EN 15470:2017
Current
The latest, up-to-date edition.
Liquefied petroleum gases - Determination of dissolved residues - High temperature Gas chromatographic method
05-07-2017
European foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
9 Calculations
10 Expression of results
11 Precision
Annex A (normative) - Equipment for sample transfer
and evaporation
Annex B (informative) - Examples of gas chromatograms
Bibliography
This European Standard specifies a method for determining the dissolved residual matter in liquefied petroleum gases (LPG), in the range of 40 mg/kg to 100 mg/kg. Higher concentrations can be determined by adjusting the sample size.The dissolved residue is the amount of organic compounds that are detectable by gas chromatography after evaporation of the sample at ambient temperature and then in an oven at 105 °C.This method is not suitable for detecting solid materials or for possibly high molar mass polymers (>1 000 g/mol).From the analysis of a limited LPG sample size (50 g to 75 g) this method allows obtaining information on the potential origin of the residue (gasoil, lubricants, plasticizers, etc.).The precision data of the method have been determined from 20 mg/kg to 100 mg/kg. For a higher content of residue, the precision has not been tested.NOTEAn alternative European Standard, EN 1547113[1], specifies a gravimetric method.WARNING - The use of this Standard can involve hazardous materials, operations and equipment. This Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this standard to take appropriate measures to ensure the safety and health of personnel prior to application of the standard, and fulfil statutory and regulatory requirements for this purpose.
Committee |
CEN/TC 19
|
DevelopmentNote |
Supersedes PREN 15470. (07/2017)
|
DocumentType |
Standard
|
PublisherName |
Comite Europeen de Normalisation
|
Status |
Current
|
Supersedes |
Standards | Relationship |
UNI EN 15470:2017 | Identical |
NF EN 15470 : 2008 | Identical |
UNE-EN 15470:2017 | Identical |
NS EN 15470 : 2017 | Identical |
DIN EN 15470:2016-01 (Draft) | Identical |
UNI EN 15470 : 2008 | Identical |
I.S. EN 15470:2017 | Identical |
NBN EN 15470 : 2008 | Identical |
PN EN 15470 : 2017 | Identical |
UNE-EN 15470:2008 | Identical |
BS EN 15470:2017 | Identical |
NEN EN 15470 : 2017 | Identical |
SN EN 15470:2017 | Identical |
DIN EN 15470:2017-09 | Identical |
I.S. EN 589:2008 | AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS |
12/30263426 DC : 0 | BS EN 16423 - LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUE - GAS CHROMATOGRAPHIC METHOD USING LIQUID, ON-COLUMN INJECTION |
DIN EN 16423:2014-02 | Liquefied petroleum gases - Determination of dissolved residue - Gas chromatographic method using liquid, on-column injection |
UNE-EN 15471:2017 | Liquefied petroleum gases - Determination of dissolved residues - High-temperature gravimetric method |
BS EN 589 : 2008 | AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS |
BS EN 16423:2013 | Liquefied petroleum gases. Determination of dissolved residue. Gas chromatographic method using liquid, on-column injection |
UNI EN 16423 : 2013 | LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUE - GAS CHROMATOGRAPHIC METHOD USING LIQUID, ON-COLUMN INJECTION |
15/30330673 DC : 0 | BS EN 15471 - LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD |
BS ISO 9162:2013 | Petroleum products. Fuels (class F). Liquefied petroleum gases. Specifications |
DIN EN 589:2012-06 | AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS |
DIN EN 15471:2016-01 (Draft) | LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD |
UNE-EN 589:2009 | Automotive fuels - LPG - Requirements and test methods |
EN 589:2008+A1:2012 | Automotive fuels - LPG - Requirements and test methods |
PREN 15471 : DRAFT 2015 | LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD |
ISO 9162:2013 | Petroleum products — Fuels (class F) — Liquefied petroleum gases — Specifications |
UNI EN 589 : 2013 | AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS |
BS EN 15471:2017 | Liquefied petroleum gases. Determination of dissolved residues. High-temperature gravimetric method |
EN 16423:2013 | Liquefied petroleum gases - Determination of dissolved residue - Gas chromatographic method using liquid, on-column injection |
EN 15471:2017 | Liquefied petroleum gases - Determination of dissolved residues - High-temperature gravimetric method |
I.S. EN 15471:2017 | LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD |
12/30261063 DC : 0 | BS ISO 9162 - PETROLEUM PRODUCTS - FUELS (CLASS F) - LIQUEFIED PETROLEUM GASES - SPECIFICATIONS |
I.S. EN 16423:2013 | LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUE - GAS CHROMATOGRAPHIC METHOD USING LIQUID, ON-COLUMN INJECTION |
16/30347787 DC : 0 | BS EN 589 - AUTOMOTIVE FUELS - LPG - REQUIREMENTS AND TEST METHODS |
DIN EN 15471:2017-09 | LIQUEFIED PETROLEUM GASES - DETERMINATION OF DISSOLVED RESIDUES - HIGH-TEMPERATURE GRAVIMETRIC METHOD |
EN ISO 4257:2001 | Liquefied petroleum gases - Method of sampling (ISO 4257:2001) |
ISO 4257:2001 | Liquefied petroleum gases Method of sampling |
EN 15471:2017 | Liquefied petroleum gases - Determination of dissolved residues - High-temperature gravimetric method |
ISO 4259:2006 | Petroleum products Determination and application of precision data in relation to methods of test |
EN ISO 4259:2006 | Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006) |
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