ASTM D 4052 : 2016
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
Hardcopy , PDF
23-01-2017
English
01-12-2016
Committee |
D 02
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DocumentType |
Test Method
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Pages |
8
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PublisherName |
American Society for Testing and Materials
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Status |
Superseded
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SupersededBy | |
Supersedes |
1.1This test method covers the determination of the density, relative density, and API Gravity of petroleum distillates and viscous oils that can be handled in a normal fashion as liquids at the temperature of test, utilizing either manual or automated sample injection equipment. Its application is restricted to liquids with total vapor pressures (see Test Method D5191) typically below 100 kPa and viscosities (see Test Method D445 or D7042) typically below about 15 000 mm2/s at the temperature of test. The total vapor pressure limitation however can be extended to >100 kPa provided that it is first ascertained that no bubbles form in the U-shaped, oscillating tube, which can affect the density determination. Some examples of products that may be tested by this procedure include: gasoline and gasoline-oxygenate blends, diesel, jet, basestocks, waxes, and lubricating oils.
1.1.1Waxes and highly viscous samples were not included in the 1999 interlaboratory study (ILS) sample set that was used to determine the current precision statements of the method, since all samples evaluated at the time were analyzed at a test temperature of 15 °C. Wax and highly viscous samples require a temperature cell operated at elevated temperatures necessary to ensure a liquid test specimen is introduced for analysis. Consult instrument manufacturer instructions for appropriate guidance and precautions when attempting to analyze wax or highly viscous samples. Refer to the Precision and Bias section of the method and Note 8 for more detailed information about the 1999 ILS that was conducted.
1.2In cases of dispute, the referee method is the one where samples are introduced manually as in 6.3 or 6.4, as appropriate for sample type.
1.3When testing opaque samples, and when not using equipment that is capable of automatic bubble detection, proper procedure shall be established so that the absence of air bubbles in the sample cell can be established with certainty. For the determination of density in crude oil samples use Test Method D5002.
1.4The values stated in SI units are regarded as the standard, unless stated otherwise. The accepted units of measure for density are grams per millilitre (g/mL) or kilograms per cubic metre (kg/m3).
1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 7.4, 7.5, and 10.3.
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ASTM D 6560 : 2017 | Standard Test Method for Determination of Asphaltenes (Heptane Insolubles) in Crude Petroleum and Petroleum Products |
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ASTM D 4615 : 2012 | Standard Specification for n-Butyl Acetate (All Grades) (Withdrawn 2021) |
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ASTM D 7806 : 2012 | Standard Test Method for Determination of the Fatty Acid Methyl Ester (FAME) Content of a Blend of Biodiesel and Petroleum-Based Diesel Fuel Oil Using Mid-Infrared Spectroscopy |
ASTM D 4837 : 2007 : R2012 | Standard Specification for Propylene Glycol Monomethyl Ether (Withdrawn 2021) |
ASTM E 2470 : 2009 : R2015 : EDT 1 | Standard Specification for Polyester Grade Ethylene Glycol |
ASTM D 7960 : 2018 | Standard Specification for Unleaded Aviation Gasoline Test Fuel Containing Non-hydrocarbon Components |
ASTM D 891 : 2018 | Standard Test Methods for Specific Gravity, Apparent, of Liquid Industrial Chemicals |
ASTM D 7318 : 2019 | Standard Test Method for Existent Inorganic Sulfate in Ethanol by Potentiometric Titration |
ASTM D 6823 : 2008 : R2013 | Standard Specification for Commercial Boiler Fuels With Used Lubricating Oils |
ASTM D 7457 : 2012 | Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry (Withdrawn 2019) |
ASTM D 5917 : 2015 : R2019 | Standard Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas Chromatography and External Calibration |
ASTM D 6709 : 2015 : REV A | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence VIII Spark-Ignition Engine (CLR Oil Test Engine) |
ASTM D 5966 : 2013 | Standard Test Method for Evaluation of Engine Oils for Roller Follower Wear in Light-Duty Diesel Engine (Withdrawn 2022) |
ASTM D 3338/D3338M : 2009 : R2014 : EDT 2 | Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels |
ASTM D 6074 : 2015 | Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils |
ASTM D 7719 : 2018 | Standard Specification for High Aromatic Content Unleaded Hydrocarbon Aviation Gasoline |
ASTM D 4652 : 2005 : R2012 | Standard Specification for Silicone Fluid Used for Electrical Insulation |
ASTM D 3131 : 2007 : R2013 | Standard Specification for Isopropyl Acetate (99 % Grade) |
ASTM E 1119 : 2009 : R2015 : EDT 1 | Standard Specification for Industrial Grade Ethylene Glycol |
ASTM D 8183 : 2018 | Standard Test Method for Determination of Indicated Cetane Number (ICN) of Diesel Fuel Oils using a Constant Volume Combustion Chamber—Reference Fuels Calibration Method |
ASTM D 5194 : 2018 | Standard Test Method for Trace Chloride in Liquid Aromatic Hydrocarbons |
ASTM D 1153 : 2012 | Standard Specification for Methyl Isobutyl Ketone (Withdrawn 2021) |
ASTM D 4895 : 2018 | Standard Specification for Polytetrafluoroethylene (PTFE) Resin Produced From Dispersion |
ASTM D 8150 : 2017 | Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography |
ASTM D 4737 : 2010 : R2016 | Standard Test Method for Calculated Cetane Index by Four Variable Equation |
ASTM D 4171 : 2016 : REV A | Standard Specification for Fuel System Icing Inhibitors |
ASTM D 7388 : 2018 | Standard Specification for Engine Coolant Grade 1,3-Propanediol (PDO) |
ASTM D 7547 : 2018 : REV A | Standard Specification for Hydrocarbon Unleaded Aviation Gasoline |
ASTM D 3227 : 2016 | Standard Test Method for (Thiol Mercaptan) Sulfur in Gasoline, Kerosine, Aviation Turbine, and Distillate Fuels (Potentiometric Method) |
ASTM D 5986 : 1996 : R2015 | Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C<inf>8</inf >–C<inf> 12</inf> Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy |
ASTM D 7951 : 2018 | Standard Specification for Disproportionation (TDP) Toluene |
ASTM D 2190 : 2007 : R2013 | Standard Specification for Vinyl Acetate |
ASTM D 2225 : 2004 : R2012 | Standard Test Methods for Silicone Fluids Used for Electrical Insulation |
ASTM D 5372 : 2017 | Standard Guide for Evaluation of Hydrocarbon Heat Transfer Fluids |
ASTM D 7863 : 2017 | Standard Guide for Evaluation of Convective Heat Transfer Coefficient of Liquids |
ASTM D 1555 : 2016 | Standard Test Method for Calculation of Volume and Weight of Industrial Aromatic Hydrocarbons and Cyclohexane |
ASTM D 2917 : 2007 : R2013 | Standard Specification for Methyl Isoamyl Ketone |
ASTM D 6618 : 2016 | Standard Test Method for Evaluation of Engine Oils in Diesel Four-Stroke Cycle Supercharged 1M-PC Single Cylinder Oil Test Engine |
ASTM D 330 : 2007 : R2013 | Standard Specification for 2-Butoxyethanol |
ASTM D 5845 : 2001 : R2016 | Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and <emph type="ital">tert</emph>-Butanol in Gasoline by Infrared Spectroscopy |
ASTM D 1969 : 2007 : R2012 | Standard Specification for 2-Ethylhexanol (Withdrawn 2021) |
ASTM D 2634 : 2007 : R2013 | Standard Specification for Methyl Amyl Acetate (95 % Grade) |
ASTM D 976 : 2006 : R2016 | Standard Test Method for Calculated Cetane Index of Distillate Fuels |
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ASTM D 3238 : 2017 : REV A | Standard Test Method for Calculation of Carbon Distribution and Structural Group Analysis of Petroleum Oils by the n-d-M Method |
ASTM D 4815 : 2015 : REV B | Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, tertiary-Amyl Alcohol and C<inf>1</inf> to C<inf>4</inf> Alcohols in Gasoline by Gas Chromatography |
ASTM D 1655 : 2019 | Standard Specification for Aviation Turbine Fuels |
ASTM D 2892 : 2018 : REV A | Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column) |
ASTM D 608 : 2005 : R2019 | Standard Specification for Dibutyl Phthalate |
ASTM D 1405/D1405M : 2008 : R2013 | Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels (Withdrawn 2019) |
ASTM D 4836 : 2009 : R2017 | Standard Specification for Dipropylene Glycol Monomethyl Ether |
ASTM D 5769 : 2015 | Standard Test Method for Determination of Benzene, Toluene, and Total Aromatics in Finished Gasolines by Gas Chromatography/Mass Spectrometry |
ASTM D 7797 : 2018 | Standard Test Method for Determination of the Fatty Acid Methyl Esters Content of Aviation Turbine Fuel Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method |
ASTM D 3735 : 2007 : R2012 | Standard Specification for VM&P Naphthas (Withdrawn 2021) |
ASTM D 6923 : 2018 | Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1R Test Procedure |
ASTM D 7826 : 2019 | Standard Guide for Evaluation of New Aviation Gasolines and New Aviation Gasoline Additives |
ASTM D 8074 : 2018 | Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine |
ASTM D 7156 : 2017 | Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine |
ASTM D 7665 : 2017 | Standard Guide for Evaluation of Biodegradable Heat Transfer Fluids |
ASTM D 3120 : 2008 : R2019 | Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry |
ASTM D 3540 : 2012 | Standard Specification for Primary Amyl Acetate, Synthetic (98 % Grade) (Withdrawn 2021) |
ASTM D 7371 : 2014 | Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method) |
ASTM D 7862 : 2019 | Standard Specification for Butanol for Blending with Gasoline for Use as Automotive Spark-Ignition Engine Fuel |
ASTM D 7666 : 2012 | Standard Specification for Triglyceride Burner Fuel |
ASTM D 4857 : 2012 | Standard Test Method for Determination of the Ability of Lubricants to Minimize Ring Sticking and Piston Deposits in Two-Stroke-Cycle Gasoline Engines Other Than Outboards (Withdrawn 2021) |
ASTM D 2635 : 2007 : R2012 | Standard Specification for Methyl Isobutyl Carbinol (Withdrawn 2021) |
ASTM D 8256 : 2019 | Standard Test Method for Evaluation of Automotive Engine Oils for Inhibition of Deposit Formation in the Sequence VH Spark-Ignition Engine Fueled with Gasoline and Operated Under Low-Temperature, Light-Duty Conditions |
ASTM D 7861 : 2014 : R2019 | Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy |
ASTM D 5222 : 2016 | Standard Specification for High Fire-Point Mineral Electrical Insulating Oils |
ASTM D 4304 : 2017 | Standard Specification for Mineral and Synthetic Lubricating Oil Used in Steam or Gas Turbines |
ASTM D 329 : 2007 : R2013 | Standard Specification for Acetone |
ASTM D 7422 : 2017 : REV A | Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine |
ASTM D 7347 : 2015 | Standard Test Method for Determination of Olefin Content in Denatured Ethanol by Supercritical Fluid Chromatography (Withdrawn 2024) |
ASTM D 5501 : 2012 : R2016 | Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography |
ASTM D 4054 : 2019 | Standard Practice for Evaluation of New Aviation Turbine Fuels and Fuel Additives |
ASTM D 6550 : 2015 | Standard Test Method for Determination of Olefin Content of Gasolines by Supercritical-Fluid Chromatography |
ASTM D 5967 : 2017 | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
ASTM D 7319 : 2017 | Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography |
ASTM D 3734 : 2005 : R2018 | Standard Specification for High-Flash Aromatic Naphthas |
ASTM D 3128 : 2007 : R2013 | Standard Specification for 2-Methoxyethanol |
ASTM D 1480 : 2015 | Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Bingham Pycnometer |
ASTM D 1160 : 2018 | Standard Test Method for Distillation of Petroleum Products at Reduced Pressure |
ASTM D 5137 : 2007 : R2013 | Standard Specification for Hexyl Acetate |
ASTM D 7589 : 2016 | Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VID Spark Ignition Engine<rangeref></rangeref > |
ASTM D 4814 : 2019 | Standard Specification for Automotive Spark-Ignition Engine Fuel |
ASTM D 5164 : 2005 : R2019 | Standard Specification for Propylene Glycol and Dipropylene Glycol |
ASTM D 1217 : 2015 | Standard Test Method for Density and Relative Density (Specific Gravity) of Liquids by Bingham Pycnometer |
ASTM D 7544 : 2012 : R2017 | Standard Specification for Pyrolysis Liquid Biofuel |
ASTM D 6615 : 2015 : REV A | Standard Specification for Jet B Wide-Cut Aviation Turbine Fuel |
ASTM D 6987/D6987M : 2013 : REV A | Standard Test Method for Evaluation of Diesel Engine Oils in T-10 Exhaust Gas Recirculation Diesel Engine (Withdrawn 2022) |
ASTM D 8147 : 2017 | Standard Specification for Special-Purpose Test Fuels for Aviation Compression-Ignition Engines |
ASTM D 7875 : 2014 | Standard Test Method for Determination of Butanol and Acetone Content of Butanol for Blending with Gasoline by Gas Chromatography |
ASTM D 8111 : 2019 | Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIH, Spark-Ignition Engine |
ASTM D 1492 : 2013 | Standard Test Method for Bromine Index of Aromatic Hydrocarbons by Coulometric Titration |
ASTM D 2140 : 2008 : R2017 | Standard Practice for Calculating Carbon-Type Composition of Insulating Oils of Petroleum Origin |
ASTM D 6710 : 2017 | Standard Guide for Evaluation of Hydrocarbon-Based Quench Oil |
ASTM D 2627 : 2008 : R2012 | Standard Specification for Diacetone Alcohol (Withdrawn 2021) |
ASTM D 2694 : 2005 : R2019 | Standard Specification for Diethylene Glycol<sup>,</sup> |
ASTM D 7328 : 2017 | Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection |
ASTM D 1045 : 2014 | Standard Test Methods for Sampling and Testing Plasticizers Used in Plastics |
ASTM D 2916 : 2009 : R2017 | Standard Specification for Isophorone |
ASTM D 2693 : 2007 : R2012 | Standard Specification for Ethylene Glycol (Withdrawn 2021) |
ASTM D 7713 : 2018 | Standard Specification for Aqueous Engine Coolant Grade Glycol (53 % by Volume Nominal) |
ASTM D 4806 : 2019 | Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel |
ASTM D 7566 : 2019 | Standard Specification for Aviation Turbine Fuel Containing Synthesized Hydrocarbons |
ASTM D 483 : 2004 : R2018 | Standard Test Method for Unsulfonated Residue of Petroleum Plant Spray Oils (Withdrawn 2024) |
ASTM D 6224 : 2016 | Standard Practice for In-Service Monitoring of Lubricating Oil for Auxiliary Power Plant Equipment |
ASTM D 117 : 2018 | Standard Guide for Sampling, Test Methods, and Specifications for Electrical Insulating Liquids |
ASTM D 1475 : 2013 | Standard Test Method For Density of Liquid Coatings, Inks, and Related Products |
ASTM D 2414 : 2018 : REV A | Standard Test Method for Carbon Black—Oil Absorption Number (OAN) |
ASTM E 1177 : 2014 | Standard Specification for Engine Coolant Grade Glycol |
ASTM D 4868 : 2017 | Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels |
ASTM D 7640 : 2016 | Standard Specification for Engine Coolant Grade Glycerin |
ASTM D 7044 : 2015 | Standard Specification for Biodegradable Fire Resistant Hydraulic Fluids (Withdrawn 2024) |
ASTM D 4529 : 2017 | Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels |
ASTM D 7583 : 2016 | Standard Test Method for John Deere Coolant Cavitation Test |
ASTM D 7041 : 2016 | Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbons and Hydrocarbon-Oxygenate Blends by Gas Chromatography with Flame Photometric Detection |
ASTM D 7620 : 2010 : R2015 | Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbon Based Fuels by Continuous Injection, Air Oxidation and Ultraviolet Fluorescence Detection |
ASTM D 7042 : 2016 : EDT 3 | Standard Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of Kinematic Viscosity) |
ASTM D 6448 : 2016 | Standard Specification for Industrial Burner Fuels from Used Lubricating Oils |
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