DIN EN 15527:2008-09
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS)
Hardcopy , PDF
29-07-2022
English, German
01-09-2008
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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
5.1 General
5.2 Reagents for extraction procedures
5.3 Reagents for clean-up procedures
5.4 Reagents for gas chromatographic analysis
5.5 Standards
6 Apparatus
6.1 Extraction and clean-up procedures
6.2 Gas chromatograph
6.3 Capillary columns
6.4 Preparation of standard solutions
7 Hazards
8 Interference
8.1 Interference during sampling, storage and extraction
8.2 Interference due to co-elution
9 Sample conservation
10 Pretreatment
10.1 General
10.2 Drying
10.3 Particle size reduction
11 Procedure
11.1 Blank
11.2 Extraction
11.3 Addition of the internal standard solution
11.4 Concentration or dilution
11.5 Clean up of the extract
11.6 Addition of the injection standard
11.7 Gas chromatographic analysis with mass
spectrometric detection
12 Performance characteristics
13 Test report
Annex A (informative) Representative chromatograms
Annex B (informative) Additional validation data
Annex C (informative) Summary of general requirements
and recommendations
Bibliography
National Annex NA (informative) Bibliography
Describes the quantitative determination of 16 polynuclear aromatic hydrocarbons (PAH) according to the priority list of the Environmental Protection Agency (EPA, 1982).
| DocumentType |
Standard
|
| Pages |
39
|
| PublisherName |
German Institute for Standardisation (Deutsches Institut für Normung)
|
| Status |
Superseded
|
| SupersededBy |
| Standards | Relationship |
| EN 15527:2008 | Identical |
| ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| ISO 18287:2006 | Soil quality Determination of polycyclic aromatic hydrocarbons (PAH) Gas chromatographic method with mass spectrometric detection (GC-MS) |
| DIN ISO 18287:2006-05 | Soil quality - Determination of polycyclic aromatic hydrocarbons (PAH) - Gas chromatographic method with mass spectrometric detection (GC-MS) (ISO 18287:2006) |
| DIN ISO 14507:2004-07 | SOIL QUALITY - PRETREATMENT OF SAMPLES FOR DETERMINATION OF ORGANIC CONTAMINANTS |
| EN 14346:2006 | Characterization of waste - Calculation of dry matter by determination of dry residue or water content |
| DIN ISO 22892:2006-09 | SOIL QUALITY - GUIDELINES FOR THE IDENTIFICATION OF TARGET COMPOUNDS BY GAS CHROMATOGRAPHY AND MASS SPECTROMETRY |
| ISO 16720:2005 | Soil quality Pretreatment of samples by freeze-drying for subsequent analysis |
| EN ISO 16720:2007 | Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005) |
| ISO 14507:2003 | Soil quality Pretreatment of samples for determination of organic contaminants |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
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