CR 10299:1998
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
Guidelines for the preparation of standard routine methods with wavelength-dispersive X-ray fluorescence spectrometry
31-12-1998
12-03-2025
1. Purpose of the guideline
2. Principals of the method
3. Terminology - Definitions
4. Instrumentation
5. Sampling and sample preparation
6. Evaluation methods
7. Calibration strategy
8. Validation of method (trueness and precision)
9. Performance Criteria
10. Radiation protection
ANNEX A - Bibliography
ANNEX B - Example of calculation of Background Equivalent
Concentration (BEC), Limit of Detection (LOD),
Limit of Quantification (LOQ) and Lower Limit
of Detection (LLD)
ANNEX C - Example of calculation of line interference of
molybdenum on phosphorus
ANNEX D - Example of Performance Criteria, precision test
ANNEX E - Example of two computerised SPC-diagrams
X-ray Fluorescence Spectrometry (XRF) has been used for several decades as an important analytical tool for production analysis. XRF is characterised by its speed and high precision over a wide concentration range and since the technique in most cases is used as an relative method the limitations are often connected to the quality of the calibration samples. The technique is well established and most of its physical properties are well known.
| Committee |
CEN/TC 459/SC 2
|
| DocumentType |
Report
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Withdrawn
|
| Standards | Relationship |
| NEN NPR CR 10299 : 1999 | Identical |
| XP CR 10299 : 99 XP | Identical |
| S.R. CR 10299:1999 | Identical |
| DIN EN 10315:2006-10 | Routine method for analysis of high alloy steel by X-ray Fluorescence Spectrometry (XRF) by using a near by technique |
| 13/30288139 DC : 0 | BS EN 15063-1 - COPPER AND COPPER ALLOYS - DETERMINATION OF MAIN CONSTITUENTS AND IMPURITIES BY WAVELENGTH DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY (XRF) - PART 1: GUIDELINES TO THE ROUTINE METHOD |
| BS EN 10315:2006 | Routine method for analysis of high alloy steel by X-ray fluorescence spectrometry (XRF) by using a near by technique |
| PREN 15063-1 : DRAFT 2013 | COPPER AND COPPER ALLOYS - DETERMINATION OF MAIN CONSTITUENTS AND IMPURITIES BY WAVELENGTH DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY (XRF) - PART 1: GUIDELINES TO THE ROUTINE METHOD |
| 08/30190548 DC : DRAFT DEC 2008 | BS EN ISO 17054 - ROUTINE METHOD FOR ANALYSIS OF HIGH ALLOY STEEL BY X-RAY FLUORESCENCE SPECTROMETRY (XRF) BY USING A NEAR BY TECHNIQUE |
| ISO 17054:2010 | Routine method for analysis of high alloy steel by X-ray fluorescence spectrometry (XRF) by using a near-by technique |
| DIN EN 15063-1:2015-03 | COPPER AND COPPER ALLOYS - DETERMINATION OF MAIN CONSTITUENTS AND IMPURITIES BY WAVELENGTH DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY (XRF) - PART 1: GUIDELINES TO THE ROUTINE METHOD |
| I.S. EN 15063-1:2014 | COPPER AND COPPER ALLOYS - DETERMINATION OF MAIN CONSTITUENTS AND IMPURITIES BY WAVELENGTH DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY (XRF) - PART 1: GUIDELINES TO THE ROUTINE METHOD |
| I.S. EN 10315:2006 | ROUTINE METHOD FOR ANALYSIS OF HIGH ALLOY STEEL BY X-RAY FLUORESCENCE SPECTROMETRY (XRF) BY USING A NEAR BY TECHNIQUE |
| PD CEN/TR 10261:2013 | Iron and steel. European standards for the determination of chemical composition |
| BS EN 15063-1:2014 | Copper and copper alloys. Determination of main constituents and impurities by wavelength dispersive X-ray fluorescence spectrometry (XRF) Guidelines to the routine method |
| EN 15063-1:2014 | Copper and copper alloys - Determination of main constituents and impurities by wavelength dispersive X-ray fluorescence spectrometry (XRF) - Part 1: Guidelines to the routine method |
| CEN/TR 10261:2013 | Iron and steel - European standards for the determination of chemical composition |
| EN 10315:2006 | Routine method for analysis of high alloy steel by X-ray Fluorescence Spectrometry (XRF) by using a near by technique |
| UNE-EN 15063-1:2015 | Copper and copper alloys - Determination of main constituents and impurities by wavelength dispersive X-ray fluorescence spectrometry (XRF) - Part 1: Guidelines to the routine method |
| ISO 5725-1:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions |
| ISO 5725-3:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 3: Intermediate measures of the precision of a standard measurement method |
| ISO 5725-6:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 6: Use in practice of accuracy values |
| ISO 5725-4:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 4: Basic methods for the determination of the trueness of a standard measurement method |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
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