ASTM C 1347 : 2008 : R2014 : EDT 1
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Practice for Preparation and Dissolution of Uranium Materials for Analysis
Hardcopy , PDF
13-01-2023
English
14-06-2014
Important note : All end users must be registered with an Account prior to user licenses being assigned.CONTAINED IN VOL. 12.01, 2015 Defines dissolution treatments for uranium materials that are applicable to the test methods used for characterizing these materials for uranium elemental, isotopic, and impurities determinations.
| Committee |
C 26
|
| DocumentType |
Standard Practice
|
| Pages |
9
|
| ProductNote |
Reconfirmed EDT 1
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
1.1This practice covers dissolution treatments for uranium materials that are applicable to the test methods used for characterizing these materials for uranium elemental, isotopic, and impurities determinations. Dissolution treatments for the major uranium materials assayed for uranium or analyzed for other components are listed.
1.2The treatments, in order of presentation, are as follows:
| Procedure Title | Section |
| Dissolution of Uranium Metal and Oxide with Nitric Acid | 8.1 |
| Dissolution of Uranium Oxides with Nitric Acid and Residue | 8.2 |
| Dissolution of Uranium-Aluminum Alloys in Hydrochloric Acid | 8.3 |
| Dissolution of Uranium Scrap and Ash by Leaching with Nitric | 8.4 |
| Dissolution of Refractory Uranium-Containing Material by | 8.5 |
| Dissolution of Uranium—Aluminum Alloys | 8.6 |
1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7.
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| ASTM C 1672 : 2017 | Standard Test Method for Determination of Uranium or Plutonium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer |
| ASTM C 1647 : 2013 | Standard Practice for Removal of Uranium or Plutonium, or both, for Impurity Assay in Uranium or Plutonium Materials |
| ASTM C 1816 : 2016 | Standard Practice for The Ion Exchange Separation of Small Volume Samples Containing Uranium, Americium, and Plutonium Prior to Isotopic Abundance and Content Analysis |
| ASTM C 968 : 2012 | Standard Test Methods for Analysis of Sintered Gadolinium Oxide-Uranium Dioxide Pellets |
| ASTM C 1474 : 2019 | Standard Test Method for Analysis of Isotopic Composition of Uranium in Nuclear-Grade Fuel Material by Quadrupole Inductively Coupled Plasma-Mass Spectrometry |
| ASTM C 1413 : 2018 | Standard Test Method for Isotopic Analysis of Hydrolyzed Uranium Hexafluoride and Uranyl Nitrate Solutions by Thermal Ionization Mass Spectrometry |
| ASTM C 1625 : 2012 | Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry |
| ASTM C 1590 : 2004 : R2014 | Standard Practice for Alternate Actinide Calibration for Inductively Coupled Plasma-Mass Spectrometry |
| ASTM C 1832 : 2016 | Standard Test Method for Determination of Uranium Isotopic Composition by the Modified Total Evaporation (MTE) Method Using a Thermal Ionization Mass Spectrometer |
| ASTM C 1845 : 2016 | Standard Practice for The Separation of Lanthanide Elements from Uranium Matrices Using High Pressure Ion Chromatography (HPIC) for Isotopic Analyses by Inductively Coupled Plasma Mass Spectrometry (ICP-MS) |
| ASTM C 696 : 2011 | Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Uranium Dioxide Powders and Pellets |
| ASTM C 1517 : 2016 | Standard Test Method for Determination of Metallic Impurities in Uranium Metal or Compounds by DC-Arc Emission Spectroscopy |
| ASTM C 1128 : 2018 | Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 1287 : 2018 | Standard Test Method for Determination of Impurities in Nuclear Grade Uranium Compounds by Inductively Coupled Plasma Mass Spectrometry |
| ASTM D 7876 : 2013 : R2018 | Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants |
| ASTM C 1267 : 2017 | Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium |
| ASTM C 1462 : 2000 : R2013 | Standard Specification for Uranium Metal Enriched to More than 15 % and Less Than 20 % 235U |
| ASTM C 1267 : 2017 : R2022 | Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium |
| ASTM C 1411 : 2020 | Standard Practice for The Ion Exchange Separation of Uranium and Plutonium Prior to Isotopic Analysis |
| ASTM C 1625 : 2019 | Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry |
| ASTM E 321 : 2020 | Standard Test Method for Atom Percent Fission in Uranium and Plutonium Fuel (Neodymium-148 Method) |
| ASTM C 1871 : 2022 | Standard Test Method for Determination of Uranium Isotopic Composition by the Double Spike Method Using a Thermal Ionization Mass Spectrometer |
| ASTM C 1832 : 2022 | Standard Test Method for Determination of Uranium Isotopic Composition by Modified Total Evaporation (MTE) Method Using Thermal Ionization Mass Spectrometer |
| ASTM C 696 : 2019 | Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Uranium Dioxide Powders and Pellets |
| ASTM C 1590 : 2021 | Standard Practice for Alternate Actinide Calibration for Inductively Coupled Plasma-Mass Spectrometry |
| ASTM C 1462 : 2021 | Standard Specification for Uranium Metal Enriched to Less Than 20 % <sup> 235</sup >U |
| ASTM C 968 : 2019 | Standard Test Methods for Analysis of Sintered Gadolinium Oxide-Uranium Dioxide Pellets |
| ASTM C 1647 : 2020 | Standard Practice for Removal of Uranium or Plutonium, or both, for Impurity Assay in Uranium or Plutonium Materials |
| ASTM C 1022 : 2017 : R2022 | Standard Test Methods for Chemical and Atomic Absorption Analysis of Uranium-Ore Concentrate |
| ASTM C 776 : 2017 : R2022 | Standard Specification for Sintered Uranium Dioxide Pellets for Light Water Reactors |
| ASTM D 1193 : 1977 : R1983 : EDT 1 | Standard Specification for Reagent Water |
| ASTM C 1168 : 2015 | Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis |
| ASTM D 1193 : 2006 : R2011 | Standard Specification for Reagent Water |
| ASTM C 753 : 2016 : REV A | Standard Specification for Nuclear-Grade, Sinterable Uranium Dioxide Powder |
| ASTM D 1193 : 1991 | Standard Specification for Reagent Water |
| ASTM C 776 : 2017 | Standard Specification for Sintered Uranium Dioxide Pellets for Light Water Reactors |
| ASTM C 1168 : 2001 | Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis |
| ASTM C 1168 : 2015 : REDLINE | Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis |
| ASTM C 1168 : 1990 : R1995 : EDT 1 | Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis |
| ASTM D 1193 : 1970 | Standard Specification For Reagent Water |
| ASTM D 1193 : 2006 | Standard Specification for Reagent Water |
| ASTM D 1193 : 1999 | Standard Specification for Reagent Water |
| ASTM D 1193 : 2006 : R2018 | Standard Specification for Reagent Water |
| ASTM C 753 : 2016 : REV A : R2021 | Standard Specification for Nuclear-Grade, Sinterable Uranium Dioxide Powder |
| ASTM C 1168 : 2008 | Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis |
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