ASTM D 5075 : 2001 : R2017 : EDT 1
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Nicotine and 3-Ethenylpyridine in Indoor Air
Hardcopy , PDF
18-06-2022
English
22-03-2017
CONTAINED IN VOL. 11.03, 2017 Specifies the sampling/analysis of nicotine and 3-ethenylpyridine (3-EP) in indoor air.
Committee |
D 22
|
DocumentType |
Test Method
|
Pages |
8
|
ProductNote |
Reconfirmed EDT 1
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy | |
Supersedes |
1.1This test method covers the sampling/analysis of nicotine and 3-ethenylpyridine (3-EP) in indoor air. This test method is based upon the collection of nicotine and 3-EP by adsorption on a sorbent resin, extraction of nicotine and 3-EP from the sorbent resin, and determination by gas chromatography (GC) with nitrogen selective detection. (1)2
1.2The active samplers consist of an macroreticular polystyrene-divinylbenzene copolymer (for example, XAD-4) sorbent tube attached to a sampling pump. Macroreticular polystyrene-divinylbenzene copolymer is referred to “sorbent resin” throughout this method. This test method is applicable to personal or area sampling.
1.3This test method is limited in sample duration by the capacity of the sorbent tube for nicotine (about 300 μg). This test method has been evaluated up to 24-h sample duration; however, samples are typically acquired for at least 1 h (sometimes only 1 h). (2)
1.4For this test method, limits of detection (LOD) and quantitation (LOQ) for nicotine at a sampling rate of 1.5 L/min are, respectively, 0.11 μg/m3 and 0.37 μg/m 3 for 1-h sample duration and 0.01 μg/m3 and 0.05 μg/m3 for 8-h sample duration. The LOD and LOQ for 3-EP at a sampling rate of 1.5 L/min are, respectively, 0.06 μg/m 3 and 0.19 μg/m3 for 1-h sample duration and 0.01 μg/m3 and 0.02 μg/m3 for 8-h sample duration (2). Both LOD and LOQ can be reduced by increasing the sensitivity of the thermionic specific detector.
1.5Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary information is given in 13.6.
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