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ASTM D 3270 : 2013

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)

Available format(s)

Hardcopy , PDF

Superseded date

18-10-2024

Language(s)

English

Published date

24-10-2013

£57.59
Excluding VAT

These test methods describe the semiautomated procedure for the analyses of various types of samples for the purpose of determining total fluoride.

Committee
D 22
DocumentType
Test Method
Pages
10
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1These test methods describe the semiautomated procedure for the analyses of various types of samples for the purpose of determining total fluoride. Since the test methods incorporate microdistillation of the sample, they may be applied to any fluoride-containing solution where standards of identical composition have been carried through the same sample preparation procedures and have proven to provide quantitative recovery when analyzed by the semiautomated system. Conversely, the methods shall not be applied for analyses until the applicability has been demonstrated.

1.2In normal use, the procedure can detect 0.1 μg/mL of F. The normal range of analysis is from 0.1 to 1.6 μg/mL of F. Higher concentrations can be analyzed by careful dilution of samples with reagent water. If digested samples routinely exceed 1.6 μg/mL of F, the analytical portion of the pump manifold can be modified to reduce sensitivity. However, the best procedure is to analyze a smaller aliquot of the sample. Most accurate results are obtained when the fluoride concentration falls in the middle or upper part of the calibration curve.

1.3The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 8.3, 10.2.4, and 10.2.5 for additional precautions.

ASTM D 3267 : 2012 Standard Test Method for Separation and Collection of Particulate and Water-Soluble Gaseous Fluorides in the Atmosphere (Filter and Impinger Method)
ASTM D 3266 : 1991 : R2018 Standard Test Method for Automated Separation and Collection of Particulate and Acidic Gaseous Fluoride in the Atmosphere (Double Paper Tape Sampler Method)

ASTM D 3268 : 1991 : R2018 Standard Test Method for Separation and Collection of Particulate and Gaseous Fluorides in the Atmosphere (Sodium Bicarbonate-Coated Glass Tube and Particulate Filter Method)
ASTM D 3267 : 1991 : R2000 : EDT 1 Standard Test Method for Separation and Collection of Particulate and Water-Soluble Gaseous Fluorides in the Atmosphere (Filter and Impinger Method)
ASTM D 3614 : 2007 Standard Guide for Laboratories Engaged in Sampling and Analysis of Atmospheres and Emissions
ASTM D 1356 : 2015 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3266 : 1991 : R2000 : EDT 1 Standard Test Method for Automated Separation and Collection of Particulate and Acidic Gaseous Fluoride in the Atmosphere (Double Paper Tape Sampler Method)
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 1356 : 2017 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3268 : 1991 : R2011 Standard Test Method for Separation and Collection of Particulate and Gaseous Fluorides in the Atmosphere (Sodium Bicarbonate-Coated Glass Tube and Particulate Filter Method)
ASTM D 1356 : 2015 : REV B Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3614 : 2007 : R2021 Standard Guide for Laboratories Engaged in Sampling and Analysis of Atmospheres and Emissions
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 3269 : 1996 Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Manual Procedures)
ASTM D 3266 : 1991 : R2011 Standard Test Method for Automated Separation and Collection of Particulate and Acidic Gaseous Fluoride in the Atmosphere (Double Paper Tape Sampler Method)
ASTM D 1356 : 2014 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3268 : 1991 : R2000 : EDT 1 Standard Test Method for Separation and Collection of Particulate and Gaseous Fluorides in the Atmosphere (Sodium Bicarbonate-Coated Glass Tube and Particulate Filter Method)
ASTM D 3267 : 2020 Standard Test Method for Separation and Collection of Particulate and Water-Soluble Gaseous Fluorides in the Atmosphere (Filter and Impinger Method)
ASTM D 3266 : 1991 : R2018 Standard Test Method for Automated Separation and Collection of Particulate and Acidic Gaseous Fluoride in the Atmosphere (Double Paper Tape Sampler Method)
ASTM D 3267 : 1991 : R2005 Standard Test Method for Separation and Collection of Particulate and Water-Soluble Gaseous Fluorides in the Atmosphere (Filter and Impinger Method)
ASTM D 3614 : 2007 : R2013 Standard Guide for Laboratories Engaged in Sampling and Analysis of Atmospheres and Emissions
ASTM D 3614 : 1997 Standard Guide for Laboratories Engaged in Sampling and Analysis of Atmospheres and Emissions
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 1356 : 2015 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3267 : 2012 Standard Test Method for Separation and Collection of Particulate and Water-Soluble Gaseous Fluorides in the Atmosphere (Filter and Impinger Method)
ASTM D 1356 : 2005 : R2010 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3266 : 1991 : R2005 Standard Test Method for Automated Separation and Collection of Particulate and Acidic Gaseous Fluoride in the Atmosphere (Double Paper Tape Sampler Method)
ASTM D 3268 : 1991 : R2005 Standard Test Method for Separation and Collection of Particulate and Gaseous Fluorides in the Atmosphere (Sodium Bicarbonate-Coated Glass Tube and Particulate Filter Method)
ASTM D 1356 : 2020 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1356 : 2000 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1356 : 2014 : REV B Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1356 : 2014 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3269 : 1996 : R2001 : EDT 1 Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Manual Procedures) (Withdrawn 2010)
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1356 : 2005 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water

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