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ASTM D 5075 : 2001 : R2017 : EDT 1

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Nicotine and 3-Ethenylpyridine in Indoor Air

Available format(s)

Hardcopy , PDF

Superseded date

18-06-2022

Language(s)

English

Published date

22-03-2017

£57.59
Excluding VAT

CONTAINED IN VOL. 11.03, 2017 Specifies the sampling/analysis of nicotine and 3-ethenylpyridine (3-EP) in indoor air.

Committee
D 22
DocumentType
Test Method
Pages
8
ProductNote
Reconfirmed EDT 1
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the sampling/analysis of nicotine and 3-ethenylpyridine (3-EP) in indoor air. This test method is based upon the collection of nicotine and 3-EP by adsorption on a sorbent resin, extraction of nicotine and 3-EP from the sorbent resin, and determination by gas chromatography (GC) with nitrogen selective detection. (1)2

1.2The active samplers consist of an macroreticular polystyrene-divinylbenzene copolymer (for example, XAD-4) sorbent tube attached to a sampling pump. Macroreticular polystyrene-divinylbenzene copolymer is referred to “sorbent resin” throughout this method. This test method is applicable to personal or area sampling.

1.3This test method is limited in sample duration by the capacity of the sorbent tube for nicotine (about 300 μg). This test method has been evaluated up to 24-h sample duration; however, samples are typically acquired for at least 1 h (sometimes only 1 h). (2)

1.4For this test method, limits of detection (LOD) and quantitation (LOQ) for nicotine at a sampling rate of 1.5 L/min are, respectively, 0.11 μg/m3 and 0.37 μg/m 3 for 1-h sample duration and 0.01 μg/m3 and 0.05 μg/m3 for 8-h sample duration. The LOD and LOQ for 3-EP at a sampling rate of 1.5 L/min are, respectively, 0.06 μg/m 3 and 0.19 μg/m3 for 1-h sample duration and 0.01 μg/m3 and 0.02 μg/m3 for 8-h sample duration (2). Both LOD and LOQ can be reduced by increasing the sensitivity of the thermionic specific detector.

1.5Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary information is given in 13.6.

ASTM D 1356 : 2015 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1357 : 1995 : R2019 Standard Practice for Planning the Sampling of the Ambient Atmosphere
ASTM D 1357 : 1995 : R2000 Standard Practice for Planning the Sampling of the Ambient Atmosphere
ASTM D 1357 : 1995 : R2005 Standard Practice for Planning the Sampling of the Ambient Atmosphere
ASTM D 1356 : 2017 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3631 : 1999 : R2004 Standard Test Methods for Measuring Surface Atmospheric Pressure
ASTM E 260 : 1996 Standard Practice for Packed Column Gas Chromatography
ASTM D 1356 : 2015 : REV B Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1357 : 1995 : R2011 Standard Practice for Planning the Sampling of the Ambient Atmosphere
ASTM D 5337 : 2011 : R2016 Standard Practice for Flow Rate Adjustment of Personal Sampling Pumps
ASTM D 1356 : 2014 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3631 : 1999 : R2007 Standard Test Methods for Measuring Surface Atmospheric Pressure
ASTM E 355 : 1996 : R2021 : EDT 1 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 3631 : 1999 : R2011 Standard Test Methods for Measuring Surface Atmospheric Pressure
ASTM D 5337 : 1997 Standard Practice for Flow Rate for Calibration of Personal Sampling Pumps
ASTM D 1356 : 2015 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1356 : 2005 : R2010 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1356 : 2020 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1356 : 2000 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 5337 : 2011 Standard Practice for Flow Rate for Calibration of Personal Sampling Pumps
ASTM D 1356 : 2014 : REV B Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1356 : 2014 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM E 355 : 1996 : R2014 Standard Practice for Gas Chromatography Terms and Relationships
ASTM D 5337 : 2004 Standard Practice for Flow Rate for Calibration of Personal Sampling Pumps
ASTM D 1356 : 2005 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3631 : 1999 Standard Test Methods for Measuring Surface Atmospheric Pressure
ASTM D 3631 : 1999 : R2017 Standard Test Methods for Measuring Surface Atmospheric Pressure

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