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EN 61619:1997

Current

Current

The latest, up-to-date edition.

Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography

Published date

23-04-1997

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1 Scope and object
2 Normative reference
3 Definitions
4 Principle
5 Reagents and auxiliary materials
6 Apparatus
7 Sample
8 Chromatograph operating conditions
9 Data-processing system
10 Checks of instrumental performance
11 Procedure
12 Test report
13 Detection limit
14 Precision
Annexes
A Test mixtures
B General informations
C Bibliography
ZA Normative references to international publications
    with their corresponding European publications

Specifies a method for the determination of polychlorinated biphenyl (PCB) concentration in non-halogenated insulating liquids by high-resolution capillary column gas chromatography using an electron capture detector (ECD). Gives total PCB content; especially useful when a detailed analysis of PCB congeners is necessary.

Committee
CLC/SR 10
DocumentType
Standard
PublisherName
European Committee for Standards - Electrical
Status
Current

Standards Relationship
NF EN 61619 : 1997 Identical
IEC 61619:1997 Identical
NBN EN 61619 : 1997 Identical
NEN EN IEC 61619 : 2004 Identical
I.S. EN 61619:1999 Identical
PN EN 61619 : 2002 Identical
SN EN 61619 : 1997 Identical
DIN EN 61619 : 1998 Identical
VDE 0371-8 : 1998 Identical
BS EN 61619:1997 Identical
CEI EN 61619 : 1998 Identical
UNE-EN 61619:1998 Identical

BS 2000-462.3(2004) : 2004 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
BS EN 60422:2013 Mineral insulating oils in electrical equipment. Supervision and maintenance guidance
BS EN 15308:2016 Characterization of waste. Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
S.R. CLC/TR 50503:2010 GUIDELINES FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
DIN EN 16167:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
I.S. EN 12766-3:2005 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
EN 62701:2014 Fluids for electrotechnical applications - Recycled mineral insulating oils for transformers and switchgears
EN 12766-2:2001 Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content
I.S. EN 60422:2013 MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE (IEC 60422:2013 (EQV))
UNI EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
BS EN 12766-3:2004 Petroleum products and used oils. Determination of PCBs and related products Determination and quantification of polychlorinated terphenyls (PCT) and polychlorinated benzyl toluenes (PCBT) content by gas chromatography (GC) using an electron capture detector (ECD)
EN 15308:2016 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
UNE-EN 15308:2017 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
05/30133366 DC : DRAFT MAY 2005 EN 5XXXX BTTF 116-1 - STANDARD FOR THE INVENTORY, CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
BS EN 16167:2012 Sludge, treated biowaste and soil. Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
06/30159746 DC : 0 BS EN 50503 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - STANDARD FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
BS EN 60296:2012 Fluids for electrotechnical applications. Unused mineral insulating oils for transformers and switchgear
12/30231385 DC BS ISO 13876. Soil quality. Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
PREN 15308 : DRAFT 2015 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
17/30364002 DC : 0 BS EN 16167 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
I.S. EN 62701:2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS
BS 2000-462.2(2001) : 2001 METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
ISO 13876:2013 Soil quality — Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
I.S. EN 12766-2:2001 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
CEI EN 60296 : 2013 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
EN 60296:2012 Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
CEI EN 62770 : 2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
05/30136951 DC : 0 EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE, SOIL AND SLUDGE BY USING CAPILLARY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
BS EN 62770:2014 Fluids for electrotechnical applications. Unused natural esters for transformers and similar electrical equipment
10/30147454 DC : 0 BS EN 16167 - SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
I.S. EN 16167:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD)
I.S. EN 62770:2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
PREN 16167 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
UNE-EN 60296:2012 Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
UNE-EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
UNE-EN 62770:2014 Fluids for electrotechnical applications - Unused natural esters for transformers and similar electrical equipment
15/30330799 DC : 0 BS EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
CLC/TR 50503:2010 Guidelines for the inventory control, management, decontamination and/or disposal of electrical equipment and insulating liquids containing PCBs
I.S. EN 15308:2016 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
I.S. EN 60296:2012 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR (IEC 60296:2012 (EQV))
EN 16167:2012 Sludge, treated biowaste and soil - Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
DIN EN 12766-3:2005-02 Petroleum products and used oils - Determination of PCBs and related products - Part 3: Determination and quantification of polychlorinated terphenyls (PCT) and polychlorinated benzyl toluenes (PCBT) content by gas chromatography (GC) using an electron capture detector (ECD)
BS EN 12766-2:2001 Methods of test for petroleum and its products. Petroleum products and used oils. Determination of PCBs and related products Calculation of polychlorinated biphenyl (PCB) content
EN 62770:2014 Fluids for electrotechnical applications - Unused natural esters for transformers and similar electrical equipment
EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
CEI EN 60422 : 2014 MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE

IEC 60475:2011 Method of sampling insulating liquids

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