ASTM D 128 : 2024
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
Standard Test Methods for Analysis of Lubricating Grease
Hardcopy , PDF
11-10-2024
English
01-06-2024
Committee |
D 02
|
DocumentType |
Test Method
|
Pages |
11
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy | |
Supersedes |
1.1These test methods for analysis cover greases of the conventional type, which consist essentially of petroleum oil and soap. The constituents that can be determined are soap, unsaponifiable matter (petroleum oil, and so forth), water, free alkalinity, free fatty acid, fat, glycerin, and insolubles.
Note 1:Any of the test methods described herein are best used by an experienced grease analyst who may also be able to make appropriate adaptations of the techniques as occasion requires.
1.2A supplementary test method is provided in Appendix X1. This test method is intended primarily for application to greases containing thickeners that are essentially insoluble in n-hexane, and to greases that cannot be analyzed by conventional methods because of the presence of such constituents as nonpetroleum fluids or nonsoap-type thickeners, or both. In some cases, these constituents can react with strong acid or alkaline solutions.
1.3These test methods appear in the following order:
Sections | |
Ash Determination | 7 – 11 |
Insolubles, Soap, Fat, Petroleum Oil, | 12 – 20 |
Free Alkali and Free Acid | 21 – 23 |
Water | 24 |
Glycerin (Quantitative) | 25 – 29 |
1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D 244 : 2023 | Standard Test Methods and Practices for Emulsified Asphalts |
ASTM D 94 : 2007 : R2017 | Standard Test Methods for Saponification Number of Petroleum Products |
ASTM D 7666 : 2012 : R2019 | Standard Specification for Triglyceride Burner Fuel |
ASTM D 4175 : 2023 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
ASTM D 4175 : 2024 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
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