PD CEN/TS 13649:2014
Current
The latest, up-to-date edition.
Stationary source emissions. Determination of the mass concentration of individual gaseous organic compounds. Sorptive sampling method followed by solvent extraction or thermal desorption
Hardcopy , PDF
English
31-12-2014
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Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Apparatus and materials
6 Sampling procedure
7 Analytical procedure
8 Calculation of results
9 Quality control
10 Report
Annex A (normative) - Sample trains
Annex B (informative) - Solvent extraction of activated
charcoal tubes
Annex C (informative) - Additional information on flue
gas sampling using thermal desorption tubes
Annex D (informative) - Validation of monitoring methods
for speciated organic substances in stack gas
Annex E (informative) - Safety measures
Bibliography
Defines procedures for the sampling, preparation and analysis of individual volatile organic compounds (VOCs) in waste gas, such as those arising from solvent using processes.
| Committee |
EH/2/1
|
| DevelopmentNote |
Supersedes BS EN 13649 & 11/30243100 DC. (12/2014)
|
| DocumentType |
Standard
|
| Pages |
52
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
| Supersedes |
This Technical Specification specifies procedures for the sampling, preparation and analysis of individual volatile organic compounds (VOCs) in waste gas, such as those arising from solvent using processes. Sampling occurs by adsorption on sorbents, preparation by solvent extraction or thermodesorption and analysis by gas chromatography. Examples of individual VOC are given in relevant industry sector BAT Reference documents (BREFs). The results obtained are expressed as the mass concentration (mg/m 3) of the individual gaseous organic compounds. This document is suitable for measuring individual VOCs whose ranges vary depending on compound and test method, refer to AnnexB and C. This Technical Specification may be used to meet the monitoring requirements of the Industrial Emission Directive (IED) and associated supporting documents. This Technical Specification is not suitable for measuring total organic carbon (TOC). For the measurement of the mass concentration of total organic carbon then EN12619 [3] is applicable.
| Standards | Relationship |
| CEN/TS 13649:2014 | Identical |
| ASTM D 3686 : 2013 : REDLINE | Standard Practice for Sampling Atmospheres to Collect Organic Compound Vapors (Activated Charcoal Tube Adsorption Method) |
| CEN/TS 14793:2005 | Stationary source emission - Intralaboratory validation procedure for an alternative method compared to a reference method |
| ISO 14956:2002 | Air quality — Evaluation of the suitability of a measurement procedure by comparison with a required measurement uncertainty |
| EN ISO 16017-1:2000 | Indoor, ambient and workplace air - Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography - Part 1: Pumped sampling (ISO 16017-1:2000) |
| EN 1076:2009 | Workplace exposure - Procedures for measuring gases and vapours using pumped samplers - Requirements and test methods |
| ISO 16017-1:2000 | Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 1: Pumped sampling |
| EN 15259:2007 | Air quality - Measurement of stationary source emissions - Requirements for measurement sections and sites and for the measurement objective, plan and report |
| EN 12619:2013 | Stationary source emissions - Determination of the mass concentration of total gaseous organic carbon - Continuous flame ionisation detector method |
| EN ISO 14956:2002 | Air quality - Evaluation of the suitability of a measurement procedure by comparison with a required measurement uncertainty (ISO 14956:2002) |
| ISO 16000-6:2011 | Indoor air Part 6: Determination of volatile organic compounds in indoor and test chamber air by active sampling on Tenax TA sorbent, thermal desorption and gas chromatography using MS or MS-FID |
| ISO/IEC Guide 98-3:2008 | Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995) |
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