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EN 62021-2:2007

Current

Current

The latest, up-to-date edition.

Insulating liquids - Determination of acidity - Part 2: Colourimetric titration

Published date

26-07-2007

FOREWORD
INTRODUCTION
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
   5.1 Titration reagent
   5.2 Titration solvent
   5.3 Potassium hydrogen phthalate, primary standard
   5.4 Standard hydrochloric acid solution
   5.5 Alkali Blue 6B indicator solution
   5.6 Cobalt nitrate solution
6 Apparatus
   6.1 Titration vessel
   6.2 Stirrer
   6.3 Burette
7 Sampling
8 Procedure
   8.1 Standardization of alcoholic potassium hydroxide
        solution
   8.2 Blank titration
   8.3 Sample titration
9 Calculation of results
10 Precision
   10.1 Repeatability
   10.2 Reproducibility
11 Report
Annex A (informative) Determination of acidity in electrical
        insulating oils by photometric titration
Annex ZA (normative) Normative references to international
         publications with their corresponding European
         publications

Describes a procedure for determination of the acidity of unused and used electrical mineral insulating oils. The method may be used to indicate relative changes that occur in a mineral insulating oil during use under oxidizing conditions that may or may not be shown by other properties of the resulting mineral oil. The acidity can be used in the quality control of unused mineral oil. As a variety of oxidation products present in used mineral oil contribute to acidity and these products vary widely in their corrosion properties, the test cannot be used to predict corrosiveness of a mineral oil under service conditions.

Committee
CLC/SR 10
DocumentType
Standard
PublisherName
European Committee for Standards - Electrical
Status
Current

BS EN 60422:2013 Mineral insulating oils in electrical equipment. Supervision and maintenance guidance
CEI EN 61099 : 2011 INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
EN 62701:2014 Fluids for electrotechnical applications - Recycled mineral insulating oils for transformers and switchgears
EN 61099:2010 Insulating liquids - Specifications for unused synthetic organic esters for electrical purposes
I.S. EN 60422:2013 MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE (IEC 60422:2013 (EQV))
I.S. EN IEC 61125:2018 INSULATING LIQUIDS - TEST METHODS FOR OXIDATION STABILITY - TEST METHOD FOR EVALUATING THE OXIDATION STABILITY OF INSULATING LIQUIDS IN THE DELIVERED STATE
I.S. EN 61099:2010 INSULATING LIQUIDS - SPECIFICATIONS FOR UNUSED SYNTHETIC ORGANIC ESTERS FOR ELECTRICAL PURPOSES
BS EN 60296:2012 Fluids for electrotechnical applications. Unused mineral insulating oils for transformers and switchgear
I.S. EN 62701:2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS
CEI EN 60296 : 2013 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
EN 60296:2012 Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
EN IEC 61125:2018 Insulating liquids - Test methods for oxidation stability - Test method for evaluating the oxidation stability of insulating liquids in the delivered state
BS EN 61099:2010 Insulating liquids. Specifications for unused synthetic organic esters for electrical purposes
UNE-EN 60296:2012 Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
UNE-EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
BS EN IEC 61125:2018 Insulating liquids. Test methods for oxidation stability. Test method for evaluating the oxidation stability of insulating liquids in the delivered state
UNE-EN 61099:2011 Insulating liquids - Specifications for unused synthetic organic esters for electrical purposes
I.S. EN 60296:2012 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR (IEC 60296:2012 (EQV))
EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
CEI EN 60422 : 2014 MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE

IEC 60475:2011 Method of sampling insulating liquids
IEC 60567:2011 Oil-filled electrical equipment - Sampling of gases and analysis of free and dissolved gases - Guidance
ISO 6619:1988 Petroleum products and lubricants — Neutralization number — Potentiometric titration method
EN 60567:2011 Oil-filled electrical equipment - Sampling of gases and analysis of free and dissolved gases - Guidance

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