ASTM B 954 : 2015
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Analysis of Magnesium and Magnesium Alloys by Atomic Emission Spectrometry
Hardcopy , PDF
01-05-2023
English
03-11-2015
Committee |
B 07
|
DocumentType |
Test Method
|
Pages |
9
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy | |
Supersedes |
1.1This test method describes the analysis of magnesium and its alloys by atomic emission spectrometry. The magnesium specimen to be analyzed may be in the form of a chill cast disk, casting, sheet, plate, extrusion or some other wrought form or shape. The elements covered in the scope of this method are listed in the table below.
Element | Mass Fraction Range (Wt %) |
Aluminum | 0.001 to 12.0 |
Beryllium | 0.0001 to 0.01 |
Boron | 0.0001 to 0.01 |
Cadmium | 0.0001 to 0.05 |
Calcium | 0.0005 to 0.05 |
Cerium | 0.01 to 3.0 |
Chromium | 0.0002 to 0.005 |
Copper | 0.001 to 0.05 |
Dysprosium | 0.01 to 1.0 |
Erbium | 0.01 to 1.0 |
Gadolinium | 0.01 to 3.0 |
Iron | 0.001 to 0.06 |
Lanthanum | 0.01 to 1.5 |
Lead | 0.005 to 0.1 |
Lithium | 0.001 to 0.05 |
Manganese | 0.001 to 2.0 |
Neodymium | 0.01 to 3.0 |
Nickel | 0.0005 to 0.05 |
Phosphorus | 0.0002 to 0.01 |
Praseodymium | 0.01 to 0.5 |
Samarium | 0.01 to 1.0 |
Silicon | 0.002 to 5.0 |
Silver | 0.001 to 0.2 |
Sodium | 0.0005 to 0.01 |
Strontium | 0.01 to 4.0 |
Tin | 0.002 to 0.05 |
Titanium | 0.001 to 0.02 |
Yttrium | 0.02 to 7.0 |
Ytterbium | 0.01 to 1.0 |
Zinc | 0.001 to 10.0 |
Zirconium | 0.001 to 1.0 |
Note 1:The mass fraction ranges given in the above scope are estimates based on two manufacturers observations and data provided by a supplier of atomic emission spectrometers. The range shown for each element does not demonstrate the actual usable analytical range for that element. The usable analytical range may be extended higher or lower based on individual instrument capability, spectral characteristics of the specific element wavelength being used and the availability of appropriate reference materials.
1.2This test method is suitable primarily for the analysis of chill cast disks as described in Sampling Practice B953. Other forms may be analyzed, provided that: (1) they are sufficiently massive to prevent undue heating, (2) they allow machining to provide a clean, flat surface which creates a seal between the specimen and the spark stand, and (3) reference materials of a similar metallurgical condition (spectrochemical response) and chemical composition are available.
1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety and health statements are given in Section 10.
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ASTM E 1329 : 2000 | Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis |
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ASTM E 135 : 2002 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
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ASTM B 953 : 2021 | Standard Practice for Sampling Magnesium and Magnesium Alloys for Spectrochemical Analysis |
ASTM E 1257 : 1993 : R2003 | Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis |
ASTM E 135 : 2022 : REV A | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
ASTM E 135 : 2021 | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
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ASTM E 1257 : 1993 : R2008 | Standard Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis |
ASTM E 1507 : 1998 | Standard Guide for Describing and Specifying the Spectrometer of an Optical Emission Direct-Reading Instrument |
ASTM E 135 : 2020 : REV B | Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials |
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