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ASTM D 4052 : 2018

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter

Available format(s)

Hardcopy , PDF

Superseded date

10-05-2023

Language(s)

English

Published date

01-05-2018

£57.59
Excluding VAT

This test method covers the determination of the density, relative density, and API Gravity of petroleum distillates and viscous oils that can be handled in a normal fashion as liquids at the temperature of test, utilizing either manual or automated sample injection equipment.

Committee
D 02
DocumentType
Test Method
Pages
8
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the determination of the density, relative density, and API Gravity of petroleum distillates and viscous oils that can be handled in a normal fashion as liquids at the temperature of test, utilizing either manual or automated sample injection equipment. Its application is restricted to liquids with total vapor pressures (see Test Method D5191) typically below 100 kPa and viscosities (see Test Method D445 or D7042) typically below about 15 000 mm2/s at the temperature of test. The total vapor pressure limitation however can be extended to >100 kPa provided that it is first ascertained that no bubbles form in the U-shaped, oscillating tube, which can affect the density determination. Some examples of products that may be tested by this procedure include: gasoline and gasoline-oxygenate blends, diesel, jet, basestocks, waxes, and lubricating oils.

1.1.1Waxes and highly viscous samples were not included in the 1999 interlaboratory study (ILS) sample set that was used to determine the current precision statements of the method, since all samples evaluated at the time were analyzed at a test temperature of 15 °C. Wax and highly viscous samples require a temperature cell operated at elevated temperatures necessary to ensure a liquid test specimen is introduced for analysis. Consult instrument manufacturer instructions for appropriate guidance and precautions when attempting to analyze wax or highly viscous samples. Refer to the Precision and Bias section of the method and Note 9 for more detailed information about the 1999 ILS that was conducted.

1.2In cases of dispute, the referee method is the one where samples are introduced manually as in 6.3 or 6.4, as appropriate for sample type.

1.3When testing opaque samples, and when not using equipment that is capable of automatic bubble detection, proper procedure shall be established so that the absence of air bubbles in the sample cell can be established with certainty. For the determination of density in crude oil samples use Test Method D5002.

1.4The values stated in SI units are regarded as the standard, unless stated otherwise. The accepted units of measure for density are grams per millilitre (g/mL) or kilograms per cubic metre (kg/m3).

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 7.4, 7.5, and 10.3.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 7547 : 2018 : REV A Standard Specification for Hydrocarbon Unleaded Aviation Gasoline
ASTM D 3227 : 2016 Standard Test Method for (Thiol Mercaptan) Sulfur in Gasoline, Kerosine, Aviation Turbine, and Distillate Fuels (Potentiometric Method)
ASTM D 5986 : 1996 : R2015 Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C<inf>8</inf >–C<inf> 12</inf> Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy
ASTM D 7951 : 2018 Standard Specification for Disproportionation (TDP) Toluene
ASTM D 2190 : 2007 : R2013 Standard Specification for Vinyl Acetate
ASTM D 2225 : 2004 : R2012 Standard Test Methods for Silicone Fluids Used for Electrical Insulation
ASTM D 5372 : 2017 Standard Guide for Evaluation of Hydrocarbon Heat Transfer Fluids
ASTM D 7863 : 2017 Standard Guide for Evaluation of Convective Heat Transfer Coefficient of Liquids
ASTM D 1555 : 2016 Standard Test Method for Calculation of Volume and Weight of Industrial Aromatic Hydrocarbons and Cyclohexane
ASTM D 2917 : 2007 : R2013 Standard Specification for Methyl Isoamyl Ketone
ASTM D 6618 : 2016 Standard Test Method for Evaluation of Engine Oils in Diesel Four-Stroke Cycle Supercharged 1M-PC Single Cylinder Oil Test Engine
ASTM D 4615 : 2012 Standard Specification for n-Butyl Acetate (All Grades) (Withdrawn 2021)
ASTM D 5580 : 2015 Standard Test Method for Determination of Benzene, Toluene, Ethylbenzene, <emph type="ital"> p/m</emph>-Xylene, <emph type="ital">o</emph>-Xylene, C<inf>9</inf> and Heavier Aromatics, and Total Aromatics in Finished Gasoline by Gas Chromatography
ASTM D 7806 : 2012 Standard Test Method for Determination of the Fatty Acid Methyl Ester (FAME) Content of a Blend of Biodiesel and Petroleum-Based Diesel Fuel Oil Using Mid-Infrared Spectroscopy
ASTM D 4837 : 2007 : R2012 Standard Specification for Propylene Glycol Monomethyl Ether (Withdrawn 2021)
ASTM E 2470 : 2009 : R2015 : EDT 1 Standard Specification for Polyester Grade Ethylene Glycol
ASTM D 7960 : 2018 Standard Specification for Unleaded Aviation Gasoline Test Fuel Containing Non-hydrocarbon Components
ASTM D 891 : 2018 Standard Test Methods for Specific Gravity, Apparent, of Liquid Industrial Chemicals
ASTM D 7318 : 2019 Standard Test Method for Existent Inorganic Sulfate in Ethanol by Potentiometric Titration
ASTM D 6823 : 2008 : R2013 Standard Specification for Commercial Boiler Fuels With Used Lubricating Oils
ASTM D 7457 : 2012 Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry (Withdrawn 2019)
ASTM D 5917 : 2015 : R2019 Standard Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas Chromatography and External Calibration
ASTM D 6709 : 2015 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence VIII Spark-Ignition Engine (CLR Oil Test Engine)
ASTM D 5966 : 2013 Standard Test Method for Evaluation of Engine Oils for Roller Follower Wear in Light-Duty Diesel Engine (Withdrawn 2022)
ASTM D 3338/D3338M : 2009 : R2014 : EDT 2 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 6074 : 2015 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
ASTM D 7719 : 2018 Standard Specification for High Aromatic Content Unleaded Hydrocarbon Aviation Gasoline
ASTM D 4652 : 2005 : R2012 Standard Specification for Silicone Fluid Used for Electrical Insulation
ASTM D 3131 : 2007 : R2013 Standard Specification for Isopropyl Acetate (99 % Grade)
ASTM E 1119 : 2009 : R2015 : EDT 1 Standard Specification for Industrial Grade Ethylene Glycol
ASTM D 8183 : 2018 Standard Test Method for Determination of Indicated Cetane Number (ICN) of Diesel Fuel Oils using a Constant Volume Combustion Chamber—Reference Fuels Calibration Method
ASTM D 5194 : 2018 Standard Test Method for Trace Chloride in Liquid Aromatic Hydrocarbons
ASTM D 1153 : 2012 Standard Specification for Methyl Isobutyl Ketone (Withdrawn 2021)
ASTM D 4895 : 2018 Standard Specification for Polytetrafluoroethylene (PTFE) Resin Produced From Dispersion
ASTM D 8150 : 2017 Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography
ASTM D 330 : 2007 : R2013 Standard Specification for 2-Butoxyethanol
ASTM D 5845 : 2001 : R2016 Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and <emph type="ital">tert</emph>-Butanol in Gasoline by Infrared Spectroscopy
ASTM D 1969 : 2007 : R2012 Standard Specification for 2-Ethylhexanol (Withdrawn 2021)
ASTM D 2634 : 2007 : R2013 Standard Specification for Methyl Amyl Acetate (95 % Grade)
ASTM D 976 : 2006 : R2016 Standard Test Method for Calculated Cetane Index of Distillate Fuels
ASTM D 5964 : 2016 Standard Practice for Rubber IRM 901, IRM 902, and IRM 903 Replacement Oils for ASTM No. 1, ASTM No. 2, ASTM No. 3 Oils, and IRM 905 formerly ASTM No. 5 Oil
ASTM D 3238 : 2017 : REV A Standard Test Method for Calculation of Carbon Distribution and Structural Group Analysis of Petroleum Oils by the n-d-M Method
ASTM D 4815 : 2015 : REV B Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, tertiary-Amyl Alcohol and C<inf>1</inf> to C<inf>4</inf> Alcohols in Gasoline by Gas Chromatography
ASTM D 1655 : 2019 Standard Specification for Aviation Turbine Fuels
ASTM D 2892 : 2018 : REV A Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
ASTM D 608 : 2005 : R2019 Standard Specification for Dibutyl Phthalate
ASTM D 1405/D1405M : 2008 : R2013 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels (Withdrawn 2019)
ASTM D 4836 : 2009 : R2017 Standard Specification for Dipropylene Glycol Monomethyl Ether
ASTM D 5769 : 2015 Standard Test Method for Determination of Benzene, Toluene, and Total Aromatics in Finished Gasolines by Gas Chromatography/Mass Spectrometry
ASTM D 7797 : 2018 Standard Test Method for Determination of the Fatty Acid Methyl Esters Content of Aviation Turbine Fuel Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method
ASTM D 3735 : 2007 : R2012 Standard Specification for VM&P Naphthas (Withdrawn 2021)
ASTM D 6923 : 2018 Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1R Test Procedure
ASTM D 7826 : 2019 Standard Guide for Evaluation of New Aviation Gasolines and New Aviation Gasoline Additives
ASTM D 8074 : 2018 Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine
ASTM D 7156 : 2017 Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine
ASTM D 7665 : 2017 Standard Guide for Evaluation of Biodegradable Heat Transfer Fluids
ASTM D 3120 : 2008 : R2019 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
ASTM D 3540 : 2012 Standard Specification for Primary Amyl Acetate, Synthetic (98 % Grade) (Withdrawn 2021)
ASTM D 7371 : 2014 Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
ASTM D 7862 : 2019 Standard Specification for Butanol for Blending with Gasoline for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 7666 : 2012 Standard Specification for Triglyceride Burner Fuel
ASTM D 4857 : 2012 Standard Test Method for Determination of the Ability of Lubricants to Minimize Ring Sticking and Piston Deposits in Two-Stroke-Cycle Gasoline Engines Other Than Outboards (Withdrawn 2021)
ASTM D 2635 : 2007 : R2012 Standard Specification for Methyl Isobutyl Carbinol (Withdrawn 2021)
ASTM D 8256 : 2019 Standard Test Method for Evaluation of Automotive Engine Oils for Inhibition of Deposit Formation in the Sequence VH Spark-Ignition Engine Fueled with Gasoline and Operated Under Low-Temperature, Light-Duty Conditions
ASTM D 7861 : 2014 : R2019 Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
ASTM D 5222 : 2016 Standard Specification for High Fire-Point Mineral Electrical Insulating Oils
ASTM D 4304 : 2017 Standard Specification for Mineral and Synthetic Lubricating Oil Used in Steam or Gas Turbines
ASTM D 7875 : 2014 Standard Test Method for Determination of Butanol and Acetone Content of Butanol for Blending with Gasoline by Gas Chromatography
ASTM D 8111 : 2019 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIH, Spark-Ignition Engine
ASTM D 329 : 2007 : R2013 Standard Specification for Acetone
ASTM D 7422 : 2017 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
ASTM D 7347 : 2015 Standard Test Method for Determination of Olefin Content in Denatured Ethanol by Supercritical Fluid Chromatography (Withdrawn 2024)
ASTM D 5501 : 2012 : R2016 Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography
ASTM D 4054 : 2019 Standard Practice for Evaluation of New Aviation Turbine Fuels and Fuel Additives
ASTM D 6550 : 2015 Standard Test Method for Determination of Olefin Content of Gasolines by Supercritical-Fluid Chromatography
ASTM D 5967 : 2017 Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine
ASTM D 7319 : 2017 Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM D 3128 : 2007 : R2013 Standard Specification for 2-Methoxyethanol
ASTM D 1480 : 2015 Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Bingham Pycnometer
ASTM D 1160 : 2018 Standard Test Method for Distillation of Petroleum Products at Reduced Pressure
ASTM D 5137 : 2007 : R2013 Standard Specification for Hexyl Acetate
ASTM D 7589 : 2016 Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VID Spark Ignition Engine<rangeref></rangeref >
ASTM D 4814 : 2019 Standard Specification for Automotive Spark-Ignition Engine Fuel
ASTM D 5164 : 2005 : R2019 Standard Specification for Propylene Glycol and Dipropylene Glycol
ASTM D 1217 : 2015 Standard Test Method for Density and Relative Density (Specific Gravity) of Liquids by Bingham Pycnometer
ASTM D 7544 : 2012 : R2017 Standard Specification for Pyrolysis Liquid Biofuel
ASTM D 6615 : 2015 : REV A Standard Specification for Jet B Wide-Cut Aviation Turbine Fuel
ASTM D 6987/D6987M : 2013 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-10 Exhaust Gas Recirculation Diesel Engine (Withdrawn 2022)
ASTM D 8147 : 2017 Standard Specification for Special-Purpose Test Fuels for Aviation Compression-Ignition Engines
ASTM D 7044 : 2015 Standard Specification for Biodegradable Fire Resistant Hydraulic Fluids (Withdrawn 2024)
ASTM D 4529 : 2017 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
ASTM D 1492 : 2013 Standard Test Method for Bromine Index of Aromatic Hydrocarbons by Coulometric Titration
ASTM D 2140 : 2008 : R2017 Standard Practice for Calculating Carbon-Type Composition of Insulating Oils of Petroleum Origin
ASTM D 6710 : 2017 Standard Guide for Evaluation of Hydrocarbon-Based Quench Oil
ASTM D 2627 : 2008 : R2012 Standard Specification for Diacetone Alcohol (Withdrawn 2021)
ASTM D 2694 : 2005 : R2019 Standard Specification for Diethylene Glycol<sup>,</sup>
ASTM D 7328 : 2017 Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 1045 : 2014 Standard Test Methods for Sampling and Testing Plasticizers Used in Plastics
ASTM D 2916 : 2009 : R2017 Standard Specification for Isophorone
ASTM D 2693 : 2007 : R2012 Standard Specification for Ethylene Glycol (Withdrawn 2021)
ASTM D 7713 : 2018 Standard Specification for Aqueous Engine Coolant Grade Glycol (53 % by Volume Nominal)
ASTM D 4806 : 2019 Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 7566 : 2019 Standard Specification for Aviation Turbine Fuel Containing Synthesized Hydrocarbons
ASTM D 483 : 2004 : R2018 Standard Test Method for Unsulfonated Residue of Petroleum Plant Spray Oils (Withdrawn 2024)
ASTM D 6224 : 2016 Standard Practice for In-Service Monitoring of Lubricating Oil for Auxiliary Power Plant Equipment
ASTM D 117 : 2018 Standard Guide for Sampling, Test Methods, and Specifications for Electrical Insulating Liquids
ASTM D 1475 : 2013 Standard Test Method For Density of Liquid Coatings, Inks, and Related Products
ASTM D 2414 : 2018 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
ASTM E 1177 : 2014 Standard Specification for Engine Coolant Grade Glycol
ASTM D 4868 : 2017 Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels
ASTM D 7583 : 2016 Standard Test Method for John Deere Coolant Cavitation Test
ASTM D 7640 : 2016 Standard Specification for Engine Coolant Grade Glycerin
ASTM D 7041 : 2016 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbons and Hydrocarbon-Oxygenate Blends by Gas Chromatography with Flame Photometric Detection
ASTM D 7620 : 2010 : R2015 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbon Based Fuels by Continuous Injection, Air Oxidation and Ultraviolet Fluorescence Detection
ASTM D 7042 : 2016 : EDT 3 Standard Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of Kinematic Viscosity)
ASTM D 6448 : 2016 Standard Specification for Industrial Burner Fuels from Used Lubricating Oils
ASTM D 7223 : 2017 Standard Specification for Aviation Certification Turbine Fuel
ASTM D 6756 : 2017 Standard Test Method for Determination of the Red Dye Concentration and Estimation of the ASTM Color of Diesel Fuel and Heating Oil Using a Portable Visible Spectrophotometer
ASTM D 4629 : 2017 Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection
ASTM D 6681 : 2017 Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test Procedure
ASTM D 8048 : 2019 Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
ASTM D 3734 : 2005 : R2018 Standard Specification for High-Flash Aromatic Naphthas
ASTM D 3487 : 2016 : EDT 1 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
ASTM D 2501 : 2014 : R2019 Standard Test Method for Calculation of Viscosity-Gravity Constant (VGC) of Petroleum Oils
ASTM D 7961 : 2017 Standard Practice for Calibrating U-tube Density Cells over Large Ranges of Temperature and Pressure
ASTM D 396 : 2019 Standard Specification for Fuel Oils
ASTM D 8047 : 2018 Standard Test Method for Evaluation of Engine Oil Aeration Resistance in a Caterpillar C13 Direct-Injected Turbocharged Automotive Diesel Engine
ASTM D 910 : 2017 : REV A Standard Specification for Leaded Aviation Gasolines
ASTM D 2636 : 2007 : R2012 Standard Specification for Hexylene Glycol (Withdrawn 2021)
ASTM D 6304 : 2016 : EDT 1 Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration
ASTM D 5622 : 2017 Standard Test Methods for Determination of Total Oxygen in Gasoline and Methanol Fuels by Reductive Pyrolysis
ASTM D 7576 : 2016 Standard Test Method for Determination of Benzene and Total Aromatics in Denatured Fuel Ethanol by Gas Chromatography (Withdrawn 2022)
ASTM D 1481 : 2017 Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer (Withdrawn 2023)
ASTM D 1718 : 2009 : R2017 Standard Specification for Isobutyl Acetate (95 % Grade)
ASTM D 6227 : 2018 Standard Specification for Unleaded Aviation Gasoline Containing a Non-hydrocarbon Component
ASTM D 6560 : 2017 Standard Test Method for Determination of Asphaltenes (Heptane Insolubles) in Crude Petroleum and Petroleum Products
ASTM D 6894 : 2013 Standard Test Method for Evaluation of Aeration Resistance of Engine Oils in Direct-Injected Turbocharged Automotive Diesel Engine (Withdrawn 2022)
ASTM D 4737 : 2010 : R2016 Standard Test Method for Calculated Cetane Index by Four Variable Equation
ASTM D 4171 : 2016 : REV A Standard Specification for Fuel System Icing Inhibitors
ASTM D 7388 : 2018 Standard Specification for Engine Coolant Grade 1,3-Propanediol (PDO)
ASTM D 1555M : 2016 Standard Test Method for Calculation of Volume and Weight of Industrial Aromatic Hydrocarbons and Cyclohexane [Metric]

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