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EN 1948-2:2006

Current

Current

The latest, up-to-date edition.

Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs

Published date

15-03-2006

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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle of the extraction and clean-up procedure
6 Device, materials and [13]C[12]-labelled standards
7 Method validation and quality control requirements
8 Sample pre-treatment and extraction
9 Report
Annex A (informative) Examples of operation of extraction and
                      clean-up methods
Annex B (informative) Relations to EU Directives
Bibliography

This European Standard specifies the extraction and clean-up procedures of the sampled PCDDs/PCDFs. It is integral part of the complete measurement procedure. The use of the other two parts prEN 1948-1:2005 and prEN 1948-3:2005 describing sampling or identification and quantification, respectively, is necessary for the determination of the PCDDs/PCDFs.This European Standard has been designed to measure PCDD/PCDF concentrations at about 0,1 ng I-TEQ/m3 in stationary source emissions.This European Standard specifies both method validation and a framework of quality control requirements which shall be fulfilled by any PCDD/PCDF extraction and clean-up methods to be applied. Some methods are described in detail in Annex A as examples of proven procedures.Each of the three sampling methods (Part 1) can be combined with the extraction and clean-up (Part 2) and the identification and quantification (Part 3) to complete the measurement procedure.During comparison measurements of the three sampling methods on municipal waste incinerators at the level of about 0,1 ng I-TEQ/m3 these methods have been deemed comparable within the expected range of uncertainty. Validation trials were performed on the flue gas of municipal waste incinerators at the level of about 0,1 ng I-TEQ/m3 and a dust loading of from 1 mg/m3 to 15 mg/m3. Although this European Standard is primarily developed and validated for gaseous streams emitted by waste incinerators, the practical experience shows that it can be applied for wide concentration ranges and various emission sources.The procedure described in the three parts of prEN 1948:2005 specifies requirements which shall be met in order to measure the 17 congeners necessary to calculate the total I-TEQ (see Table A.1 of prEN 1948-1:2005).Besides the determination of PCDDs/PCDFs the described measurement methods are suitable for determination of other low-volatile substances, e.g. of dioxin-like PCBs (details for sampling and analyses se

Committee
CEN/TC 264
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
UNE-EN 1948-2:2007 Identical
NEN EN 1948-2 : 2006 Identical
NF EN 1948-2 : 2006 Identical
BS EN 1948-2:2006 Identical
I.S. EN 1948-2:2006 Identical
SN EN 1948-2 : 2006 Identical
PN EN 1948-2 : 2006 Identical
NS EN 1948-2 : 2ED 2006 Identical
UNI EN 1948-2 : 2006 Identical
NBN EN 1948-2 : 2006 Identical
DIN EN 1948-2:2006-06 Identical

DD CEN/TS 1948-4:2007 Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Sampling and analysis of dioxin-like PCBs
PD CEN/TS 1948-5:2015 Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Long-term sampling of PCDDs/PCDFs and PCBs
ISO 16000-14:2009 Indoor air — Part 14: Determination of total (gas and particle-phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDDs/PCDFs) — Extraction, clean-up and analysis by high-resolution gas chromatography and mass spectrometry
UNI CEN/TS 16190 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
CEN/TS 1948-5:2015 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 5: Long-term sampling of PCDDs/PCDFs and PCBs
EN 1948-4:2010+A1:2013 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs
CEN/TS 15675:2007 Air quality - Measurement of stationary source emissions - Application of EN ISO/IEC 17025:2005 to periodic measurements
03/320960 DC : DRAFT NOV 2003 EN 1948-1 - STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 1: SAMPLING
03/320962 DC : DRAFT DEC 2003 EN 1948-3 - STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 3: IDENTIFICATION AND QUANTIFICATION OF PCDDS/PCDFS
I.S. EN 1948-4:2010 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
BS ISO 13914:2013 Soil quality. Determination of dioxins and furans and dioxin-like polychlorinated biphenyls by gas chromatography with high-resolution mass selective detection (GC/HRMS)
S.R. CEN TS 15675:2007 AIR QUALITY - MEASUREMENT OF STATIONARY SOURCE EMISSIONS - APPLICATION OF EN ISO/IEC 17025:2005 TO PERIODIC MEASUREMENTS
PREN 16190 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
I.S. EN 1948-1:2006 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 1: SAMPLING OF PCDDS/PCDFS
DIN EN 1948-1:2006-06 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs
DIN EN 1948-3:2006-06 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
I.S. EN 1948-3:2006 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 3: IDENTIFICATION AND QUANTIFICATION OF PCDDS/PCDFS
VDI 3890:2016-03 Emission control - Pet cremation facilities
VDI 2597:2004-07 Emission control - Plants for the production of lead and lead alloys
VDI 3927 Blatt 2:2015-05 Waste gas cleaning - Reduction of inorganic and organic trace species in combustion flue gases
VDI 3476 Blatt 1:2015-06 Waste gas cleaning - Methods of catalytic waste gas cleaning - Fundamentals
VDI 3891:2015-07 Emission control - Human cremation facilities
VDI 3498 Blatt 2:2002-07 Ambient air measurement - Indoor air measurement - Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans; Method using small filters
VDI 3899 Blatt 1:2016-05 Emission control - Landfill gas - Utilisation and treatment of landfill gas
VDI 2576:2010-01 Emission control - Carbothermic and metallothermic production of ferroalloys and silicon metal
VDI 3498 Blatt 1:2002-07 Ambient air measurement - Indoor air measurement - Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans; Method using large filters
VDI 3475-3 : 2006 COR 2007 Emission control - Mechnical-biological treatment facilities for municipal solid waste - Corrigendum concerning guideline VDI 3475 Part 3:2006-12
VDI 2464 Blatt 3:2012-07 Ambient air measurement - Indoor air measurement - Measurement of polybrominated diphenylether, hexabromocyclododecane and hexabromobenzene by GC/MS
VDI 2262 Blatt 1:2013-06 Workplace air - Reduction of exposure to air pollutants - Legal principles, terms and definitions, basic organisational measures for industrial safety and environmental protection
VDI 3898:2013-01 Emission control - Plants for dry mechanical, physio-chemical, thermal and biological soil treatment
VDI 2102 Blatt 1:2007-04 (Draft) Emission control - Secondary copper smelting and refining plants
VDI 2102 Blatt 2:2013-04 Emission control - Copper and copper alloy melting plants
VDI 3476 Blatt 2:2010-01 Waste gas cleaning - Catalytic waste gas cleaning methods - Oxidative processes
09/30198710 DC : 0 BS EN 1948-4 - STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
12/30231398 DC : 0 BS ISO 13914 - SOIL QUALITY - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH-RESOLUTION MASS SELECTIVE DETECTION (HR GC/MS)
DIN EN 1948-4:2014-03 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
BS EN 1948-3:2006 Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Identification and quantification of PCDDs/PCDFs
UNI EN 1948-3 : 2006 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 3: IDENTIFICATION AND QUANTIFICATION OF PCDDS/PCDFS
UNI EN 1948-1 : 2006 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 1: SAMPLING OF PCDDS/PCDFS
S.R. CEN TS 1948-4:2007 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
BS ISO 16000-14:2009 Indoor air Determination of total (gas and particle-phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDDs/PCDFs). Extraction, clean-up and analysis by high-resolution gas chromatography and mass spectrometry
UNE-EN 1948-4:2011 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs
EN 1948-1:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs
EN 1948-3:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
07/30146333 DC : 0 BS ISO 16000-14 - INDOOR AIR - PART 14: DETERMINATION OF TOTAL (GAS AND PARTICLE-PHASE) POLYCHLORINATED DIOXIN-LIKE BIPHENYLS (PCBS) AND POLYCHLORINATED DIBENZO-P-DIOXINS/DIBENZOFURANS (PCDDS/PCDFS) - EXTRACTION, CLEAN-UP AND ANALYSIS BY HIGH-RESOLUTION GAS CHROMATOGRAPHY/MASS SPECTROMETRY
DD CEN/TS 15675:2007 Air quality. Measurement of stationary source emissions. Application of EN ISO/IEC 17025:2005 to periodic measurements
BS EN 1948-4 : 2010 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
S.R. CEN/TS 16190:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
DIN ISO 16000-14:2012-03 Indoor air - Part 14: Determination of total (gas and particle-phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDDs/PCDFs) - Extraction, clean-up and analysis by high-resolution gas chromatography and mass spectrometry (ISO 16000-14:2009)
17/30363999 DC : 0 BS EN 16190 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
S.R. CEN/TS 1948-5:2015 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 5: LONG-TERM SAMPLING OF PCDDS/PCDFS AND PCBS
UNI EN 1948-4 : 2014 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
ISO 13914:2013 Soil quality — Determination of dioxins and furans and dioxin-like polychlorinated biphenyls by gas chromatography with high-resolution mass selective detection (GC/HRMS)
CEN/TS 16190:2012 Sludge, treated biowaste and soil - Determination of dioxins and furans and dioxin-like polychlorinated biphenyls by gas chromatography with high resolution mass selective detection (HR GC-MS)
CEN/TS 1948-4:2007 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs

ISO 4793:1980 Laboratory sintered (fritted) filters — Porosity grading, classification and designation
EN 13284-1:2017 Stationary source emissions - Determination of low range mass concentration of dust - Part 1: Manual gravimetric method
EN 1948-1:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs
EN 1948-3:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs

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