelength Dispersive X-Ray Fluorescence (Withdrawn 2022) |
ASTM D 4628 : 2016 | Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry |
ASTM D 1318 : 2023 | Standard Test Method for Sodium in Residual Fuel Oil (Flame Photometric Method) |
ASTM D 7319 : 2022 | Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography |
ASTM D 5291 : 2016 | Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants |
ASTM D 3231 : 2018 | Standard Test Method for Phosphorus in Gasoline |
ASTM D 3831 : 2022 | Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy |
ASTM D 445 : 1988 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity) |
ASTM D 6792 : 2023 : REV B | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 1552 : 2023 | Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD) |
ASTM D 5863 : 2000 : REV A : R2016 | Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry |
ASTM D 3228 : 2022 | Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method |
ASTM D 5059 : 2021 | Standard Test Methods for Lead and Manganese in Gasoline by X-Ray Fluorescence Spectroscopy |
ASTM D 4294 : 2008 | Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry |
ASTM E 77 : 2014 : EDT 1 | Standard Test Method for Inspection and Verification of Thermometers |
ASTM D 6792 : 2020 | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 6792 : 2021 | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 6728 : 2016 | Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry |
ASTM D 1318 : 2016 | Standard Test Method for Sodium in Residual Fuel Oil (Flame Photometric Method) |
ASTM D 5622 : 2024 | Standard Test Methods for Determination of Total Oxygen in Gasoline and Methanol Fuels by Reductive Pyrolysis |
ASTM D 7212 : 2013 : R2018 | Standard Test Method for Low Sulfur in Automotive Fuels by Energy-Dispersive X-ray Fluorescence Spectrometry Using a Low-Background Proportional Counter (Withdrawn 2024) |
ASTM D 2622 : 2024 | Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry |
ASTM D 1091 : 2011 : R2016 | Standard Test Methods for Phosphorus in Lubricating Oils and Additives (Withdrawn 2021) |
ASTM D 6481 : 2014 : R2019 | Standard Test Method for Determination of Phosphorus, Sulfur, Calcium, and Zinc in Lubrication Oils by Energy Dispersive X-ray Fluorescence Spectroscopy |
ASTM D 5056 : 1996 | Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption |
ASTM D 7319 : 2017 | Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography |
ASTM D 1552 : 2016 : EDT 1 | Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD) |
ASTM D 7318 : 2019 | Standard Test Method for Existent Inorganic Sulfate in Ethanol by Potentiometric Titration |
ASTM D 5600 : 2022 | Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
ASTM D 3228 : 2020 | Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method |
ASTM D 874 : 2023 | Standard Test Method for Sulfated Ash from Lubricating Oils and Additives |
ASTM E 319 : 1985 : R2014 | Standard Practice for the Evaluation of Single-Pan Mechanical Balances (Withdrawn 2021) |
ASTM D 445 : 2019 : REV A | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
ASTM D 6481 : 2024 | Standard Test Method for Determination of Phosphorus, Sulfur, Calcium, and Zinc in Lubrication Oils by Energy Dispersive X-ray Fluorescence Spectroscopy |
ASTM D 6792 : 2021 : REV C | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 5059 : 2020 | Standard Test Methods for Lead and Manganese in Gasoline by X-Ray Spectroscopy |
ASTM D 8127 : 2017 : EDT 1 | Standard Test Method for Coupled Particulate and Elemental Analysis using X-ray Fluorescence (XRF) for In-Service Lubricants |
ASTM D 4307 : 2017 | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
ASTM D 5762 : 1998 | Standard Test Method for Nitrogen in Petroleum and Petroleum Products by Boat-Inlet Chemiluminescence |
ASTM D 6667 : 2014 : R2019 | Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence |
ASTM D 6595 : 2022 | Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry |
ASTM D 6792 : 2023 : REV A | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 4294 : 2016 : EDT 1 | Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry |
ASTM D 5453 : 2016 : EDT 1 | Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence |
ASTM D 8150 : 2022 | Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography |
ASTM D 7691 : 2016 | Standard Test Method for Multielement Analysis of Crude Oils Using Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
ASTM D 8127 : 2023 | Standard Test Method for Coupled Particulate and Elemental Analysis using X-ray Fluorescence (XRF) for In-Service Lubricants |
ASTM D 5600 : 2017 | Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
ASTM D 7220 : 2022 | Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry |
ASTM D 5800 : 2021 | Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method |
ASTM D 445 : 2019 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
ASTM D 4629 : 2017 | Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection |
ASTM D 4307 : 2017 : R2021 | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
ASTM D 3246 : 2015 | Standard Test Method for Sulfur in Petroleum Gas by Oxidative Microcoulometry (Withdrawn 2024) |
ASTM D 4294 : 2021 | Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry |
ASTM D 5291 : 2001 | Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants |
ASTM D 445 : 2001 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity) |
ASTM D 2622 : 2021 | Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry |
ASTM D 445 : 2024 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
ASTM D 445 : 2021 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
ASTM D 6792 : 2022 | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 5453 : 2019 : REV A | Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence |
ASTM D 7751 : 2016 | Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis |
ASTM D 6595 : 2017 | Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry |
ASTM D 892 : 2023 | Standard Test Method for Foaming Characteristics of Lubricating Oils |
ASTM D 6443 : 2014 : R2019 : EDT 1 | Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure) |
ASTM D 7328 : 2017 | Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection |
ASTM D 7455 : 2024 | Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis |
ASTM D 7041 : 2016 | Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbons and Hydrocarbon-Oxygenate Blends by Gas Chromatography with Flame Photometric Detection |
ASTM D 5800 : 2020 | Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method |
ASTM D 892 : 2018 : EDT 1 | Standard Test Method for Foaming Characteristics of Lubricating Oils |
ASTM D 3237 : 2017 | Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy |
ASTM D 5453 : 2019 | Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence |
ASTM D 3831 : 1998 | Standard Test Method for Manganese In Gasoline By Atomic Absorption Spectroscopy |
ASTM D 445 : 2018 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
ASTM D 8150 : 2017 | Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography |
ASTM D 7757 : 2017 | Standard Test Method for Silicon in Gasoline and Related Products by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry |
ASTM D 3237 : 1997 | Standard Test Method for Lead In Gasoline By Atomic Absorption Spectroscopy |
ASTM D 4629 : 2024 | Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection |
ASTM D 6792 : 2023 | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 445 : 2021 : EDT 1 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
ASTM D 1552 : 2016 : R2021 | Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD) |
ASTM D 7111 : 2016 : R2021 | Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
ASTM D 3831 : 2012 : R2017 | Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy |
ASTM D 7303 : 2023 | Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry |
ASTM D 7455 : 2019 | Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis |
ASTM D 5056 : 2022 | Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption |
ASTM E 77 : 1998 | Standard Test Method for Inspection and Verification of Thermometers |
ASTM D 6792 : 2022 : REV A | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
ASTM D 3237 : 2022 | Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy |
ASTM D 7751 : 2016 : R2021 | Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis |
ASTM D 5453 : 2024 | Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence |
ASTM E 77 : 2014 : R2021 | Standard Test Method for Inspection and Verification of Thermometers |
ASTM D 5762 : 2018 : REV A | Standard Test Method for Nitrogen in Liquid Hydrocarbons, Petroleum and Petroleum Products by Boat-Inlet Chemiluminescence |
ASTM D 7691 : 2023 | Standard Test Method for Multielement Analysis of Crude Oils Using Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) |
ASTM D 445 : 2023 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
ASTM D 2622 : 2016 | Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry |
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