ASTM D 7528 : 2017 : REV A
Superseded
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
Standard Test Method for Bench Oxidation of Engine Oils by ROBO Apparatus
Available format(s)
Hardcopy , PDF
Superseded date
11-01-2021
Superseded by
Language(s)
English
Published date
17-10-2017
Important note : All end users must be registered with an Account prior to user licenses being assigned.| Committee |
D 02
|
| DocumentType |
Test Method
|
| Pages |
23
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
1.1This test method describes a bench procedure to simulate the oil aging encountered in Test Method D7320, the Sequence IIIG engine test method. These aged oils are then tested for kinematic viscosity and for low-temperature pumpability properties as described in the Sequence IIIGA engine test, Appendix X1 of Test Method D7320.
1.2Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2.1Exceptions—There are no SI equivalents for some apparatus in Section 6, and there are some figures where inch units are to be regarded as standard.
1.3This test method is arranged as follows:
| Section | |
| Scope | 1 |
| Reference Documents | 2 |
| Terminology | 3 |
| Summary of Test Method | 4 |
| Significance and Use | 5 |
| Apparatus | 6 |
| Reagents and Materials | 7 |
| Hazards | 8 |
| New and Existing Test Stand Calibration | 9 |
| Procedure | 10 |
| Cleaning | 11 |
| Calculations and Determination of Test Results | 12 |
| Report | 13 |
| Precision and Bias | 14 |
| Keywords | 15 |
| Annexes | |
| ASTM Test Monitoring Center: Organization | Annex A1 |
| ASTM Test Monitoring Center: Calibration Procedures | Annex A2 |
| ASTM Test Monitoring Center: Maintenance Activities | Annex A3 |
| ASTM Test Monitoring Center: Related Information | Annex A4 |
| Reaction Vessel | Annex A5 |
| Reaction Vessel Head | Annex A6 |
| Reaction Vessel-to-Head Seal | Annex A7 |
| Agitator Turbine Blade | Annex A8 |
| Agitator Packing Gland | Annex A9 |
| Nitrogen Dioxide Graduated Tube | Annex A10 |
| Vacuum System Plumbing | Annex A11 |
| Vacuum Trap Condensers | Annex A12 |
| Setting the Vacuum Control Valve | Annex A13 |
| Appendixes | |
| Sample Preparation and Addition | Appendix X1 |
| Charging the Liquid Nitrogen Dioxide | Appendix X2 |
| Nitrogen Dioxide Precision Needle Valve | Appendix X3 |
| Example of an Assembled ROBO Apparatus | Appendix X4 |
| Information Package to Aid Setting Up a New Robo Apparatus | Appendix X5 |
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Sections 7 and 8.
1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| ASTM D 4175 : 2020 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 7320 : 2011 | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4175 : 2014 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2003 : REV A | Standard Specification for Performance of Engine Oils |
| ASTM D 4175 : 2009 : REV A : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4684 : 2002 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 4175 : 2008 : REV B : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2006 | Standard Specification for Performance of Engine Oils |
| ASTM D 4175 : 2005 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2011 : REV C | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 4175 : 2005 : EDT 2 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2001 | Standard Specification for Performance of Engine Oils |
| ASTM D 4175 : 2015 : REV C | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2017 : REV A : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4485 : 2003 | Standard Specification for Performance of Engine Oils |
| ASTM D 4485 : 2008 | Standard Specification for Performance of Engine Oils |
| ASTM D 4485 : 2015 | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 4485 : 2005 : REV A | Standard Specification for Performance of Engine Oils |
| ASTM D 4684 : 2008 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 4175 : 2008 : REV A | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2020 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4684 : 2020 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 4175 : 2017 : REV B | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4175 : 2009 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2011 : REV A | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 5293 : 2010 : EDT 1 | Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between <span class='unicode'>–</span>5 and <span class='unicode'>–</span>35<span class='unicode'>°</span>C Using Cold-Cranking Simulator |
| ASTM D 7320 : 2014 | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4485 : 2018 | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 5293 : 2020 | Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator |
| ASTM D 4175 : 2009 : REV A : EDT 4 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2009 : REV A : EDT 3 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2011 : REV B | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 4684 : 2007 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 4485 : 2016 | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 4175 : 2018 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4485 : 2007 | Standard Specification for Performance of Engine Oils |
| ASTM D 4485 : 2010 | Standard Specification for Performance of Engine Oils |
| ASTM D 4485 : 2001 : REV A | Standard Specification for Performance of Engine Oils |
| ASTM D 4175 : 2001 : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4684 : 2017 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 4175 : 2001 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2005 : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2002 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 7320 : 2015 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4485 : 2004 | Standard Specification for Performance of Engine Oils |
| ASTM D 5293 : 2014 | Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –5°C and –35°C Using Cold-Cranking Simulator |
| ASTM D 7320 : 2016 | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4684 : 2012 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 7320 : 2015 | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4175 : 2015 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2000 | Standard Specification for Performance of Engine Oils |
| ASTM D 4175 : 2002 : REV A : EDT 2 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 5293 : 2008 : EDT 1 | Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator |
| ASTM D 4485 : 2015 : REV A | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 7320 : 2007 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 5293 : 2017 : REV A | Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator |
| ASTM D 4684 : 2014 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 4175 : 2009 : REV A : EDT 5 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2016 : REV C | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4175 : 2015 : REV B | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 7320 : 2011 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 7320 : 2006 | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 7320 : 2017 | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4175 : 2015 : REV A | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2006 : REV A | Standard Specification for Performance of Engine Oils |
| ASTM D 4684 : 2002 : REV A | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 4175 : 2009 : REV A | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2016 : REV B | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4175 : 2002 : REV A : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2008 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 5293 : 2009 | Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator |
| ASTM D 4175 : 2002 : REV A | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2000 : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2016 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4684 : 2007 : EDT 1 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 4684 : 1999 : EDT 1 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 4175 : 2019 : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 7320 : 2009 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4485 : 2018 : REV A | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 7320 : 2013 | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 5293 : 1999 : REV A : EDT 1 | Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35<sup>o</sup>C Using the Cold-Cranking Simulator |
| ASTM D 4485 : 2005 | Standard Specification for Performance of Engine Oils |
| ASTM D 4684 : 2017 : REV A | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 7320 : 2008 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 5293 : 2017 : EDT 1 | Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator |
| ASTM D 4485 : 2014 | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 4485 : 2002 | Standard Specification for Performance of Engine Oils |
| ASTM D 4175 : 2017 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 7320 : 2018 | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4485 : 2005 : EDT 1 | Standard Specification for Performance of Engine Oils |
| ASTM D 4175 : 2009 : REV A : EDT 2 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 7320 : 2017 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4175 : 2018 : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4175 : 2016 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 5293 : 2004 | Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator |
| ASTM D 5293 : 2015 | Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator |
| ASTM D 4684 : 2018 | Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature |
| ASTM D 5293 : 2008 | Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator |
| ASTM D 7320 : 2012 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4175 : 2017 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 7320 : 2010 : REV B | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 5293 : 2010 | Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator |
| ASTM D 7320 : 2016 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 7320 : 2010 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine |
| ASTM D 4175 : 2019 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4485 : 2009 | Standard Specification for Performance of Engine Oils |
| ASTM D 4485 : 2019 | Standard Specification for Performance of Active API Service Category Engine Oils |
| ASTM D 4175 : 2015 : REV B : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2010 : REV A | Standard Specification for Performance of Engine Oils |
| ASTM D 5293 : 2017 | Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator |
| ASTM D 5293 : 2002 | Standard Test Method for Apparent Viscosity of Engine Oils Between -5 and -35°C Using the Cold-Cranking Simulator |
| ASTM D 4485 : 2011 | Standard Specification for Performance of Engine Oils |
| ASTM D 4175 : 2008 : REV B | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4485 : 2007 : REV A | Standard Specification for Performance of Engine Oils |
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