ASTM D 5765 : 2016
Current
The latest, up-to-date edition.
Standard Practice for Solvent Extraction of Total Petroleum Hydrocarbons from Soils and Sediments Using Closed Vessel Microwave Heating
Hardcopy , PDF
English
01-01-2016
Important note : All end users must be registered with an Account prior to user licenses being assigned.This practice covers the solvent extraction of total petroleum hydrocarbon (TPH) from soils and sediments, using closed vessel microwave heating, for subsequent determination by gravimetric or gas chromatographic techniques.
| Committee |
D 19
|
| DocumentType |
Standard Practice
|
| Pages |
3
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Current
|
| Supersedes |
1.1This practice covers the solvent extraction of total petroleum hydrocarbon (TPH) from soils and sediments, using closed vessel microwave heating, for subsequent determination by gravimetric or gas chromatographic techniques.
1.2This practice is recommended only for solid samples that can pass through a ten mesh screen (approximately 2 mm openings).
1.3The solvent extract obtained by this practice may be analyzed for total or specific nonvolatile and semivolatile petroleum hydrocarbons but may require sample clean-up procedures prior to specific compound analysis.
1.4This practice is limited to solvents that are recommended for use in microwave solvent extraction systems.
1.5The values stated in SI units are to be regarded as standard.
1.5.1Exception—The inch-pound values given for units of pressure are to be regarded as standard; SI unit conversions are shown in parentheses.
1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 9.
| ASTM D 7876 : 2013 : R2018 | Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants |
| ASTM D 3694 : 1996 : R2011 | Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents |
| ASTM D 1129 : 2003 | Standard Terminology Relating to Water |
| ASTM D 3974 : 1981 : R2008 | Standard Practices for Extraction of Trace Elements from Sediments |
| ASTM D 5368 : 1993 : R2006 | Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples |
| ASTM D 1129 : 2013 | Standard Terminology Relating to Water |
| ASTM D 1129 : 2013 : R2020 | Standard Terminology Relating to Water |
| ASTM D 3694 : 1996 | Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents |
| ASTM D 3976 : 1992 : R2005 | Standard Practice for Preparation of Sediment Samples for Chemical Analysis |
| ASTM D 1129 : 2013 : R2020 : EDT 2 | Standard Terminology Relating to Water |
| ASTM D 3976 : 1992 : R2001 | Standard Practice for Preparation of Sediment Samples for Chemical Analysis |
| ASTM D 1129 : 2006 | Standard Terminology Relating to Water |
| ASTM D 3976 : 1992 : R2010 | Standard Practice for Preparation of Sediment Samples for Chemical Analysis |
| ASTM D 3974 : 2009 : R2023 | Standard Practices for Extraction of Trace Elements from Sediments |
| ASTM D 3974 : 2009 | Standard Practices for Extraction of Trace Elements from Sediments |
| ASTM D 3974 : 2009 : R2015 | Standard Practices for Extraction of Trace Elements from Sediments |
| ASTM D 3976 : 1992 : R1996 | Standard Practice for Preparation of Sediment Samples for Chemical Analysis |
| ASTM D 3694 : 1996 : R2017 | Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents |
| ASTM D 1129 : 2013 : R2020 : EDT 1 | Standard Terminology Relating to Water |
| ASTM D 1129 : 1999 : REV A | Standard Terminology Relating to Water |
| ASTM D 3856 : 2011 | Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water |
| ASTM D 1129 : 2006 : REV A | Standard Terminology Relating to Water |
| ASTM D 3974 : 1981 : R2003 : EDT 1 | Standard Practices for Extraction of Trace Elements from Sediments |
| ASTM D 1129 : 2003 : REV A | Standard Terminology Relating to Water |
| ASTM D 3694 : 1996 : R2004 | Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents |
| ASTM D 1129 : 2002 | Standard Terminology Relating to Water |
| ASTM D 5368 : 2013 | Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples (Withdrawn 2014) |
| ASTM D 3856 : 1995 : R2006 | Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water |
| ASTM D 3974 : 1981 : R1999 | Standard Practices for Extraction of Trace Elements from Sediments |
| ASTM D 5368 : 1993 | Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples |
| ASTM D 1129 : 2004 | Standard Terminology Relating to Water |
| ASTM D 3976 : 2022 | Standard Practice for Preparation of Sediment Samples for Chemical Analysis |
| ASTM D 3976 : 1992 : R2015 | Standard Practice for Preparation of Sediment Samples for Chemical Analysis |
| ASTM D 3856 : 2011 : R2015 | Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024) |
| ASTM D 3856 : 1995 : R2000 | Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water |
| ASTM D 5368 : 1993 : R2001 | Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples |
| ASTM D 1129 : 2002 : REV A | Standard Terminology Relating to Water |
| ASTM D 1129 : 2010 | Standard Terminology Relating to Water |
| ASTM D 1129 : 2006 : REV A : EDT 1 | Standard Terminology Relating to Water |
| ASTM D 1129 : 2001 | Standard Terminology Relating to Water |
| ASTM D 1129 : 2004 : EDT 1 | Standard Terminology Relating to Water |
| ASTM D 3694 : 1996 : R2024 | Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents |
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