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ASTM D 5739 : 2006 : R2020

Current

Current

The latest, up-to-date edition.

Standard Practice for Oil Spill Source Identification by Gas Chromatography and Positive Ion Electron Impact Low Resolution Mass Spectrometry

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2020

£52.98
Excluding VAT

Committee
D 19
DocumentType
Standard Practice
Pages
12
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1This practice covers the use of gas chromatography and mass spectrometry to analyze and compare petroleum oil spills and suspected sources.

1.2The probable source for a spill can be ascertained by the examination of certain unique compound classes that also demonstrate the most weathering stability. To a greater or lesser degree, certain chemical classes can be anticipated to chemically alter in proportion to the weathering exposure time and severity, and subsequent analytical changes can be predicted. This practice recommends various classes to be analyzed and also provides a guide to expected weathering-induced analytical changes.

1.3This practice is applicable for moderately to severely degraded petroleum oils in the distillate range from diesel through Bunker C; it is also applicable for all crude oils with comparable distillation ranges. This practice may have limited applicability for some kerosenes, but it is not useful for gasolines.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 3415 : 1998 : R2017 Standard Practice for Identification of Waterborne Oils
ASTM E 3163 : 2018 Standard Guide for Selection and Application of Analytical Methods and Procedures Used during Sediment Corrective Action

ASTM D 3328 : 2006 : R2020 Standard Test Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM D 1129 : 2013 : R2020 : EDT 2 Standard Terminology Relating to Water
ASTM D 3325 : 1990 : R2020 Standard Practice for Preservation of Waterborne Oil Samples
ASTM D 3415 : 1998 : R2024 Standard Practice for Identification of Waterborne Oils
ASTM D 1129 : 2013 : R2020 : EDT 1 Standard Terminology Relating to Water
ASTM D 3326 : 2007 : R2017 Standard Practice for Preparation of Samples for Identification of Waterborne Oils
ASTM E 355 : 1996 : R2021 : EDT 1 Standard Practice for Gas Chromatography Terms and Relationships
ASTM E 355 : 1996 : R2014 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 3326 : 2007 : R2024 Standard Practice for Preparation of Samples for Identification of Waterborne Oils

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