ASTM D 6300 : 2024
Current
Current
The latest, up-to-date edition.
Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
Available format(s)
Hardcopy , PDF
Language(s)
English
Published date
14-03-2024
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D 02
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| DocumentType |
Standard Practice
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| Pages |
42
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| PublisherName |
American Society for Testing and Materials
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| Status |
Current
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| Supersedes |
1.1This practice covers the necessary preparations and planning for the conduct of interlaboratory programs for the development of estimates of precision (determinability, repeatability, and reproducibility) and of bias (absolute and relative), and further presents the standard phraseology for incorporating such information into standard test methods.
1.2This practice is generally limited to homogeneous petroleum products, liquid fuels, and lubricants with which serious sampling problems (such as heterogeneity or instability) do not normally arise.
1.3This practice may not be suitable for products with sampling problems as described in 1.2, solid or semisolid products such as petroleum coke, industrial pitches, paraffin waxes, greases, or solid lubricants when the heterogeneous properties of the substances create sampling problems. In such instances, consult a trained statistician.
1.4This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| ASTM D 7423 : 2023 | Standard Test Method for Determination of Oxygenates in C2, C3, C4, and C5 Hydrocarbon Matrices by Gas Chromatography and Flame Ionization Detection |
| ASTM D 7501 : 2022 | Standard Test Method for Determination of Fuel Filter Blocking Potential of Biodiesel Fuel Blendstock (B100) by Cold Soak Filtration Test (CSFT) |
| ASTM D 8290 : 2022 | Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Aviation Turbine Fuel using Mid-Infrared Laser Spectroscopy |
| ASTM D 7687 : 2023 | Standard Test Method for Measurement of Cellular Adenosine Triphosphate in Fuel and Fuel-associated Water With Sample Concentration by Filtration |
| ASTM D 2887 : 2023 | Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography |
| ASTM D 1552 : 2023 | Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD) |
| ASTM D 2532 : 2022 | Standard Test Method for Viscosity and Viscosity Change After Standing at Low Temperature of Aircraft Turbine Lubricants |
| ASTM D 7619 : 2022 | Standard Test Method for Sizing and Counting Particles in Light and Middle Distillate Fuels, by Automatic Particle Counter |
| ASTM D 7212 : 2013 : R2018 | Standard Test Method for Low Sulfur in Automotive Fuels by Energy-Dispersive X-ray Fluorescence Spectrometry Using a Low-Background Proportional Counter (Withdrawn 2024) |
| ASTM D 613 : 2024 | Standard Test Method for Cetane Number of Diesel Fuel Oil |
| ASTM D 7039 : 2015 : REV A : R2020 | Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry |
| ASTM D 7798 : 2020 | Standard Test Method for Boiling Range Distribution of Petroleum Distillates with Final Boiling Points up to 538 °C by Ultra Fast Gas Chromatography (UF GC) |
| ASTM E 3146 : 2020 | Standard Test Method for Determination of Carbonyls in Pyrolysis Bio-Oils by Potentiometric Titration |
| ASTM D 8183 : 2022 | Standard Test Method for Determination of Indicated Cetane Number (ICN) of Diesel Fuel Oils using a Constant Volume Combustion Chamber—Reference Fuels Calibration Method |
| ASTM D 2425 : 2023 | Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry |
| ASTM D 8267 : 2019 : REV A | Standard Test Method for Determination of Total Aromatic, Monoaromatic and Diaromatic Content of Aviation Turbine Fuels Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV) |
| ASTM D 3831 : 2022 | Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy |
| ASTM D 2500 : 2023 | Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels |
| ASTM D 7236 : 2016 : REV A : R2021 | Standard Test Method for Flash Point by Small Scale Closed Cup Tester (Ramp Method) |
| ASTM D 6259 : 2023 | Standard Practice for Determination of a Pooled Limit of Quantitation for a Test Method |
| ASTM D 7918 : 2023 | Standard Test Method for Measurement of Flow Properties and Evaluation of Wear, Contaminants, and Oxidative Properties of Lubricating Grease by Die Extrusion Method and Preparation |
| ASTM D 8519 : 2023 | Standard Test Method for Determination of Hydrocarbon Types in Waste Plastic Process Oil Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV) |
| ASTM D 5800 : 2021 | Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method |
| ASTM D 4814 : 2023 : REV A | Standard Specification for Automotive Spark-Ignition Engine Fuel |
| ASTM D 8276 : 2019 | Standard Test Method for Hydrocarbon Types in Middle Distillates, including Biodiesel Blends by Gas Chromatography/Mass Spectrometry |
| ASTM D 7344 : 2017 : REV A | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Mini Method) |
| ASTM D 7945 : 2023 | Standard Test Method for Determination of Dynamic Viscosity and Derived Kinematic Viscosity of Liquids by Constant Pressure Viscometer |
| ASTM D 7621 : 2016 : R2021 | Standard Test Method for Determination of Hydrogen Sulfide in Fuel Oils by Rapid Liquid Phase Extraction |
| ASTM D 8150 : 2022 | Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography |
| ASTM D 8322 : 2020 | Standard Test Method for Determination of Elements in Residual Fuels and Crude Oils by Microwave Plasma Atomic Emission Spectroscopy (MP-AES) |
| ASTM D 8383 : 2021 | Standard Test Method for Methyl Hydrogen Content of Hydrocarbon Oils by High Resolution Nuclear Magnetic Resonance Spectroscopy |
| ASTM D 8243 : 2019 | Standard Test Method for Determination of APS Reductase to Estimate Sulfate Reducing Bacterial Bioburdens in Water – Enzyme-Linked Immunosorbent Assay Method (Withdrawn 2024) |
| ASTM D 2700 : 2023 : REV B | Standard Test Method for Motor Octane Number of Spark-Ignition Engine Fuel |
| ASTM D 8304 : 2019 | Standard Test Method for Determination of Compounded Forms of Iron in In-service Fluids |
| ASTM D 7847 : 2022 | Standard Guide for Interlaboratory Studies for Microbiological Test Methods |
| ASTM D 8073 : 2022 | Standard Test Method for Determination of Water Separation Characteristics of Aviation Turbine Fuel by Small Scale Water Separation Instrument |
| ASTM D 8396 : 2022 | Standard Test Method for Group Types Quantification of Hydrocarbons in Hydrocarbon Liquids with a Boiling Point between 36 °C and 343 °C by Flow Modulated GCxGC – FID |
| ASTM D 4741 : 2021 | Standard Test Method for Measuring Viscosity at High Temperature and High Shear Rate by Tapered-Plug Viscometer |
| ASTM D 7757 : 2022 | Standard Test Method for Silicon in Gasoline and Related Products by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry |
| ASTM D 8386 : 2021 | Standard Test Method for Determining Enhanced Filter Blocking Tendency (EFBT) |
| ASTM D 86 : 2023 : REV A : EDT 1 | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 6824 : 2023 | Standard Test Method for Determining Filterability of Aviation Turbine Fuel |
| ASTM D 7463 : 2021 | Standard Test Method for Adenosine Triphosphate (ATP) Content of Microorganisms in Fuel, Fuel/Water Mixtures, and Fuel Associated Water |
| ASTM D 7060 : 2020 | Standard Test Method for Determination of the Maximum Flocculation Ratio and Peptizing Power in Residual and Heavy Fuel Oils (Optical Detection Method) |
| ASTM D 6299 : 2023 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 8368 : 2022 : REV A | Standard Test Method for Determination of Totals of Aromatic, Polyaromatic and Fatty Acid Methyl Esters (FAME) Content of Diesel Fuel Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV) |
| ASTM D 2885 : 2021 | Standard Test Method for Determination of Octane Number of Spark-Ignition Engine Fuels by On-Line Direct Comparison Technique |
| ASTM D 7483 : 2021 | Standard Test Method for Determination of Dynamic Viscosity and Derived Kinematic Viscosity of Liquids by Oscillating Piston Viscometer |
| ASTM D 1218 : 2021 | Standard Test Method for Refractive Index and Refractive Dispersion of Hydrocarbon Liquids |
| ASTM D 7094 : 2023 | Standard Test Method for Flash Point by Modified Continuously Closed Cup (MCCCFP) Tester |
| ASTM D 8098 : 2023 | Standard Test Method for Permanent Gases in C<inf>2</inf> and C<inf>3</inf> Hydrocarbon Products by Gas Chromatography and Pulse Discharge Helium Ionization Detector |
| ASTM D 7861 : 2014 : R2019 | Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy |
| ASTM D 8277 : 2020 | Standard Test Method for Wet Filterability of Lubricants and Hydraulic Fluids by Mass Flow Technique |
| ASTM D 7345 : 2023 | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Micro Distillation Method) |
| ASTM D 8473 : 2022 | Standard Test Method for Determining the Biobased content of Liquid Hydrocarbon Fuels Using Liquid Scintillation Counting with Spiked Carbon-14 |
| ASTM D 6378 : 2022 | Standard Test Method for Determination of Vapor Pressure (VP<inf>X</inf>) of Petroleum Products, Hydrocarbons, and Hydrocarbon-Oxygenate Mixtures (Triple Expansion Method) |
| ASTM D 5580 : 2021 | Standard Test Method for Determination of Benzene, Toluene, Ethylbenzene, <emph type="ital"> p/m</emph>-Xylene, <emph type="ital">o</emph>-Xylene, C<inf>9</inf> and Heavier Aromatics, and Total Aromatics in Finished Gasoline by Gas Chromatography |
| ASTM D 8166 : 2022 | Standard Test Method for Sizing and Counting Particulates in Middle Distillate Fuels and Biodiesel Blend (B6 to B20) Using Continuous Flow and Bottle Sampler Particle Contamination Monitors |
| ASTM D 7668 : 2023 | Standard Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel Oils—Ignition Delay and Combustion Delay Using a Constant Volume Combustion Chamber Method |
| ASTM D 8110 : 2017 | Standard Test Method for Elemental Analysis of Distillate Products by Inductively Coupled Plasma Mass Spectrometry (ICP-MS) |
| ASTM D 7279 : 2020 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer |
| ASTM D 2699 : 2023 : REV B | Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel |
| ASTM D 8315 : 2020 | Standard Test Method for Determination of Wear Metals and Contamination Elements in Used Industrial Oils by Sweeping Flat Electrode Atomic Emission Spectrometry |
| ASTM D 8146 : 2022 | Standard Guide for Evaluating Test Method Capability and Fitness for Use |
| ASTM D 1160 : 2018 | Standard Test Method for Distillation of Petroleum Products at Reduced Pressure |
| ASTM D 7620 : 2010 : R2020 | Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbon Based Fuels by Continuous Injection, Air Oxidation and Ultraviolet Fluorescence Detection |
| ASTM D 97 : 2017 : REV B : R2022 | Standard Test Method for Pour Point of Petroleum Products |
| ASTM D 1266 : 2018 | Standard Test Method for Sulfur in Petroleum Products (Lamp Method) |
| ASTM E 2056 : 2004 : R2016 | Standard Practice for Qualifying Spectrometers and Spectrophotometers for Use in Multivariate Analyses, Calibrated Using Surrogate Mixtures |
| ASTM D 6792 : 2023 : REV C | Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories |
| ASTM D 4012 : 2023 : REV A | Standard Test Method for Adenosine Triphosphate (ATP) Content of Microorganisms in Water |
| ASTM D 7807 : 2020 | Standard Test Method for Determination of Boiling Range Distribution of Hydrocarbon and Sulfur Components of Petroleum Distillates by Gas Chromatography and Chemiluminescence Detection |
| ASTM D 7346 : 2015 : R2021 | Standard Test Method for No Flow Point and Pour Point of Petroleum Products and Liquid Fuels |
| ASTM D 7963 : 2022 | Standard Test Method for Determination of Contamination Level of Fatty Acid Methyl Esters in Middle Distillate and Residual Fuels Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method |
| ASTM E 1655 : 2017 | Standard Practices for Infrared Multivariate Quantitative Analysis |
| ASTM D 8206 : 2018 | Standard Test Method for Oxidation Stability of Lubricating Greases—Rapid Small-Scale Oxidation Test (RSSOT) |
| ASTM D 8126 : 2021 | Standard Test Method for Efficient Basicity Determination by Potentiometric Hydrochloric Acid Titration |
| ASTM D 7525 : 2014 : R2019 : EDT 1 | Standard Test Method for Oxidation Stability of Spark Ignition Fuel—Rapid Small Scale Oxidation Test (RSSOT) |
| ASTM D 8356 : 2020 | Standard Test Method for Sonic Velocity in Manufactured Carbons and Graphite Materials for use in Obtaining Approximate Elastic Constants: Young’s Modulus, Shear Modulus, and Poisson’s Ratio |
| ASTM D 8184 : 2018 : EDT 1 | Standard Test Method for Ferrous Wear Debris Monitoring in In-Service Fluids Using a Particle Quantifier Instrument |
| ASTM D 6450 : 2016 : REV A : R2021 | Standard Test Method for Flash Point by Continuously Closed Cup (CCCFP) Tester |
| ASTM D 3244 : 2021 : REV A | Standard Practice for Utilization of Test Data to Determine Conformance with Specifications |
| ASTM D 445 : 2023 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 2892 : 2023 | Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column) |
| ASTM D 7751 : 2016 : R2021 | Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis |
| ASTM D 56 : 2022 | Standard Test Method for Flash Point by Tag Closed Cup Tester |
| ASTM D 7778 : 2015 : R2022 : EDT 1 | Standard Guide for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
| ASTM D 6822 : 2023 | Standard Test Method for Density, Relative Density, and API Gravity of Crude Petroleum and Liquid Petroleum Products by Thermohydrometer Method |
| ASTM D 7157 : 2023 | Standard Test Method for Determination of Intrinsic Stability of Asphaltene-Containing Residues, Heavy Fuel Oils, and Crude Oils (<emph type="ital">n</emph >-Heptane Phase Separation; Optical Detection) |
| ASTM D 8351 : 2022 | Standard Test Method for Determination of Trace Elements in Biodiesel and Biodiesel Blends by Microwave Plasma Atomic Emission Spectrometry (MP-AES) |
| ASTM D 8288 : 2019 | Standard Test Method for Comparison of Metalworking Fluids Using a Tapping Torque Test Machine |
| ASTM D 7416 : 2009 : R2020 | Standard Practice for Analysis of In-Service Lubricants Using a Particular Five-Part (Dielectric Permittivity, Time-Resolved Dielectric Permittivity with Switching Magnetic Fields, Laser Particle Counter, Microscopic Debris Analysis, and Orbital Viscometer) Integrated Tester |
| ASTM D 5481 : 2021 | Standard Test Method for Measuring Apparent Viscosity at High-Temperature and High-Shear Rate by Multicell Capillary Viscometer |
| ASTM D 5769 : 2022 | Standard Test Method for Determination of Benzene, Toluene, and Total Aromatics in Finished Gasolines by Gas Chromatography/Mass Spectrometry |
| ASTM D 7042 : 2021 : REV A | Standard Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of Kinematic Viscosity) |
| ASTM D 2068 : 2020 | Standard Test Method for Determining Filter Blocking Tendency |
| ASTM D 7623 : 2020 | Standard Test Method for Total Mercury in Crude Oil Using Combustion-Gold Amalgamation and Cold Vapor Atomic Absorption Method |
| ASTM D 7220 : 2022 | Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry |
| ASTM D 8385 : 2022 | Standard Test Method for Dry Filterability of Lubricants and Hydraulic Fluids by Mass Flow Technique |
| ASTM D 7261 : 2022 | Standard Test Method for Determining Water Separation Characteristics of Diesel Fuels by Portable Separometer |
| ASTM D 7806 : 2020 | Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Ester) and Triglyceride Content in Diesel Fuel Oil Using Mid-Infrared Spectroscopy (FTIR Transmission Method) |
| ASTM D 7756 : 2019 | Standard Test Method for Residues in Liquefied Petroleum (LP) Gases by Gas Chromatography with Liquid, On-Column Injection |
| ASTM D 8071 : 2021 | Standard Test Method for Determination of Hydrocarbon Group Types and Select Hydrocarbon and Oxygenate Compounds in Automotive Spark-Ignition Engine Fuel Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV) |
| ASTM D 8369 : 2021 | Standard Test Method for Detailed Hydrocarbon Analysis by High Resolution Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy (GC-VUV) |
| ASTM D 8545 : 2023 : EDT 1 | Standard Test Method for Determination of the Metal Deactivator Additive (MDA) (N,N′-disalicylidene-1,2-propanediamine) Content in Aviation Turbine Fuel by High Performance Liquid Chromatography (HPLC) |
| ASTM D 7419 : 2018 | Standard Test Method for Determination of Total Aromatics and Total Saturates in Lube Basestocks by High Performance Liquid Chromatography (HPLC) with Refractive Index Detection |
| ASTM D 8420 : 2021 | Standard Test Method for Wax Appearance Temperature and Wax Disappearance Temperature of Petroleum Products and Liquid Fuels |
| ASTM D 2266 : 2023 | Standard Test Method for Wear Preventive Characteristics of Lubricating Grease (Four-Ball Method) |
| ASTM D 8302 : 2020 | Standard Test Method for Determination of Cycloparaffin Content in Saturated ATJ-SPK Jet Fuel Gas Chromatography |
| ASTM D 1319 : 2020 : REV A | Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption |
| ASTM D 7622 : 2020 | Standard Test Method for Total Mercury in Crude Oil Using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction |
| ASTM D 7959 : 2019 | Standard Test Method for Chloride Content Determination of Aviation Turbine Fuels using Chloride Test Strip |
| ASTM D 7797 : 2023 | Standard Test Method for Determination of the Fatty Acid Methyl Esters Content of Aviation Turbine Fuel Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method |
| ASTM D 4683 : 2020 | Standard Test Method for Measuring Viscosity of New and Used Engine Oils at High Shear Rate and High Temperature by Tapered Bearing Simulator Viscometer at 150 °C |
| ASTM D 6890 : 2022 | Standard Test Method for Determination of Ignition Delay and Derived Cetane Number (DCN) of Diesel Fuel Oils by Combustion in a Constant Volume Chamber |
| ASTM D 6550 : 2020 | Standard Test Method for Determination of Olefin Content of Gasolines by Supercritical-Fluid Chromatography |
| ASTM D 7096 : 2019 | Standard Test Method for Determination of the Boiling Range Distribution of Gasoline by Wide-Bore Capillary Gas Chromatography |
| ASTM D 8274 : 2020 : REV A | Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil by Portable Rapid Mid-Infrared Analyzer |
| ASTM D 7043 : 2021 | Standard Test Method for Indicating Wear Characteristics of Non-Petroleum and Petroleum Hydraulic Fluids in a Constant Volume Vane Pump |
| ASTM D 130 : 2019 | Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test |
| ASTM D 8305 : 2019 | Standard Test Method for The Determination of Total Aromatic Hydrocarbons and Total Polynuclear Aromatic Hydrocarbons in Aviation Turbine Fuels and other Kerosene Range Fuels by Supercritical Fluid Chromatography |
| ASTM D 8148 : 2022 | Standard Test Method for Spectroscopic Determination of Haze in Fuels |
| ASTM D 7875 : 2020 | Standard Test Method for Determination of Butanol and Acetone Content of Butanol for Blending with Gasoline by Gas Chromatography |
| ASTM D 4929 : 2022 | Standard Test Method for Determination of Organic Chloride Content in Crude Oil |
| ASTM E 456 : 2013 : REV A : R2022 | Standard Terminology Relating to Quality and Statistics |
| ASTM E 456 : 2013 : REV A : R2022 : EDT 1 | Standard Terminology Relating to Quality and Statistics |
| ASTM D 6708 : 2024 | Standard Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material |
| ASTM D 3606 : 2022 | Standard Test Method for Determination of Benzene and Toluene in Spark Ignition Fuels by Gas Chromatography |
| ASTM D 3606 : 2024 | Standard Test Method for Determination of Benzene and Toluene in Spark Ignition Fuels by Gas Chromatography |
| ASTM D 6708 : 2021 | Standard Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material |
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