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ASTM D 4052 : 2015

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter

Available format(s)

Hardcopy , PDF

Superseded date

04-02-2016

Superseded by

ASTM D 4052 : 2016

Language(s)

English

Published date

15-12-2015

£57.59
Excluding VAT

Committee
D 02
DocumentType
Test Method
Pages
8
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the determination of the density, relative density, and API Gravity of petroleum distillates and viscous oils that can be handled in a normal fashion as liquids at the temperature of test, utilizing either manual or automated sample injection equipment. Its application is restricted to liquids with total vapor pressures (see Test Method D5191) typically below 100 kPa and viscosities (see Test Method D445 or D7042) typically below about 15 000 mm2/s at the temperature of test. The total vapor pressure limitation however can be extended to >100 kPa provided that it is first ascertained that no bubbles form in the U-shaped, oscillating tube, which can affect the density determination. Some examples of products that may be tested by this procedure include: gasoline and gasoline-oxygenate blends, diesel, jet, basestocks, waxes, and lubricating oils.

1.1.1Waxes and highly viscous samples were not included in the 1999 interlaboratory study (ILS) sample set that was used to determine the current precision statements of the method, since all samples evaluated at the time were analyzed at a test temperature of 15 °C. Wax and highly viscous samples require a temperature cell operated at elevated temperatures necessary to ensure a liquid test specimen is introduced for analysis. Consult instrument manufacturer instructions for appropriate guidance and precautions when attempting to analyze wax or highly viscous samples. Refer to the Precision and Bias section of the method and Note 8 for more detailed information about the 1999 ILS that was conducted.

1.2In cases of dispute, the referee method is the one where samples are introduced manually as in 6.3 or 6.4, as appropriate for sample type.

1.3This test method should not be applied to samples so dark in color that the absence of air bubbles in the sample cell cannot be established with certainty. For the determination of density in crude oil samples use Test Method D5002.

1.4The values stated in SI units are regarded as the standard, unless stated otherwise. The accepted units of measure for density are grams per millilitre (g/mL) or kilograms per cubic metre (kg/m3).

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 7.4, 7.5, and 10.3.

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